Synthesis of rod-like ternary carbide LaNiC2 by a solvothermal route
Yuanzhu Mi , Yingliang Liu , Jingxian Zhang , Dingsheng Yuan
Journal of Wuhan University of Technology Materials Science Edition ›› 2007, Vol. 22 ›› Issue (2) : 253 -255.
Synthesis of rod-like ternary carbide LaNiC2 by a solvothermal route
LaNiC2 was synthesized by a solvothermal route in a stainless steel autoclave at 600 °C. In this process, nickel chloride, lanthanum chloride and toluene were used as raw materials, and metallic Na and Li alloy were used as reductant. The products were characterized with an X-ray diffractometer (XRD) and a scanning electron microscope (SEM). The LaNiC2 products consisted of a great deal of micro-rods. The micro-rods had diameters ranging from hundreds of nanometers to several micrometers and lengths ranging from several micrometers to tens of micrometers.
micro-rod / LaNiC2 / solvothermal route
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