Heterogeneous twin structure and spontaneous plastic strain evolution in extruded AZ31 Mg alloy under multi-degree-of-freedom reciprocating torsion-compression

Mingyang Jiao , Xuejian Yang , Zhijia Liu , Ruihong Li , Baodong Shi , Yan Peng , Xianhua Chen

Microstructures ›› 2026, Vol. 6 ›› Issue (2) -2026046.

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Microstructures ›› 2026, Vol. 6 ›› Issue (2) -2026046. DOI: 10.20517/microstructures.2025.105
Research Article
Heterogeneous twin structure and spontaneous plastic strain evolution in extruded AZ31 Mg alloy under multi-degree-of-freedom reciprocating torsion-compression
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Abstract

The microstructural evolution and mechanical responses under multi-degree-of-freedom reciprocating torsion-compression deformations remain to be fully elucidated, particularly regarding the Swift and inverse Swift effects and their physical mechanisms, which constrain the design and formability of textured Mg alloys. Therefore, the multi-degree-of-freedom reciprocating pre-torsional-compressive loadings along extrusion direction (ED) were specifically designed. The twinning behaviours and the radial distribution of twin structures were systematically analysed. The driving mechanisms of the Swift and subsequent inverse Swift effects were discussed. Results demonstrated that free end torsion (FET) deformation induced radially linear-gradient twinning structure, while reverse FET (RFET) loading triggered FET twins detwinning and extensive {10$ \bar{1} $2} tensile twin activation within the basal textures, driving the reverse FET twin texture further tend towards ED aggregation. FET twins inhibited the nucleation of RFET twins, resulting in the formation of a distinctive inverse-gradient twinning structure. 65% of the Swift-effect strain under low-strain FET (γ < 0.12) was coordinated by dislocation slip, whereas the misfit strain induced by FET twins accommodated more than 85% of the axial shortening during γFET = 0.38. RFET-stage axial elongation was governed by detwinning, with subsequent axial shortening attributable to large-scale RFET twin activation. {10$ \bar{1} $2} tensile twins dominated initial free rotational compression (FRC) strain, the interactions between the release of residual shear stress and the reverse shear strain component induced by FRC twins results in the circumferential motionlessness during initial FRC. Proliferation of FRC twins promoted cumulative circumferential shear strain component, inducing further macroscopic reverse spontaneous rotation.

Keywords

Magnesium alloy / multi-degree-of-freedom / reciprocating torsion / compression / twinning / inverse Swift effect

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Mingyang Jiao, Xuejian Yang, Zhijia Liu, Ruihong Li, Baodong Shi, Yan Peng, Xianhua Chen. Heterogeneous twin structure and spontaneous plastic strain evolution in extruded AZ31 Mg alloy under multi-degree-of-freedom reciprocating torsion-compression. Microstructures, 2026, 6(2): -2026046 DOI:10.20517/microstructures.2025.105

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References

[1]

Chen Y.,Liu F.,Wu Y..et al. Outstanding fatigue performance of Mg-Gd-Zn-Zr alloy enriched with SFs rather than LPSO Structure J. Magnes. Alloys 2025 13 90 100

[2]

Mouhib F.,Xie Z.,Atila A.,Guénolé J.,Korte-kerzel S.,Al-samman T.. Exploring solute behavior and texture selection in magnesium alloys at the atomistic level Acta Mater. 2024 266 119677

[3]

Qu X.,Li G.,Wang F..et al. In-situ electrochemical activation accelerates the magnesium-ion storage Nat. Commun. 2025 16 1310 PMC11791179

[4]

Cui Y.,Guo L.,Gui Y..et al. Segregation behaviors in {10$ \bar{1} $1} compressive twin boundaries of Mg-RE alloy under deformation at room temperature J. Magnes. Alloys 2025 13 330 7

[5]

Wang A.,Chen X.,Li Q..et al. Hot deformation behavior and microstructure evolution of Mg-Gd-Sm(-Zn)-Zr alloys Int. J. Miner. Metall. Mater. 2025 32 1162 75

[6]

Gautam P. C.,Biswas S.. Anisotropic compressive deformation behavior of hot-rolled Mg-3Al-0.5Ce alloy J. Magnes. Alloys 2024 12 4646 66

[7]

Song Y.,Li X.,Xu J..et al. Effect of annealing treatment on the microstructure and mechanical properties of warm-rolled Mg-Zn-Gd-Ca-Mn alloys Int. J. Miner. Metall. Mater. 2024 31 2208 20

