Enhancing P(AM-co-AA) hydrogel performance: Dual crosslinking effects on structural strength, thermal stability, swelling capacity, and rheological behavior for effective sand production control in oil reservoirs

Abstract

The effici ciency of mechanical methods in controlling water production and fine migration in reservoirs has been limited, prompting researchers to focus on developing more resilient chemical methods. However, the challenge lies in the limited resistance and stability of these chemical methods in harsh reservoir conditions. To address this challenge, a study evaluated a dual crosslinker polyethyleneimine compound as a double crosslink in hydrogel composite structures. Using FTIR techniques, the study examined the structure of hydrogel compounds with single and double crosslinkers. Microscopic imaging, including SEM and ESEM analyses, provided insights into sample morphology. Equilibrium swelling and rheological tests assessed the hydrogels' three-dimensional structure and solvent retention capacity, while TGA determined sample stability. The study confirm rmed chemical bond formation between double crosslinkers via FTIR analysis. SEM and ESEM images displayed a porous, homogeneous, three-dimensional structure. The increase in pore size in the swollen state without tearing highlighted the hydrogel's elastic and self-healing properties. TGA revealed reduced weight loss with double crosslinking at 120 ° C. Strain sweep and frequency sweep tests demonstrated enhancements in critical strain and frequency with the dual crosslinker, supporting the sample's viscoelastic behavior. The hydrogel with a single crosslink maintained linear viscoelastic behavior up to 85 ° C, while the dual crosslinked sample retained it up to 200 ° C, suitable for high-temperature conditions. Swelling tests confirm rmed the sample's ability to absorb 2000% of water under reservoir conditions. Sandpack compressive strength testing indicated a fivefold increase in strength with the dual crosslinked hydrogel composite, effectively preventing fine migration.

Keywords

Sand control / Water management / Hydrogel composites / Dual crosslinking / Rheology

CRediT authorship contribution statement

Fardin Saghandali: Writing-original draft, Data curation, Methodology, Visualization. Mahsa Baghban Salehi: Validation, Project administration, Writing-review & editing, Resources, Funding acquisition, Conceptualization, Supervision, Investigation. Farzin Saghandali: Writing-review & editing, Formal analysis, Investigation, Writing-original draft, Data curation. Vahid Taghikhani: Validation, Supervision.

Declaration of competing interest

The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influe uence the work reported in this paper.

Acknowledgements

The authors would like to acknowledge the support of the Iran Nanotechnology Innovation Council (INIC) with Project No. of 4031705 in this study.

References

[1] P.G. Ranjith, M.S.A. Perera, W.K.G. Perera, S.K. Choi, E. Yasar, Sand production during the extrusion of hydrocarbons from geological formations: a review, J. Pet. Sci. Eng. 124 (2014) 72-82, https://doi.org/10.1016/j.petrol.2014.10.017.

[2] M. Bajus, Petrochemistry: Petrochemical Processing, Hydrocarbon Technology and Green Engineering, John Wiley & Sons, 2020.

[3] A.O. Gbadamosi, R. Junin, M.A. Manan, A. Agi, A.S. Yusuff, An Overview of Chemical Enhanced Oil Recovery: Recent Advances and Prospects, Springer Berlin Heidelberg, 2019, https://doi.org/10.1007/s40089-019-0272-8.

[4] S. Aghaei, F. Saghandali, M.B. Salehi, B. Mokhtarani, V. Taghikhani, S. Saviz, A micromodel investigation on the flooding of glycolipid biosurfactants for enhanced oil recovery, Geoenergy Sci. Eng. 230 (2023) 212219.

[5] A.M. Moghadam, M.V. Sefti, M.B. Salehi, H. Naderi, Bulk and rheological properties of polyacrylamide hydrogels for water shutoff treatment, Kor. J. Chem. Eng. 31 (2014) 532-539.

