RESEARCH ARTICLE

Effects of rotor and stator geometry on dissolution process and power consumption in jet-flow high shear mixers

  • Lin Yang 1 ,
  • Wenpeng Li , 1 ,
  • Junheng Guo 1 ,
  • Wei Li 1,3 ,
  • Baoguo Wang 2 ,
  • Minqing Zhang 1 ,
  • Jinli Zhang , 1
Expand
  • 1. School of Chemical Engineering and Technology, Tianjin University, Tianjin 300350, China
  • 2. Southern University of Science and Technology, Shenzhen 518055, China
  • 3. Beiyang National Distillation Technology Engineering Development Co., Ltd., Tianjin 300072, China

Received date: 03 Jan 2020

Accepted date: 20 Feb 2020

Published date: 15 Apr 2021

Copyright

2020 Higher Education Press

Abstract

The jet-flow high shear mixer (JF-HSM) is a new type of intensified equipment with special configurations of the rotor and the stator. The mass transfer property and power consumption were studied in the solid-liquid system for a series of JF-HSMs involving different configuration parameters, such as rotor diameter, rotor blade inclination, rotor blade bending direction, stator diameter, and stator bottom opening diameter. The flow characteristics were examined by computational fluid dynamic simulations. Results indicate that the turbulent power consumption of the JF-HSM is affected by the change in rotor blade inclination and stator bottom opening. With the increase in the shear head size and the change in the rotor into a backward-curved blade, the solid-liquid mass transfer rate can be remarkably increased under the same input power. Dimensionless correlations for the mass transfer coefficient and power consumption were obtained to guide the scale-up design and selection of such a new type of equipment to intensify the overall mixing efficiency.

Cite this article

Lin Yang , Wenpeng Li , Junheng Guo , Wei Li , Baoguo Wang , Minqing Zhang , Jinli Zhang . Effects of rotor and stator geometry on dissolution process and power consumption in jet-flow high shear mixers[J]. Frontiers of Chemical Science and Engineering, 2021 , 15(2) : 384 -398 . DOI: 10.1007/s11705-020-1928-7

Acknowledgments

This work was supported by the National Key Research and Development Program of China (Grant No. 2016YFD0501402-04), the National Natural Science Foundation of China (Grant Nos. 21776179, 21621004) and the Program for Changjiang Scholars and Innovative Research Team in University (No. IRT_15R46).
1
John T P, Fonte C P, Kowalski A, Rodgers T L. A comparison of power and flow characteristics between batch and in-line rotor-stator mixers. Chemical Engineering Science, 2019, 202: 481–490

DOI

2
James J, Cooke M, Trinh L, Hou R, Martin P, Kowalski A, Rodgers T L. Scale-up of batch rotor–stator mixers. Part 1—power constants. Chemical Engineering Research & Design, 2017, 124: 313–320

DOI

3
Utomo A T, Baker M, Pacek A W. Flow pattern, periodicity and energy dissipation in a batch rotor–stator mixer. Chemical Engineering Research & Design, 2008, 86(12): 1397–1409

DOI

4
Qin H, Xu Q, Li W, Dang X, Han Y, Lei K, Zhou L, Zhang J. Effect of stator geometry on the emulsification and extraction in the inline single-row blade-screen high shear mixer. Industrial & Engineering Chemistry Research, 2017, 56(33): 9376–9388

DOI

5
Shiba R, Uddin M A, Kato Y, Kitamura S Y. Solid/liquid mass transfer correlated to mixing pattern in a mechanically-stirred vessel. Iron and Steel Institute of Japan International, 2014, 54(12): 2754–2760

DOI

6
Yang L, Cheng J, Fan P, Yang C, Mao Z. Micromixing of solid-liquid systems in a stirred tank with double impellers. Chemical Engineering & Technology, 2013, 36(3): 443–449

DOI

7
Chen G, Luo G, Xu J, Wang J. Preparation of barium sulfate particles using filtration dispersion precipitation method in O/W system. Powder Technology, 2005, 153(2): 90–94

DOI

8
Montante G, Carletti C, Maluta F, Paglianti A. Solid dissolution and liquid mixing in turbulent stirred tanks. Chemical Engineering & Technology, 2019, 42(8): 1627–1634

DOI

9
Stoian D, Eshtiaghi N, Wu J, Parthasarathy R. Enhancing impeller power efficiency and solid–liquid mass transfer in an agitated vessel with dual impellers through process intensification. Industrial & Engineering Chemistry Research, 2017, 56(24): 7021–7036

DOI

10
Tokura Y, Uddin M A, Kato Y. Effect of suspension pattern of sedimentary particles on solid/liquid mass transfer in a mechanically stirred vessel. Industrial & Engineering Chemistry Research, 2019, 58(24): 10172–10178

DOI

11
Viten’ko T N, Gumnitskii Y M. Mass transfer during dissolution of solids using hydrodynamic cavitation devices. Theoretical Foundations of Chemical Engineering, 2006, 40(6): 598–603

