Preparation of Functionalized Graphene Nano-platelets and Use for Adsorption of Pb2+ from Solution

Zhibo Sheng , Ming Cao , Yin Hong , Shengniang Wang , Zhihong Fan , Jianbo Xiong , Haicheng Yang , Chunlin Deng

Journal of Wuhan University of Technology Materials Science Edition ›› 2018, Vol. 33 ›› Issue (6) : 1395 -1401.

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Journal of Wuhan University of Technology Materials Science Edition ›› 2018, Vol. 33 ›› Issue (6) : 1395 -1401. DOI: 10.1007/s11595-018-1981-y
Advanced Materials

Preparation of Functionalized Graphene Nano-platelets and Use for Adsorption of Pb2+ from Solution

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Abstract

Functionalized graphene nano-platelets (FGN) were obtained via treating graphene nanoplatelets (GN) with HNO3, and served as adsorbent for the removal of Pb2+ from solutions. We investigated the FGN adsorption capacity for Pb2+ at different initial concentrations, varying pH, contact time and temperature. The characterization results of scanning electron microscopy (SEM), thermal analysis (TG/DTG), Fourier transform infrared spectroscopy (FT-IR) and Brunauer-Emmett-Teller (BET) method indicated that FGN layers were thin and possess large specific area with oxygen-containing functional groups grafted onto their surface. Meanwhile, the determined equilibrium adsorption capacity of FGN for Pb2+ was 57.765 mg/g and adsorption isotherms well confirmed to Langmuir isotherms models. The results reveals that the FGN has better effect of water treatment.

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functionalized graphene nano-platelets / water treatment / adsorption

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Zhibo Sheng, Ming Cao, Yin Hong, Shengniang Wang, Zhihong Fan, Jianbo Xiong, Haicheng Yang, Chunlin Deng. Preparation of Functionalized Graphene Nano-platelets and Use for Adsorption of Pb2+ from Solution. Journal of Wuhan University of Technology Materials Science Edition, 2018, 33(6): 1395-1401 DOI:10.1007/s11595-018-1981-y

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