[6] M. Abedi Lenji, M. Vafaie Sefti, M. Baghban Salehi, A. Mousavi Moghadam, H. Naderi, Gelation time of hexamethylenetetramine polymer gels used in water shutoff treatment, J. Petrol. Sci. Technol. 2 (2012) 3-11.

[7] M.B. Salehi, A.M. Moghadam, K. Jarrahian, Effect of network parameters of preformed particle gel on structural strength for water management, SPE Prod. Oper. 35 (2020) 362-372, https://doi.org/10.2118/193631-PA.

[8] M.A. Lenji, M. Haghshenasfard, M.V. Sefti, M.B. Salehi, A. heidari, Experimental study of swelling and rheological behavior of preformed particle gel used in water shutoff treatment, J. Pet. Sci. Eng. 169 (2018) 739-747, https://doi.org/10.1016/j.petrol.2018.06.029.

[9] F. Saghandali, M. Baghban Salehi, R. Hosseinzadehsemnani, R.G. Moghanloo, V. Taghikhani, A review on chemical sand production control techniques in oil reservoirs, Energy Fuels (2022), https://doi.org/10.1021/acs.energyfuels.2c00700.

[10] L. Zhang, F. Zhou, S. Zhang, Y. Wang, J. Wang, J. Wang, Investigation of water-sensitivity damage for tight low-permeability sandstone reservoirs, ACS Omega 4 (2019) 11197-11204, https://doi.org/10.1021/acsomega.9b01286.

[11] F. Paskvan, J. Turak, G. Jerauld, T. Gould, R. Skinner, A. Garg, Alaskan viscous oil: EOR opportunity, or waterfloo ood sand control first?, in:SPE Western Regional Meeting, 2016. OnePetro.

[12] J. Robles, F. Sapag, L. Sanchez, W. Morris, H. Peacock, J. Bravo,Cementing unconsolidated sandstone formations with coexisting oil and water, in: SPE Latin American and Caribbean Petroleum Engineering Conference Proceedings, vol. 2, 2012, pp. 941-952, https://doi.org/10.2118/152977-ms.

[13] M.B. Salehi, E. Vasheghani-Farahani, M.V. Sefti, A.M. Moghadam, H. Naderi, Rheological and transport properties of sulfonated polyacrylamide hydrogels for water shutoff in porous media, Polym. Adv. Technol. 25 (2014) 396-405.

[14] F. Salimi, M.V. Sefti, K. Jarrahian, M. Rafipoor, S.S. Ghorashi, Preparation and investigation of the physical and chemical properties of clay-based polyacrylamide/Cr (III) hydrogels as a water shut-off agent in oil reservoirs, Kor. J. Chem. Eng. 31 (2014) 986-993.

[15] F. Mohd Noordin, M.H.A. Razak, M. Ismail, Case study: water shut-off mechanism in Small, remote platform-process & challenge,in: 8th European Formation Damage Conference, 2009. OnePetro.

[16] S.U.N. Xindi, B.A.I. Baojun, Comprehensive review of water shutoff methods for horizontal wells, Petrol. Explor. Dev. 44 (2017) 1022-1029.

[17] A. Taha, M. Amani, Overview of water shutoff operations in oil and gas wells; chemical and mechanical solutions, ChemEngineering 3 (2019) 51.

[18] S. Mohammadi, M. Vafaie Sefti, M. Baghban Salehi, A. Mousavi Moghadam, S. Rajaee, H. Naderi, Hydrogel swelling properties: comparison between conventional and nanocomposite hydrogels for water shutoff treatment, Asia Pac. J. Chem. Eng. 10 (2015) 743-753.

[19] S. Vossoughi, Profile modifica tion using in situ gelation technology — a review, J. Pet. Sci. Eng. 26 (2000) 199-209.

[20] Y. Song, C.-S. Lee, In situ gelation of monodisperse alginate hydrogel in microflui uidic channel based on mass transfer of calcium ions, Korean Chem. Eng. Res. 52 (2014) 632-637.

