Synthesis and characterization of mesoporous silicon oxynitride MCM-41 with high nitrogen content

Zhang Cunman; Xu Zheng; Liu Qian

doi:10.1007/BF02838482

Journal of Wuhan University of Technology Materials Science Edition ›› 2005, Vol. 20 ›› Issue (2) : 32 -34. DOI: 10.1007/BF02838482

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Synthesis and characterization of mesoporous silicon oxynitride MCM-41 with high nitrogen content

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Abstract

Mesoporous silicon oxynitrides MCM-41 were synthesized successfully. The resulting materials not only have high nitrogen contents and good structural characteristics of MCM-41 (high surface area, narrow pore size distribution and good order), but also are amorphous. The composition and structure of the materials were investigated by CNH element analysis, XPS, Si MAS NMR, XRD, HRTEM and N₂ sorption, respectively. Mesoporous silicon oxynitrides MCM-41 with a high nitrogen content are still non-crystal (amorphous).

Keywords

mesoporous / silicon oxynitride / MCM-41 / high nitrogen content

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Zhang Cunman, Xu Zheng, Liu Qian. Synthesis and characterization of mesoporous silicon oxynitride MCM-41 with high nitrogen content. Journal of Wuhan University of Technology Materials Science Edition, 2005, 20(2): 32-34 DOI:10.1007/BF02838482

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