Analysis of χ phase precipitation in aged 2205 duplex stainless steel

Heping Liu , Hu’er Sun , Bin Liu , Dazhao Li , Fenger Sun , Yongtao Zhang

Journal of Wuhan University of Technology Materials Science Edition ›› 2015, Vol. 30 ›› Issue (3) : 591 -595.

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Journal of Wuhan University of Technology Materials Science Edition ›› 2015, Vol. 30 ›› Issue (3) : 591 -595. DOI: 10.1007/s11595-015-1194-6
Metallic Materials

Analysis of χ phase precipitation in aged 2205 duplex stainless steel

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Abstract

Analysis of χ phase precipitation in 2205 duplex stainless steel aged at 700 and 750 °C has been investigated systematically. The experimental results showed that χ phase forms prior to the precipitation of σ phase and disappears once σ phase starts to precipitate. This phenomenon indicates that σ phase nucleated and consumed the χ phase. The σ phase nucleated mainly at ferrite/austenite interface and grew inwards into the ferrite phase. The morphology of σ phase reveals a coral-like structure at the temperature of 700 °C for 120 min followed by quenching in water. The decomposition of ferrite occurs via the following eutectoid reaction: Fσ+γ 2. The selected area diffraction pattern of zone axes is$[\bar 31\bar 3]_\chi ||[\bar 31\bar 3]_\delta $, indicating a characteristic orientation relationship between χ phase and δ-ferrite.

Keywords

duplex stainless steel / χ phase / σ phase / microstructure analysis

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Heping Liu, Hu’er Sun, Bin Liu, Dazhao Li, Fenger Sun, Yongtao Zhang. Analysis of χ phase precipitation in aged 2205 duplex stainless steel. Journal of Wuhan University of Technology Materials Science Edition, 2015, 30(3): 591-595 DOI:10.1007/s11595-015-1194-6

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References

[1]

Nilsson J O, Wilson A. Influence of Isothermal Phase Transformations on Toughness and Pitting Corrosion of Super Duplex Stainless Steel SAF 2507 [J]. Mater. Sci. Technol., 1993, 9: 545-554.

[2]

Huang C S, Shih C C. Effects of Nitrogen and High Temperature Aging on σ Phase Precipitation of Duplex Stainless Steel[J]. Mater. Sci. Eng. A, 2005, 402: 66-75.

[3]

Wang Y Q, Han J, Wu H C, et al. Effect of Sigma Phase Precipitation on the Mechanical and Wear Properties of Z3CN20.09M Cast Duplex Stainless Steel [J]. Nuclear Eng. Design, 2013, 259: 1-7.

[4]

Nilsson J O, Huhtala T, Karlsson L, et al. Structural Stability of Super Duplex Stainless Weld Metals and Its Dependence on Tungsten and Copper [J]. Metall. Mater. Trans. A, 1996, 27: 2 196-2 208.

[5]

Nilsson J O, Kangas P, Karlsson T, et al. Mechanical Properties, Microstructural Stability and Kinetics of σ-phase Formatiion in 29Cr-6Ni-2Mo-0.38N Super Duplex Stainless Steel [J]. Metall. Mater. Trans. A, 2000, 31: 35-45.

[6]

Yang Y Z, Wang Z Y, Tan H, et al. Effect of a Brief Post-weld Heat Treatment on the Microstructure Evolution and Pitting Corrosion of Laser Beam Welded UNS S31803 Duplex Stainless Steel [J]. Corrosion Sci., 2012, 65: 472-80.

[7]

Nilsson J O. The Physical Metallurgy of Duplex Stainless Steels[C]. Proc. 5th World Conf. on Duplex Stainless Steels, Maastricht, 1997 73-83.

[8]

Martins M, Carlos C L. Microstructural Characteristics and Corrosion Behavior of a Super Duplex Stainless Steel Casting [J]. Mater. Charact., 2009, 60: 150-155.

[9]

Michalska J, Sozańska M. Qualitative and Quantitative Analysis of σ and χ Phases in 2205 Duplex Stainless Steel [J]. Mater. Charact., 2006, 56: 355-362.

[10]

Escriba D M, Materna-Morris E, Plaut R L, et al. Chi-phase Precipitation in a Duplex Stainless Steel [J]. Mater. Charact., 2009, 60: 1 214-1 219.

[11]

Kashiwar A, Phani Vennela N, Kamath S L, et al. Effect of Solution Annealing Temperature on Precipitation in 2205 Duplex Stainless Steel [J]. Mater. Charact., 2012, 74: 55-63.

[12]

Cho H S, Lee K. Effect of Cold Working and Isothermal Aging on the Precipitation of Sigma Phase in 2205 Duplex Stainless Steel [J]. Mater. Charact., 2013, 75: 29-34.

[13]

Tavares S S M, Pardal J M G J L, et al. Magnetic Detection of Sigma Phase in Duplex Stainless Steel UNS S31803 [J]. J. Magn. Magn. Mater., 2010, 322: L29-L33.

[14]

Jeon S H, Kim S T, Lee I S, et al. Effects of Cu on the Precipitation of Intermetallic Compounds and the Intergranular Corrosion of Hyper Duplex Stainless Steels [J]. Corrosion Sci., 2013, 66: 217-24.

[15]

Andersson J O, Halender T, Höglund L, et al. Thermo-Calc & DICTRA, Computational Tools for Materials Science [J]. Calphad, 2002, 26: 273-312.

[16]

Ferro P, Bonollo F. A Semiempirical Model for Sigma-phase Precipitation in Duplex and Super Duplex Stainless Steels [J]. Metall. Mater. Trans. A, 2012, 43: 1 109-1 116.

[17]

He Y L, Zhu N Q, Lu X G, et al. Experimental and Computational Study on Microstructural Evolution in 2205 Duplex Stainless Steel During High Temperature Aging [J]. Mater. Sci. Eng. A, 2010, 528: 721-29.

[18]

Chen T H, Weng K L, Yang J R. The Effect of High-temperature Exposure on the Microstructural Stability and Toughness Property in a 2205 Duplex Stainless Steel [J]. Mater. Sci. Eng. A, 2002, 338: 259-267.

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