Self-assembling synthesis of vanadium oxide nanotubes and simple determination of the content of V(IV)

Mai Li-qiang , Chen Wen , Xu Qing , Zhu Quan-yao , Han Chun-hua , Peng Jun-feng

Journal of Wuhan University of Technology Materials Science Edition ›› 2003, Vol. 18 ›› Issue (4) : 21 -23.

PDF
Journal of Wuhan University of Technology Materials Science Edition ›› 2003, Vol. 18 ›› Issue (4) : 21 -23. DOI: 10.1007/BF02838382
Article

Self-assembling synthesis of vanadium oxide nanotubes and simple determination of the content of V(IV)

Author information +
History +
PDF

Abstract

High-yielding low-cost vanadium oxide nanotubes were prepared by the hydrothermal self-assembling process from vanadium pentoxide and organic molecules as structure-directing templates. Moreover, a new method was discovered for determining the content of V (IV) in vanadium oxide nanotubes by thermogravimetric analysis (TGA). This method is simple, precise and feasible and can be extended to determine the content of low oxidation state in the other transition metal oxide nanomaterials.

Keywords

vanadium oxides nanotube / self-assembling synthesis / thermogravimetric analysis / vanadium (IV)

Cite this article

Download citation ▾
Mai Li-qiang, Chen Wen, Xu Qing, Zhu Quan-yao, Han Chun-hua, Peng Jun-feng. Self-assembling synthesis of vanadium oxide nanotubes and simple determination of the content of V(IV). Journal of Wuhan University of Technology Materials Science Edition, 2003, 18(4): 21-23 DOI:10.1007/BF02838382

登录浏览全文

4963

注册一个新账户 忘记密码

References

[1]

Dekker C. Carbon Nanotubes as Molecular Wires. Phys. Today, 1999, 52: 22-28.

[2]

Shan S G, Gao D S, Chen W. The Layered-nanocomposite Film of Polymer Intercalation in V2O5 Xerogel. J. Wuhan University of Technology—Mater. Sci. Ed., 2000, 15: 1-5.

[3]

Chen W, Xu Q, Hu Y S, Mai L Q, Zhu Q Y. Effect of Modification by Poly (ethylene-oxide) on Reversibility of Insertion/Extraction of Li+ Ion in V2O5 Xerogel Films. J. Mater Chem, 2002, 12: 1926-1929.

[4]

Mai L Q, Chen W, Xu Q, Zheng J X, Ke M Z. Preparation and Applications of V2O5 Xerogel Thin Films. Mater. Rev., 2002, 16: 39-41.

[5]

Krumeich F, Muhr H J, Niederberger M, Bieri F, Schnyder B, Nesper R. Morphology and Topochemical Reactions of Novel Vanadium Oxide Nanotubes. J. Am. Chem. Soc., 1999, 121: 8324-8328.

[6]

Spahr M E, Bitterli P, Nesper R. Redox-Active Nanotubes of Vanadium Oxide. Angew. Chem. Int. Ed., 1998, 37: 1263-1265.

[7]

Mai L Q, Chen W, Xu Q, Zhu Q Y. Research on Chemical States of Vanadium in PEO-V2O5 Xerogel Nanocomposite Films. Chinese J. Nonferrous Met., 2002, S2: 70-74.

[8]

Doubley A, Ngala K, Yang S, Zavalij P Y, Whittingham M S. Manganese Vanadium Oxide Nanotubes: Synthesis, Characterization, and Electrochemistry. Chem. Mater., 2000, 13: 4382-4386.

AI Summary AI Mindmap
PDF

125

Accesses

0

Citation

Detail

Sections
Recommended

AI思维导图

/