Preparation of La0.9K0.1 CoO3 perovskite composite oxide
Wang Wei , Du Chuanjin , Xu Xiang , Qiu Xiaojin
Journal of Wuhan University of Technology Materials Science Edition ›› 2005, Vol. 20 ›› Issue (4) : 32 -34.
Preparation of La0.9K0.1 CoO3 perovskite composite oxide
Two methods for preparing la2.9K0: CoO3 perovskite composite oxides, traditional solid state reaction method and sol-gel method, were compared. The characteristics of the powders, such as purity, particle diameter, BET surface area, pore diameter, were investigated by using TG-DTA, XRD, SEM and BET methods. The experimental results show that La0.9K0.1 CoO3 perovskite composite oxide can be obtained by using the two methods. The purity of La0.9K0: CoO3 powders can be increased by raising the calcining temperature while the particle diameter increased and BET surface area decreased. At the same calcining temperature, the properties of the La0.9K0: CoO3 powders synthesized by the sol-gel method are superior to those synthesized by the solid state reaction method, such as purer phase, smaller particle diameter, which can be used as a satisfactory catalyst in diesel waste gas cleaning.
La0.9K0: CoO3 / perovskite composite oxides / Sol-gel method / diesel waste gas cleaning
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