[8]

Wang H.,Zhang X.,Wu W..et al. On the torsional and coupled torsion-tension/compression behavior of magnesium alloy solid rod: a crystal plasticity evaluation Int. J. Plast. 2022 151 103213

[9]

Chaudry U. M.,Tariq H. M. R.,Zubair M.,Ansari N.,Jun T.. Implications of twinning on the microstructure development, crystallographic texture and mechanical performance of Mg alloys- a critical review J. Magnes. Alloys 2023 11 4146 65

[10]

Han Y.,Chen S.,Wan Y.,Liu C.,Chen Z.. Microstructure, texture evolution and mechanical anisotropy of Mg-Gd-Y-Zn-Zr alloy sheets produced by unidirectional and cross rolling Mater. Sci. Eng. A 2024 893 146127

[11]

Li J.,Chen H.,Wu D.,Chen R.,Song J.,Yi X.. Strain rate-dependent tension-compression asymmetry in cast Mg-Gd-Y alloy: Insights into slip and twinning mechanisms J. Mater. Sci. Technol. 2025 219 134 46

[12]

Zhang J.,Ye Y.,Li Z.,Chen X.,Wang W.,Huang G.. Unveiling the mechanical anisotropy and related deformation mechanisms of heterostructured Mg alloy laminate with unique texture feature J. Alloys Compd. 2025 1010 177404

[13]

Zhang C.,Yang G.,Xiao L..et al. Effects of the extrusion parameters on microstructure, texture and room temperature mechanical properties of extruded Mg-2.49Nd-1.82Gd-0.2Zn-0.2Zr alloy Int. J. Miner. Metall. Mater. 2024 32 136 46

[14]

Li Z.,Zhang J.,Xiao T..et al. Regulating microstructure and improving precipitation hardening response of fine-grained Mg-RE-Ag hot-extruded alloy by extreme short-time heat treatment Mater. Sci. Eng. A 2024 892 146059

[15]

Yang Y.,Wang J.,Ferdowsi M. R. G..et al. A coupled model for precipitation strengthening in Mg-Zn alloys Acta Mater. 2024 281 120392

[16]

Zhang Z.,Hou S.,Wang H.,Zhang D.,Zhang J.. Achieving microstress-induced strengthening and grain refinement of crossover Al-Mg-Zn-Cu alloy via deformation-induced precipitation of multiscale T-phase Mg32(Al Zn Cu)49 J. Alloys Compd. 2024 988 174296

[17]

Rezaei A.,Mahmudi R.,Logé R.. Microstructural and hardness homogeneity in an Mg-Gd-Y-Ag alloy processed by simple shear extrusion Mater. Sci. Eng. A 2023 876 145159

[18]

Bayat Tork N.,Saghafian H.,Razavi S.,Al-fadhalah K.,Ebrahimi R.,Mahmudi R.. Microstructure and texture characterization of Mg-Al and Mg-Gd binary alloys processed by simple shear extrusion J. Mater. Res. Technol. 2019 8 1288 99

[19]

Wu F.,Jiang F.,Ye P.,Su Y.,Long M.. A bimodal grain structured Al-Mg-Sc-Zr alloy with excellent strength and ductility by the combination of hot rolling and thermal-ECAP Mater. Today Commun. 2025 43 111632

[20]

Zhou X.,Xia H.,Zhang J..et al. Effect of ECAP temperature and deformation route on mechanical properties of pre-extruded Mg-5Gd-3Y-1Zn-0.5Zr alloys J. Mater. Sci. Technol. 2025 212 237 50

[21]

Li C.,Kim R.,Qiao X..et al. Achieving exceptional room-temperature ductility in ultrafine-grained Mg-0.8Mn alloy via high pressure torsion J. Alloys Compd. 2025 1020 179411

[22]

Ren X.,An X.,Ni S.,Huang Y.,Song M.. Formation of nanocrystalline grain structure in an Mg-Gd-Y-Zr alloy processed by high-pressure torsion Mater. Charact. 2022 191 112088

[23]

Tian L.,Wang L.,Chen X..et al. Optimal design and fabrication of thin‑walled microtubules via a novel screw twist extrusion technology on Mg-Zn-Nd-Y alloy J. Alloys Compd. 2025 1010 178301

[24]

Wang K.,Wang X.,Luo C..et al. A generic framework for tailoring microstructures and mechanical properties in extruded magnesium alloys via rotational strain porthole die extrusion: a case study on Mg-RE hollow profiles J. Mater. Process. Technol. 2025 337 118732

