Synthesis of SWNTs from charcoal by arc-discharging

Weiwei Fan , Juan Zhao , Yongkang Lv , Weiren Bao , Xuguang Liu

Journal of Wuhan University of Technology Materials Science Edition ›› 2010, Vol. 25 ›› Issue (2) : 194 -196.

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Journal of Wuhan University of Technology Materials Science Edition ›› 2010, Vol. 25 ›› Issue (2) : 194 -196. DOI: 10.1007/s11595-010-2194-1
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Synthesis of SWNTs from charcoal by arc-discharging

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Abstract

With charcoal as carbon source and FeS (20wt%) as catalyst, single-wall carbon nanotubes (SWNTs) were successfully produced by dc arc-discharge method. The analysis by scanning electron microscopy, high-resolution transmission electron microscopy and Raman spectroscopy clearly demonstrated that the SWNTs developed from charcoal achieved a high purity with diameter about 1.2 nm, and FTIR measurement showed the inner structural transformation of carbon source, in which functional groups and grapheme sheets were decomposed and then ordered into nanotubes. By this easy-get and relatively low cost material, the experimenal results clearly indicate that charcoal has the opportunity of reducing the cost of SWNTs production.

Keywords

charcoal / single-wall carbon nanotubes / catalyst

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Weiwei Fan, Juan Zhao, Yongkang Lv, Weiren Bao, Xuguang Liu. Synthesis of SWNTs from charcoal by arc-discharging. Journal of Wuhan University of Technology Materials Science Edition, 2010, 25(2): 194-196 DOI:10.1007/s11595-010-2194-1

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References

[1]

Iijima S. Helical Microtubues of Graphitic Carbon[J]. Nature, 1991, 354: 56-58.

[2]

Zhu H. W., Wu D. H., Xu C. L. Carbonnanotube[M], 2003 Beijing China Machine Press

[3]

Ebbesen T. W., Ajayan P. M. Large-scale Synthesis of Carbon Nanotubes[J]. Nature, 1992, 358(6383): 220

[4]

Liu C., Cheng H. M., Cong H. T., . Synthesis of Macroscopically Long Ropes of Well-aligned Single-walled Carbon Nanotues[J]. Adv. Mater., 2000, 12(16): 1190-1192.

[5]

Zhao T. K., Liu Y. N. Large Scale Synthesis of Single-walled Carbon Nanotubes by an Arc-discharge Method at Controlled Temperatures[J]. Acta Phys. Sin., 2004, 53: 3961-3965.

[6]

Liu C., Cong H. T., Li F., . Semi-continuous Synthesis of single-walled Carbon Nanotubes by a Hydrogen Arc Discharge Method[J]. Carbon, 1999, 37(11): 1865-1868.

[7]

Pang L. S., Willson M. A., Vassallo M. Fullerene from Coal[J]. Nature, 1991, 352: 480

[8]

Wilson M. A., Patney H. K., Kalman J. New Development in the Formation of Nanotubes from Coal[J]. Fuel, 2002, 81(1): 5-14.

[9]

Qiu J. S., Li Y. F., Wang Y. P., . High-purity Single-wall Carbon Nanotubes Synthesized from Coal by Arc Discharge[J]. Carbon, 2003, 41: 2170-2173.

[10]

Veziri C. M., Pilatos G., Karanikolos G. N., . Growth and Optimization of Carbon Nanotubes in Activated Carbonby Catalytic Chemical Vapor Deposition[J]. Micropor. Mesopor. Mat., 2008, 110: 41-50.

[11]

Singjai P., Wongjamras A., Yu L. D., . Production and Characterization of Beaded Nanofibers from Current Heating of Charcoal[J]. Chem. Phys. Lett., 2002, 366(1): 51-55.

[12]

Wei J. Q., Zhu H. W., Yi J., . The Effect of Sulfur on the Number of Layers in a Carbon Nanotube[J]. Carbon, 2007, 45: 2152-2158.

[13]

Ando Y., Zhao X. L., Hirahara K., . Mass Production of Single-wall Carbon Nanotubes by the Arc Plasma Jet Method[J]. Chem. Phys. Lett., 2000, 323: 580-585.

[14]

Rao A. M., Chen J., Richter E., . Effect of van der waals Interactions on the Raman Modes in Single Walled Carbon Nanotubes[J]. Phys. Rev. Lett., 2001, 86: 3895-3898.

[15]

Li F., Cheng H. M., Wei Y. L., . Effect of Sulfur-containing Promoter on the Synthesis of Single-walled Barbon Nanotubes[ J]. Chinese J. Mater. Res., 1999, 13(4): 401-404.

[16]

Li W. Z., Xie S., Liu W. A Structure Model and Growth Mechanism for Novel Carbon Nanotubes[J]. J. Mater. Sci., 1999, 34: 2745-2749.

[17]

Bourrat X., Oberlin A., Escalier J. C. Sulphur Behaviour During asphalt Heat-treatment[J]. Fuel, 1987, 64: 542-550.

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