Alumina Ceramics Fabricated by in-situ Consolidation of Pre-gelling Starch

Abstract

An in-situ consolidation method was developed and optimized to successfully fabricate alumina ceramics using pre-gelling starch. Our results showed that the obtained ceramics have more homogeneous microstructure, higher density, higher flexural strength, and favorable biocompatibility compared to the regular one. During the process, cornstarch granules swelled and deformed but no fracture was observed. After the cornstarch granules bursted, alumina particles were suspended uniformly in the three-dimensional network structure to generate a much smoother surface. Below 0.5 wt% higher cornstarch content increased the flexural strength of prepared ceramics, while above 0.5 wt% the mechanical properties were compromised. Therefore the cornstarch content of 0.5% was the optimal concentration to achieve the highest mechanical strength of the prepared ceramics, with a measured flexural strength of 341 MPa, and a relative density of 96.01%.

Keywords

pre-gelling / starch in-situ consolidation / alumina-ceramic / flexural strength / biocompatibility

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