[21] J. Du, Q. Wang, P. Liu, G. Xiong, P. Chen, X. Chen, J. Liu, Nanocomposite gels for water shut-off and temporary plugging in the petroleum industry: a review, Petrol. Sci. Technol. 41 (2023) 2204-2239.

[22] Z. Xiong, F. Fu, Z. Zou, X. Li, S. Tao, Y. Li, Development and application of guar gum crosslinked gel with adjustable gelation time for total loss treatment, Petroleum 9 (2022) 621-628.

[23] F. Saghandali, M.B. Salehi, V. Taghikhani, Iran. Polym. J. (Improved oil recovery by 3D hydrogel composite reinforced with natural bentonite nanoparticles, Engl. Ed.) 32 (2023) 1393-1404.

[24] F. Saghandali, M.B. Salehi, V. Taghikhani, Hydrogel nanocomposite network elasticity parameters as a function of swelling ratio: from micro to macro flooding, J. Ind. Eng. Chem. 125 (2023) 163-177.

[25] F. Aqcheli, M.B. Salehi, H. Pahlevani, V. Taghikhani, Rheological properties and the micromodel investigation of nanosilica gel-reinforced preformed particle gels developed for improved oil recovery, J. Pet. Sci. Eng. 192 (2020), https://doi.org/10.1016/j.petrol.2020.107258.

[26] H. Jia, J. Wu, S. Wu, Y. Liang, M. Wang, X. Wan, P. Li, New insights into the DPR mechanism of elastic energy released by polymer gel for enhanced oil recovery, Petroleum 10 (2022) 539-547.

[27] F. Saghandali, M.B. Salehi, V. Taghikhani, Design and fabrication of a Preformed Thixotropic-Viscoelastic Nanocomposite hydrogel system (PNCH) for controlling sand production in reservoirs, Results Eng. 18 (2023) 101089.

[28] H. Jia, Q. Ren, Y.M. Li, X.P. Ma, Evaluation of polyacrylamide gels with accelerator ammonium salts for water shutoff in ultralow temperature reservoirs: gelation performance and application recommendations, Petroleum 2 (2016) 90-97.

[29] F. Aqcheli, M.B. Salehi, H. Pahlevani, V. Taghikhani, Rheological properties and the micromodel investigation of nanosilica gel-reinforced preformed particle gels developed for improved oil recovery, J. Pet. Sci. Eng. 192 (2020) 107258, https://doi.org/10.1016/j.petrol.2020.107258.

[30] F. Saghandali, M. Baghban Salehi, V. Taghikhani, Synthesis of Cobalt nanocomposite hydrogel based on Acrylamide as an effici ent chemical for sand control in the oil reservoir, Iran. J. Polym. Sci. Technol. 35 (2023) 529-540.

[31] N. Lai, S. Chen, L. Tang, Y. Huang, H. Xu, Migration characteristics and profile le control capabilities of preformed particle gel in porous media, Petroleum 8 (2022) 483-498.

[32] F. Saghandali, M.B. Salehi, H. Pahlevani, V. Taghikhani, S. Riahi, M. Ebrahimi, S. Saviz, A. Roomi, Fabrication of a hydrogel reinforced with titanium nanoparticles to reduce fine migration and remediation of formation damage during low-salinity waterfloo ooding, Geoenergy Sci. Eng. 241 (2024) 213173.

[33] Y. Bao, J. Ma, N. Li, Synthesis and swelling behaviors of sodium carboxymethyl cellulose-g-poly(AA-co-AM-co-AMPS)/MMT superabsorbent hydrogel, Carbohydr. Polym. 84 (2011) 76-82, https://doi.org/10.1016/j.carbpol.2010.10.061.

[34] R. Mahon, Y. Balogun, G. Oluyemi, J. Njuguna, Swelling performance of sodium polyacrylate and poly(acrylamide-co-acrylic acid) potassium salt, SN Appl. Sci. 2 (2020), https://doi.org/10.1007/s42452-019-1874-5.