[25]

He L.,Zheng J.,He Q..et al. Achieving superior strength and ductility synergy of WE54 alloy via combined dislocation introduction and twinning J. Mater. Sci. Technol. 2025 227 174 91

[26]

Lv N.,Zhao L.,Yan H.,Liu B.,Chen R.,Shan Z.. Unusual twin induced recrystallization and corresponding texture optimization in a cold rolled Mg-Gd-Zr alloy during annealing J. Magnes. Alloys 2025 13 1099 115

[27]

Yang B.,Wang J.,Li Y.,Barnett M.,Llorca J.. Deformation mechanisms of dual-textured Mg-6.5Zn alloy with limited tension-compression yield asymmetry Acta Mater. 2023 248 118766

[28]

Song B.,Wang M.,Shi R..et al. Promoting hybrid twins structure to reduce yield asymmetry of rolled AZ31 plates by combining side-rolling and torsion J. Magnes. Alloys 2023 11 2096 105

[29]

Guo X.,Yang S.,Bai G..et al. Study on anisotropic mechanical behavior of AZ31 magnesium alloys under free-end torsion J. Mater. Res. Technol. 2024 30 5724 32

[30]

Guo X.,Wu W.,Wu P.,Qiao H.,An K.,Liaw P.. On the Swift effect and twinning in a rolled magnesium alloy under free-end torsion Scr. Mater. 2013 69 319 22

[31]

Zhang X.,Zhou K.,Wang H..et al. On the cyclic torsion behavior of extruded AZ61A magnesium alloy tube Int. J. Fatigue 2023 174 107704

[32]

Carneiro L.,Yu Q.,Jiang Y.. An experimental study of the mechanical behavior of rolled AZ31B magnesium alloy under combined axial-torsion loading Int. J. Plast. 2022 155 103319

[33]

Jiao M.,Yang X.,Zhao H..et al. Abnormal recoverable plastic strain evolution of extruded AZ31 alloy under multiple-degree-of-freedom tension after reciprocating torsion J. Mater. Sci. Technol. 2025 237 171 87

[34]

Yang Q.,Lv S.,Chen P.,Xie Z.,Zhou S.,Qiu X.. Formation and solute segregation for an asymmetric tilt boundary on {10$ \bar{1} $2} twin boundaries J. Magnes. Alloys 2025 13 583 91

[35]

Guo X.,Cheng Y.,Xin Y..et al. Crystal plasticity modeling of low-cycle fatigue behavior of an Mg-3Al-1Zn alloy based on a model, including twinning and detwinning mechanisms J. Mech. Phys. Solids 2022 168 105030

[36]

Ji C.,Li K.,Liao R..et al. Tensile creep mechanisms of laser powder bed fused WE43 alloy with heterogeneous microstructure: Evolution in dislocations and precipitates J. Mater. Sci. Technol. 2025 238 209 29

[37]

Carneiro L.,Culbertson D.,Yu Q.,Jiang Y.. Twinning in rolled AZ31B magnesium alloy under free-end torsion Mater. Sci. Eng. A 2021 801 140405

[38]

Zhao L.,Chen W.,Zhou B..et al. Quantitative study on the tension-compression yield asymmetry of a Mg-3Al-1Zn alloy with bimodal texture components J. Magnes. Alloys 2022 10 1680 93

[39]

Xia D.,Chen X.,Huang G..et al. Calculation of Schmid factor in Mg alloys: influence of stress state Scr. Mater. 2019 171 31 5

[40]

Wang H.,Wu P.,Tomé C.,Wang J.. Study of lattice strains in magnesium alloy AZ31 based on a large strain elastic-viscoplastic self-consistent polycrystal model Int. J. Solids Struct. 2012 49 2155 67

[41]

Yang H.,Xie W.,Song J..et al. Current progress of research on heat-resistant Mg alloys: a review Int. J. Miner. Metall. Mater. 2024 31 1406 25

[42]

Shi R.,Song B.,Xia D..et al. Influence of initial {10-12} twins on twinning behavior of extruded AZ31 alloys during free-end torsion Mater. Charact. 2023 201 112932

[43]

Jonas J.,Shrivastava S.,Tóth L.. The inverse swift effect: experiments and theory Acta Mater. 1998 46 51 60

[44]

Chen W.,He W.,Jiang B.,Pan F.. Revealing the effect of misorientation on the deformation behavior of a Mg-Y alloy from the perspective of local strain Int. J. Plast. 2023 170 103753

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