Optimization of the main liming process for inulin crude extract from Jerusalem artichoke tubers

Huandong LI , Hongji ZHU , Jianjun QIAO , Junhu DU , Hua ZHANG

Front. Chem. Sci. Eng. ›› 2012, Vol. 6 ›› Issue (3) : 348 -355.

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Front. Chem. Sci. Eng. ›› 2012, Vol. 6 ›› Issue (3) : 348 -355. DOI: 10.1007/s11705-012-1295-0
RESEARCH ARTICLE
RESEARCH ARTICLE

Optimization of the main liming process for inulin crude extract from Jerusalem artichoke tubers

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Abstract

A three-stage homogenate extraction was used as a new method for inulin extraction from Jerusalem artichoke tubers. Compared with the results from conventional hot water extraction, the three-stage homogenate extraction gave higher yields and caused less degradation of the inulin. The inulin crude extract was then clarified by a carbonate-precipitation method, during which three variables — the quicklime mass, the reaction temperature and the reaction time were optimized for the main liming process to give the best clarification effect. A Plackett-Burman design, the path of steepest ascent method, a Box-Behnken design and response surface methodology (RSM) were employed in the experimental design. The optimal conditions for the main liming process were determined to be 12.0 g/L, 71.4°C and 8 min. The confirmatory tests proved that the best clarification efficiency (92.74%) was achieved at these conditions and this was approximately equal to the value predicted by the model.

Keywords

inulin / homogenate extraction / Jerusalem artichoke / main liming process

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Huandong LI, Hongji ZHU, Jianjun QIAO, Junhu DU, Hua ZHANG. Optimization of the main liming process for inulin crude extract from Jerusalem artichoke tubers. Front. Chem. Sci. Eng., 2012, 6(3): 348-355 DOI:10.1007/s11705-012-1295-0

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References

[1]

Carpita N C, Kanabus J, Housley T L. Linkage structure of fructans and fructan oligomers from Triticum aestivum and Festuca arundinacea leaves. Journal of Plant Physiology, 1989, 134(2): 162–168

[2]

Niness K R. Inulin and oligofructose: what are they? Journal of Nutrition, 1999, 129(7 Suppl): 1402S–1406S

[3]

van Loo J, Coussement P, de Leenheer L, Hoebregs H, Smits G. On the presence of inulin and oligofructose as natural ingredients in the western diet. Critical Reviews in Food Science and Nutrition, 1995, 35(6): 525–552

[4]

Roberfroid M B. Inulin-type fructans: functional food ingredients. Journal of Nutrition, 2007, 137(11 Suppl): 2493S–2502S

[5]

Chen Q, Zhang M, Shen S. Effect of salt on malondialdehyde and antioxidant enzymes in seedling roots of Jerusalem artichoke (Helianthus tuberosus L.). Acta Physiologiae Plantarum, 2011, 33(2): 273–278

[6]

Huang J, Cai J, Wang J, Zhu X, Huang L, Yang S T, Xu Z. Efficient production of butyric acid from Jerusalem artichoke by immobilized Clostridium tyrobutyricum in a fibrous-bed bioreactor. Bioresource Technology, 2011, 102(4): 3923–3926

[7]

Kocsis L, Liebhard P, Praznik W. Effect of seasonal changes on content and profile of soluble carbohydrates in tubers of different varieties of Jerusalem artichoke (Helianthus tuberosus L.). Journal of Agriculture and Chemical, 2007, 55(23): 9401–9408

[8]

The Ministry of public health of the People’s Republic of China. Announcement on approval inulin and polyfructose as novel food by the Minstry of Public Health. Beijing: The Ministry of Public Health of PRC, 2009 (in Chinese)

[9]

Matusek A, Merész P, Le T K D, Örsi F. Effect of temperature and pH on the degradation of fructo-oligosaccharides. European Food Research and Technology, 2009, 228(3): 355–365

[10]

Wei L, Wang J, Zheng X, Teng D, Yang Y, Cai C, Feng T, Zhang F. Studies on the extracting technical conditions of inulin from Jerusalem artichoke tubers. Journal of Food Engineering, 2007, 79(3): 1087–1093

[11]

