Analyses of dynamic rheological behavior of polymer melt based on novel experimental equipment and procedures
Liu Yuejun , Qu Jinping , Cao Xianwu , Shi Pu
Journal of Wuhan University of Technology Materials Science Edition ›› 2005, Vol. 20 ›› Issue (2) : 45 -48.
Analyses of dynamic rheological behavior of polymer melt based on novel experimental equipment and procedures
By introducing a vibrating, force field into the extrusion process of polymer melt, an experimental equipment of constant velocity type dynamic rheometer of capillary (CVDRC) was designed. A set of experimental procedures was established, by which the dynamic rheological parameters of polymer can be acquired, and a set of data management methods to undergo time-domain or frequency-domain analysis was set up for dynamic rheological data of polymer melt. Meantime, the characterization formula of polymer melt’s rheological behavior in a vibrating force field was set up. The instantaneous value of capillary entry pressure, capillary volume flow rate and their phase difference were measured and analyzed, and the melt apparent viscosity, which describes the rheological behavior of polymer melt in a vibrating force field, was obtained.
polymer melt / vibrating force field / rheological behavior / measurement / characterization formula
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