DOI

12
Myers K J, Reeder M F, Ryan D. Power draw of a high-shear homogenizer. Canadian Journal of Chemical Engineering, 2001, 79(1): 94–99

DOI

13
Padron G. Measurement and comparison of power draw in batch rotor-stator mixers. Dissertation for the Master’s Degree. Maryland: University of Maryland, 2001, 126–127

14
Doucet L, Ascanio G, Tanguy P A. Hydrodynamics characterization of rotor-stator mixer with viscous fluids. Chemical Engineering Research & Design, 2005, 83(10): 1186–1195

DOI

15
James J, Cooke M, Kowalski A, Rodgers T L. Scale-up of batch rotor-stator mixers. Part 2—Mixing and emulsification. Chemical Engineering Research & Design, 2017, 124: 321–329

DOI

16
Carletti C, Montante G, De Blasio C, Paglianti A. Liquid mixing dynamics in slurry stirred tanks based on electrical resistance tomography. Chemical Engineering Science, 2016, 152: 478–487

DOI

17
Altheimer M, Becker D, D’Aleo F P, Rudolf von Rohr P. Flow regime and liquid–solid mass transfer investigation in a designed porous structure using electrochemical micro-probes. Chemical Engineering Science, 2016, 152: 699–708

DOI

18
Paglianti A, Carletti C, Busciglio A, Montante G. Solid distribution and mixing time in stirred tanks: The case of floating particles. Canadian Journal of Chemical Engineering, 2017, 95(9): 1789–1799

DOI

19
Koganti V, Carroll F, Ferraina R, Falk R, Waghmare Y, Berry M, Liu Y, Norris K, Leasure R, Gaudio J. Application of modeling to scale-up dissolution in pharmaceutical manufacturing. American Association of Pharmaceutical Scientists PharmSciTech, 2010, 11(4): 1541–1548

DOI

20
Håkansson A, Mortensen H H, Andersson R, Innings F. Experimental investigations of turbulent fragmenting stresses in a rotor-stator mixer. Part 1. Estimation of turbulent stresses and comparison to breakup visualizations. Chemical Engineering Science, 2017, 171: 625–637

DOI

21
Qi N, Wang H, Zhang K, Zhang H. Numerical simulation of fluid dynamics in the stirred tank by the SSG Reynolds Stress Model. Frontiers of Chemical Engineering in China, 2010, 4(4): 506–514

DOI

22
Jasińska M. Test reactions to study efficiency of mixing. Chemical & Process Engineering, 2015, 36(2): 171–208

DOI

23
John T P, Panesar J S, Kowalski A, Rodgers T L P, Fonte C. Linking power and flow in rotor-stator mixers. Chemical Engineering Science, 2019, 207: 504–515

DOI

24
Xu S, Cheng Q, Li W, Zhang J. LDA measurements and CFD simulations of an in-line high shear mixer with ultrafine teeth. AIChE Journal. American Institute of Chemical Engineers, 2014, 60(3): 1143–1155

DOI

25
Levins D, Glastonbury J. Application of Kolmogorofff’s theory to particle—liquid mass transfer in agitated vessels. Chemical Engineering Science, 1972, 27(3): 537–543

DOI

26
Harriott P. Mass transfer to particles: Part I. Suspended in agitated tanks. AIChE Journal. American Institute of Chemical Engineers, 1962, 8(1): 93–101

DOI

27
Nienow A W, Miles D. The effect of impeller/tank, configurations on fluid-particle mass transfer. Chemical Engineering Journal, 1978, 15(1): 13–24

DOI

28
Pangarkar V G, Yawalkar A A, Sharma M M, Beenackers A A C M. Particle-liquid mass transfer coefficient in two-/three-phase stirred tank reactors. Industrial & Engineering Chemistry Research, 2002, 41(17): 4141–4167

DOI

29
Bong E. Solid-liquid mass transfer in agitated vessels with high solids concentration. Dissertation for the Doctoral Degree. Melbourne: Royal Melbourne Institute of Technology University, 2013, 47–58

30
Özcan-Taşkın G, Kubicki D, Padron G. Power and flow characteristics of three rotor-stator heads. Canadian Journal of Chemical Engineering, 2011, 89(5): 1005–1017

DOI

31
Cooke M, Rodgers T L, Kowalski A J. Power consumption characteristics of an in-line silverson high shear mixer. AIChE Journal. American Institute of Chemical Engineers, 2012, 58(6): 1683–1692

DOI

32
Carletti C, Bikić S, Montante G, Paglianti A. Mass transfer in dilute solid–liquid stirred tanks. Industrial & Engineering Chemistry Research, 2018, 57(18): 6505–6515

DOI

33
Bong E Y, Eshtiaghi N, Wu J, Parthasarathy R. Optimum solids concentration for solids suspension and solid–liquid mass transfer in agitated vessels. Chemical Engineering Research & Design, 2015, 100: 148–156

DOI

Outlines

/