Synthesis of single hexagonal-phase AlN nanocrystallines by a liquid-solid metathetical reaction in an organic solution

Guojun Yan , Guangde Chen , Huiming Lu , Lei Guo

Journal of Wuhan University of Technology Materials Science Edition ›› 2008, Vol. 23 ›› Issue (3) : 334 -337.

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Journal of Wuhan University of Technology Materials Science Edition ›› 2008, Vol. 23 ›› Issue (3) : 334 -337. DOI: 10.1007/s11595-007-3334-0
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Synthesis of single hexagonal-phase AlN nanocrystallines by a liquid-solid metathetical reaction in an organic solution

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Abstract

A liquid-solid metathetical reaction method (LSMRM) of synthesizing AlN nanocrystallines is presented. AlN nanocrystallines made through LSMRM are characterized by X-ray diffractions (XRD), X-ray photoelectron spectroscopy (XPS), transmission electron microscopy (TEM), Fourier transformation infrared (FT-IR) spectroscopy, and Raman spectroscopy. The results show that the samples are single hexagonal-phase AlN and the size of the AlN samples is about tens of nanometer.

Keywords

AlN nanocrystalline / synthesis / organic solvent thermal method

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Guojun Yan, Guangde Chen, Huiming Lu, Lei Guo. Synthesis of single hexagonal-phase AlN nanocrystallines by a liquid-solid metathetical reaction in an organic solution. Journal of Wuhan University of Technology Materials Science Edition, 2008, 23(3): 334-337 DOI:10.1007/s11595-007-3334-0

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