Holford K C, Edwards K A, Bendena W G, Tobe S S, Wang Z, Borst D W. Purification and characterization of a mandibular organ protein from the American lobster, Homarus americanus: a putative farnesoic acid O-methyltransferase. Insect Biochemistry and Molecular Biology, 2004, 34(8): 785–798

[12]

Malpiedi L P, Picó G A, Nerli B B. Studies of protein partition in non conventional aqueous two-phase systems as method to purify trypsinogen and alpha-chymotrypsinogen from bovine pancreas. Separation and Purification Technology, 2011, 78(1): 91–96

[13]

Sezgintürk M K, Dinçkaya E. An amperometric inhibitor biosensor for the determination of reduced glutathione (GSH) without any derivatization in some plants. Biosensors & Bioelectronics, 2004, 19(8): 835–841

[14]

McCarron P, Emteborg H, Nulty C, Rundberget T, Loader J I, Teipel K, Miles C O, Quilliam M A, Hess P. A mussel tissue certified reference material for multiple phycotoxins. Part 1: design and preparation. Analytical and Bioanalytical Chemistry, 2011, 400(3): 821–833

[15]

Poel P W, Schiweck H, Schwartz T. Sugar Technology. Beet and Cane Sugar Manufacture. Berlin: Bartens, 1998, 88–107

[16]

Bubnik Z, Kadlek P, Urban D, Bruhns M. Sugar Technologists Manual: Chemical and Physical Data for Sugar Manufactures and Users. Berlin: Bartens, 1995, 43–86

[17]

Saengthongpinit W, Sajjaanantakul T. Influence of harvest time and storage temperature on characteristics of inulin from Jerusalem artichoke (Helianthus tuberosus L.) tubers. Postharvest Biology and Technology, 2005, 37(1): 93–100

[18]

Vámos-Vigyázó L, Haard N F. Polyphenol oxidase and peroxidase in fruits and vegetables. Critical Reviews in Food Science and Nutrition, 1981, 15(1): 49–127

[19]

Vukov K. Absorption function of calcium carbonate on coloring matter. Sugar Journal, 1977, 39(8): 15–18 (in Chinese)

[20]

Reddy L V A, Wee Y J, Yun J S, Ryu H W. Optimization of alkaline protease production by batch culture of Bacillus sp. RKY3 through Plackett-Burman and response surface methodological approaches. Bioresource Technology, 2008, 99(7): 2242–2249

[21]

Ferreira S L C, Bruns R E, Ferreira H S, Matos G D, David J M, Brandão G C, da Silva E G P, Portugal L A, dos Reis P S, Souza A S, dos Santos W N L. Box-Behnken design: an alternative for the optimization of analytical methods. Analytica Chimica Acta, 2007, 597(2): 179–186

[22]

Toneli J T C, Murr F E X, Martinelli P, Dal Fabbro I M. Optimization of a physical concentration process for inulin. Journal of Food Engineering, 2007, 80(3): 832–838

[23]

Miller G L. Use of dinitrosalicylic acid reagent for determination of reducing sugar. Analytical Chemistry, 1959, 31(3): 426–428

[24]

Dubois M, Gilles K A, Hamilton J K, Rebers P A, Smith F. Colorimetric method for determination of sugar and related substances. Analytical Chemistry, 1956, 28(3): 350–356

[25]

Spector T. Refinement of the coomassie blue method of protein quantification: A simple and linear spectrophotometric assay for 0.5 to 50 μg of protein. Analytical Biochemistry, 1978, 86(1): 142–146

[26]

Kuntz J B. Determination of sucrose turbidity and color value. China Beet Sugar, 1994, 1: 62–64 (in Chinese)

[27]

Zhou C, Fu B. Concise Handbook of Analytical Chemistry. Beijing: Chemical Industry Press, 2010, 45–60 (in Chinese)

[28]

van Waes C, Baert J, Carlier L, van Bockstaele E. A rapid determination of the total sugar content and the average inulin chain length in roots of chicory (Cichorium intybus L). Journal of the Science of Food and Agriculture, 1998, 76(1): 107–110

[29]

Takeuchi J, Nagashima T. Preparation of dried chips from Jerusalem artichoke (Helianthus tuberosus) tubers and analysis of their functional properties. Food Chemistry, 2011, 126(3): 922–926

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