Variables Affecting the pH Measurement of Cement Mortars

Shafigh Payam , Yousuf Sumra , Ibrahim Zainah

Journal of Wuhan University of Technology Materials Science Edition ›› 2022, Vol. 36 ›› Issue (5) : 689 -696.

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Journal of Wuhan University of Technology Materials Science Edition ›› 2022, Vol. 36 ›› Issue (5) : 689 -696. DOI: 10.1007/s11595-021-2461-3
Cementitious Materials

Variables Affecting the pH Measurement of Cement Mortars

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Abstract

A quantitative pH measuring method has been used to measure the pH of pure and blended cement mortars. The blended cement mortars incorporating supplementary cementitious materials (SCMs) such as fly ash (FA), ground granulated ballast furnace slag (GGBFS) and palm oil fuel ash (POFA) were used. Moreover, different variables affecting the pH values of CBMs such as temperature of sample solution, quantity of sample powder, dilution ratio and temporary storage of sample during pH measuring process have been studied for all cement mortars.

Keywords

mortar / cementitious materials / pH value / dilution ratio / temperature

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Shafigh Payam, Yousuf Sumra, Ibrahim Zainah. Variables Affecting the pH Measurement of Cement Mortars. Journal of Wuhan University of Technology Materials Science Edition, 2022, 36(5): 689-696 DOI:10.1007/s11595-021-2461-3

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References

[1]

Matalkah F, Salem T, Soroushian P. Acid Resistance and Corrosion Protection Potential of Concrete Prepared with Alkali Aluminosilicate Cement[J]. Journal of Building Engineering, 2018, 20: 705-711.

[2]

Enevoldsen J N, Hansson C M, Hope B B. The Influence of Internal Relative Humidity on the Rate of Corrosion of Steel Embedded in Concrete and Mortar[J]. Cement and Concrete Research, 1994, 24(7): 1373-1382.

[3]

Vollpracht A, Lothenbach B, Snellings R, et al. The Pore Solution of Blended Cements: A Review[J]. Materials and Structures, 2016, 49(8): 3341-3367.

[4]

Zhang P, Ou L, Liu K, et al. Physical Properties and Hydration of Cementitious Materials Prepared from Vanadium Slag and Phosphate Slag[J]. Journal of Wuhan University of Technology-Mater. Sci. Ed., 2018, 33(6): 1459-1464.

[5]

Plusquellec G, Geiker M R, Lindgárd J, et al. Determination of the pH and the Free Alkali Metal Content in the Pore Solution of Concrete: Review and Experimental Comparison[J]. Cement and Concrete Research, 2017, 96: 13-26.

[6]

Angst U, Elsener B, Larsen C K, et al. Critical Chloride Content in Reinforced Concrete — A Review[J]. Cement and Concrete Research, 2009, 39(12): 1122-1138.

[7]

Grubb J A, Limaye H S, Kakade A M. Testing pH of Concrete[J]. Concrete International, 2007, 29(04): 78-83.

[8]

Ahmad S. Reinforcement Corrosion in Concrete Structures, Its Monitoring and Service Life Prediction—A Review[J]. Cement and Concrete Composites, 2003, 25(4): 459-471.

[9]

Katpady D N, Hazehara H, Soeda M, et al. Durability Assessment of Blended Concrete by Air Permeability[J]. International Journal of Concrete Structures and Materials, 2018, 12(1): 30

[10]

Cao H T, Bucea L, Ray A, et al. The Effect of Cement Composition and pH of Environment on Sulfate Resistance of Portland Cements and Blended Cements[J]. Cement and Concrete Composites, 1997, 19(2): 161-171.

[11]

Wang Y, Xu C, Li H. Property and Degradation Characteristics of Concrete Prepared with Aggregate Contained Montmorillonite[J]. Journal of Wuhan University of Technology-Mater. Sci. Ed., 2019, 34(1): 127-131.

[12]

Thomas M. The Effect of Supplementary Cementing Materials on Alkali-Silica Reaction: A Review[J]. Cement and Concrete Research, 2011, 41(12): 1224-1231.

[13]

Lu G, Deng M, Mo L. Adsorption and Desorption Characteristics of Alkali Ions in Hydrated C3S-nano SiO2 Pastes[J]. Journal of Wuhan University of Technology-Mater. Sci. Ed., 2018, 33(5): 1176-1185.

[14]

Ge X, Fang K, Zeng L, et al. Properties of Leakage Corrosion of Concrete and Its Durability[J]. Journal of Wuhan University of Technology-Mater. Sci. Ed., 2008, 23(6): 946-949.

[15]

Deschner F, Winnefeld F, Lothenbach B, et al. Hydration of Portland Cement with High Replacement by Siliceous Fly Ash[J]. Cement and Concrete Research, 2012, 42(10): 1389-1400.

[16]

Lothenbach B, Le Saout G, Gallucci E, et al. Influence of Limestone on the Hydration of Portland Cements[J]. Cement and Concrete Research, 2008, 38(6): 848-860.

[17]

Rajabipour F, Sant G, Weiss J. Interactions Between Shrinkage Reducing Admixtures (SRA) and Cement Paste’s Pore Solution[J]. Cement and Concrete Research, 2008, 38(5): 606-615.