[35] M. Seidy Esfahlan, E. Khodapanah, S.A. Tabatabaei-Nezhad, M. Salami-Kalajahi, Fabrication, optimization and characterization of preformed-particle-gel containing nanogel particles for conformance control in oil reservoirs, Polym. Bull. 79 (2022) 7137-7159.

[36] S. Amiri, A. Asghari, V. Vatanpour, M. Rajabi, Fabrication of chitosan-aminopropylsilane graphene oxide nanocomposite hydrogel embedded PES membrane for improved filtration performance and lead separation, J. Environ. Manag. 294 (2021) 112918, https://doi.org/10.1016/j.jenvman.2021.112918.

[37] A. Pourjavadi, R. Soleyman, G.R. Bardajee, S. Ghavami, Novel superabsorbent hydrogel based on natural hybrid backbone: optimized synthesis and its swelling behavior, Bull. Kor. Chem. Soc. 30 (2009) 2681.

[38] S. Hezari, A. Olad, A. Dilmaghani, Modified ed gelatin/iron- based metal-organic framework nanocomposite hydrogel as wound dressing: synthesis, antibacterial activity, and Camellia sinensis release, Int. J. Biol. Macromol. 218 (2022) 488-505, https://doi.org/10.1016/j.ijbiomac.2022.07.150.

[39] F. Saghandali, M. Kazemeini, S. Sadjadi, Halloysite-supported silicotungstic acid as an effici ent catalyst for dehydration of fructose to 5-hydroxymethylfurfural, J. Phys. Chem. Solid. 184 (2024) 111697.

[40] J. Aalaie, A. Rahmatpour, E. Vasheghani-Farahani, Rheological and swelling behavior of semi-interpenetrating networks of polyacrylamide and scleroglucan, Polym. Adv. Technol. 20 (2009) 1102-1106.

[41] S. Wang, H. Tang, J. Guo, K. Wang, Effect of pH on the rheological properties of borate crosslinked hydroxypropyl guar gum hydrogel and hydroxypropyl guar gum, Carbohydr. Polym. 147 (2016) 455-463.

[42] U.L.F. Gedde, Polymer Physics, Springer Science & Business Media, 1995.

[43] B. Wang, A.G. Moura, J. Chen, A. Erturk, Y. Hu, Characterization of hydrogel structural damping, Extreme Mech. Lett. 40 (2020) 100841.

[44] M. Ge, L. Zhang, Ultrastretchable hydrogels with strong damping effects, Polym. J. (2024) 1-9.

[45] G. Stojkov, Z. Niyazov, F. Picchioni, R.K. Bose, Relationship between structure and rheology of hydrogels for various applications, Gels 7 (2021) 255.

[46] F. Ganji, F.S. Vasheghani, F.E. Vasheghani, Theoretical Description of Hydrogel Swelling: a Review, 2010.

[47] N.-H. Kim, T.H. Lee, J.S. Choi, Swelling equilibria of polymeric hydrogels containing poly (acrylamidesodiumallylsulfonate-acrylic acid), Kor. J. Chem. Eng. 17 (2000) 534-540.

[48] M.A. Lenji, M. Haghshenasfard, M.V. Sefti, M.B. Salehi, A.M. Moghadam, Numerical modeling and experimental investigation of inorganic and organic crosslinkers effects on polymer gel properties, J. Pet. Sci. Eng. 160 (2018) 160-169.

[49] A.M. Moghadam, M.V. Sefti, M.B. Salehi, H. Naderi, Preparation an optimal hydrogel of water shutoff for Iranian oilfield, J. Petrol. Res. Stud. 5 (2014) 169-181.

[50] T. Zhao, J. Peng, Y. Zhang, J. Chen, Y. Chen, W. Sun, S. Li, Synthesis of ultra-high concentration of salt-resistant polyacrylamide, Polym. Adv. Technol. 31 (2020) 2980-2989.