[18]

Larbi J A, Bijen J M J M. Interaction of Polymers with Portland Cement During Hydration: A Study of the Chemistry of the Pore Solution of Polymer-Modified Cement Systems[J]. Cement and Concrete Research, 1990, 20(1): 139-147.

[19]

Leemann A, Lothenbach B, Thalmann C. Influence of Superplasticizers on Pore Solution Composition and on Expansion of Concrete due to Alkali-Silica Reaction[J]. Construction and Building Materials, 2011, 25(1): 344-350.

[20]

Wan X-m, Wittmann F H, Zhao T-j, et al. Chloride Content and pH Value in the Pore Solution of Concrete under Carbonation[J]. Journal of Zhejiang University Science A, 2013, 14(1): 71-78.

[21]

Duchesne J, Bérubé M A. Evaluation of the Validity of the Pore Solution Expression Method from Hardened Cement Pastes and Mortars[J]. Cement and Concrete Research, 1994, 24(3): 456-462.

[22]

Cyr M, Rivard P, Labrecque F, et al. High-Pressure Device for Fluid Extraction from Porous Materials: Application to Cement-based Materials[J]. Journal of the American Ceramic Society, 2008, 91(8): 2653-2658.

[23]

Sagüés A A, Moreno E I, Andrade C. Evolution of pH during In-Situ Leaching in Small Concrete Cavities[J]. Cement and Concrete Research, 1997, 27(11): 1747-1759.

[24]

Li L, Sagüés A A, Poor N. In situ Leaching Investigation of pH and Nitrite Concentration in Concrete Pore Solution[J]. Cement and Concrete Research, 1999, 29(3): 315-321.

[25]

Li L, Nam J, Hartt W H. Ex Situ Leaching Measurement of Concrete Alkalinity[J]. Cement and Concrete Research, 2005, 35(2): 277-283.

[26]

Pu Q, Jiang L, Xu J, et al. Evolution of pH and Chemical Composition of Pore Solution in Carbonated Concrete[J]. Construction and Building Materials, 2012, 28(1): 519-524.

[27]

Räsänen V, Penttala V. The pH Measurement of Concrete and Smoothing Mortar Using a Concrete Powder Suspension[J]. Cement and Concrete Research, 2004, 34(5): 813-820.

[28]

Nguyen T H, Venugopala T, Chen S, et al. Fluorescence Based Fibre Optic pH Sensor for the pH 10–13 Range Suitable for Corrosion Monitoring in Concrete Structures[J]. Sensors and Actuators B: Chemical, 2014, 191: 498-507.

[29]

Ghandehari M, Vimer C S. In Situ Monitoring of pH Level with Fiber Optic Evanescent Field Spectroscopy[J]. NDT & E International, 2004, 37(8): 611-616.

[30]

Habel W R, Krebber K. Fiber-Optic Sensor Applications in Civil and Geotechnical Engineering[J]. Photonic Sensors, 2011, 1(3): 268-280.

[31]

Safiuddin M, Abdus Salam M, Jumaat M Z. Utilization of Palm Oil Fuel Ash in Concrete: A Review[J]. Journal of Civil Engineering and Management, 2011, 17(2): 234-247.

[32]

Awal A S M A, Hussin M W. The Effectiveness of Palm Oil Fuel Ash in Preventing Expansion due to Alkali-Silica Reaction[J]. Cement and Concrete Composites, 1997, 19(4): 367-372.

[33]

ASTM International. Standard Test Method for Compressive Strength of Hydraulic Cement Mortars (using 2-in. Or [50-mm] Cube Specimens)[S]. C109/C109M-16a, USA, 2013

[34]

Aprianti E, Shafigh P, Zawawi R, et al. Introducing an Effective Curing Method for Mortar Containing High Volume Cementitious Materials[J]. Construction and Building Materials, 2016, 107: 365-377.

[35]

Toutanji H, Delatte N, Aggoun S, et al. Effect of Supplementary Cementitious Materials on the Compressive Strength and Durability of Short-term Cured Concrete[J]. Cement and Concrete Research, 2004, 34(2): 311-319.

[36]

Feldman R F, Carette G G, Malhotra V M. Studies on Mechanics of Development of Physical and Mechanical Properties of High-Volume Fly Ash-Cement Pastes[J]. Cement and Concrete Composites, 1990, 12(4): 245-251.

[37]

Berry E E, Hemmings R T, Cornelius B J. Mechanisms of Hydration Reactions in High Volume Fly Ash Pastes and Mortars[J]. Cement and Concrete Composites, 1990, 12(4): 253-261.

[38]

Pacheco Torgal F, Miraldo S, Labrincha J A, et al. An Overview on Concrete Carbonation in the Context of Eco-efficient Construction: Evaluation, Use of SCMs and/or RAC[J]. Construction and Building Materials, 2012, 36: 141-150.

[39]

Elahi A, Basheer P A M, Nanukuttan S V, et al. Mechanical and Durability Properties of High Performance Concretes Containing Supplementary Cementitious Materials[J]. Construction and Building Materials, 2010, 24(3): 292-299.

[40]

Fraay A L A, Bijen J M, de Haan Y M. The Reaction of Fly Ash in Concrete a Critical Examination[J]. Cement and Concrete Research, 1989, 19(2): 235-246.

[41]

Rashad A M. An Investigation on Very High Volume Slag Pastes Subjected to Elevated Temperatures[J]. Construction and Building Materials, 2015, 74: 249-258.

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