Multi-scale quantitative study on cemented tailings and waste-rock backfill under different loading rates

Sheng-hua Yin , Jun-wei Chen , Ze-peng Yan , Jia-lu Zeng , Yun Zhou , Jian Yang , Fu-shun Zhang

Journal of Central South University ›› 2026, Vol. 33 ›› Issue (1) : 357 -374.

PDF
Journal of Central South University ›› 2026, Vol. 33 ›› Issue (1) :357 -374. DOI: 10.1007/s11771-026-6167-8
Research Article
research-article
Multi-scale quantitative study on cemented tailings and waste-rock backfill under different loading rates
Author information +
History +
PDF

Abstract

The development of metallic mineral resources generates a significant amount of solid waste, such as tailings and waste rock. Cemented tailings and waste-rock backfill (CTWB) is an effective method for managing and disposing of this mining waste. This study employs a macro-meso-micro testing method to investigate the effects of the waste rock grading index (WGI) and loading rate (LR) on the uniaxial compressive strength (UCS), pore structure, and micromorphology of CTWB materials. Pore structures were analyzed using scanning electron microscopy (SEM) and mercury intrusion porosimetry (MIP). The particles (pores) and cracks analysis system (PCAS) software was used to quantitatively characterize the multi-scale micropores in the SEM images. The key findings indicate that the macroscopic results (UCS) of CTWB materials correspond to the microscopic results (pore structure and micromorphology). Changes in porosity largely depend on the conditions of waste rock grading index and loading rate. The inclusion of waste rock initially increases and then decreases the UCS, while porosity first decreases and then increases, with a critical waste rock grading index of 0.6. As the loading rate increases, UCS initially rises and then falls, while porosity gradually increases. Based on MIP and SEM results, at waste rock grading index 0.6, the most probable pore diameters, total pore area (TPA), pore number (PN), maximum pore area (MPA), and area probability distribution index (APDI) are minimized, while average pore form factor (APF) and fractal dimension of pore porosity distribution (FDPD) are maximized, indicating the most compact pore structure. At a loading rate of 12.0 mm/min, the most probable pore diameters, TPA, PN, MPA, APF, and APDI reach their maximum values, while FDPD reaches its minimum value. Finally, the mechanism of CTWB materials during compression is analyzed, based on the quantitative results of UCS and porosity. The research findings play a crucial role in ensuring the successful application of CTWB materials in deep metal mines.

Keywords

cemented backfill / waste rock / loading rate / multi-scale analysis / mercury intrusion porosimetry / pore structure / micromorphology

Cite this article

Download citation ▾
Sheng-hua Yin, Jun-wei Chen, Ze-peng Yan, Jia-lu Zeng, Yun Zhou, Jian Yang, Fu-shun Zhang. Multi-scale quantitative study on cemented tailings and waste-rock backfill under different loading rates. Journal of Central South University, 2026, 33(1): 357-374 DOI:10.1007/s11771-026-6167-8

登录浏览全文

4963

注册一个新账户 忘记密码

References

[1]

Yin S-h, Shao Y-j, Wu A-xet al. . A systematic review of paste technology in metal mines for cleaner production in China [J]. Journal of Cleaner Production. 2020, 247: 119590.

[2]

Soltani K A, Osanloo M, Esfahanipour A. Optimization of open pit to underground transition depth: An idea for reducing waste rock contamination while maximizing economic benefits [J]. Journal of Cleaner Production. 2020, 277123530.

[3]

Uskov V A, Kondrat’ev S A, Neverov S A. Economic expediency of copper ore mining with waste rock fill of secondary stopes in the west wing of the Oktyabrsky deposit [J]. Journal of Mining Science. 2017, 53(6): 1090-1095.

[4]

Holmberg K, Kivikytö-reponen P, Härkisaari Pet al. . Global energy consumption due to friction and wear in the mining industry [J]. Tribology International. 2017, 115: 116-139.

[5]

Guo Z-b, Qiu J-p, Kirichek Aet al. . Recycling waste tyre polymer for production of fibre reinforced cemented tailings backfill in green mining [J]. Science of the Total Environment. 2024, 908: 168320.

[6]

Owens B. Mining: Extreme prospects [J]. Nature. 2013, 4957440S4-S6.

[7]

Behera S K, Mishra D P, Singh Pet al. . Utilization of mill tailings, fly ash and slag as mine paste backfill material: Review and future perspective [J]. Construction and Building Materials. 2021, 309: 125120.

[8]

Wang L-m, Cheng L, Yin S-het al. . Multiphase slurry flow regimes and its pipeline transportation of underground backfill in metal mine: Mini review [J]. Construction and Building Materials. 2023, 402133014.

[9]

Xu D-m, Zhan C-l, Liu H-xet al. . A critical review on environmental implications, recycling strategies, and ecological remediation for mine tailings [J]. Environmental Science and Pollution Research. 2019, 263535657-35669.

[10]

Hou Y-b, Ding P-c, Han Det al. . Study on the preparation and hydration properties of a new cementitious material for tailings discharge [J]. Processes. 2019, 7147.

[11]

Yin S-h, Yan Z-p, Chen Xet al. . Active roof-contact: The future development of cemented paste backfill [J]. Construction and Building Materials. 2023, 370: 130657.

[12]

Cheng H-y, Wu S-c, Li Het al. . Influence of time and temperature on rheology and flow performance of cemented paste backfill [J]. Construction and Building Materials. 2020, 231117117.

[13]

Yin S-h, Zhou Y, Chen Xet al. . A new acoustic emission characteristic parameter can be utilized to evaluate the failure of cemented paste backfill and rock combination [J]. Construction and Building Materials. 2023, 392132017.

[14]

Deng D-q, Wang Y, Liang Y-het al. . Strength variation characteristics of waste tailings cemented backfill materials with ultrafine particles [J]. Frontiers in Materials. 2023, 101166065.

[15]

Wang X-l, Guo J-p, Wu A-xet al. . Wear characteristics of the pipeline transporting cemented paste backfill containing coarse aggregate [J]. Construction and Building Materials. 2024, 410134170.

[16]

Fatah T A, Zhang R-j, Miao Yet al. . Strength and leaching behavior of tailing-based paste backfill at high water content amended with lime activated ground granulated blast furnace slag and flocculant [J]. Environmental Science and Pollution Research. 2024, 31711115-11127.

[17]

Ouattara D, Belem T, Mbonimpa Met al. . Effect of superplasticizers on the consistency and unconfined compressive strength of cemented paste backfills [J]. Construction and Building Materials. 2018, 181: 59-72.

[18]

Dong H-z, Abdul A N, Zulhaidi Mohd Shafri Het al. . Computational fluid dynamics study on cemented paste backfill slurry: Review [J]. Construction and Building Materials. 2023, 369: 130558.

[19]

Ma Q-h, Liu G-s, Yang X-cet al. . Physical model investigation on effects of drainage condition and cement addition on consolidation behavior of tailings slurry within backfilled stopes [J]. International Journal of Minerals, Metallurgy and Materials. 2023, 3081490-1501.

[20]

Smoliński A, Malashkevych D, Petlovanyi Met al. . Research into impact of leaving waste rocks in the mined-out space on the geomechanical state of the rock mass surrounding the longwall face [J]. Energies. 2022, 15249522.

[21]

He X-y, Li W-l, Yang Jet al. . Multi-solid waste collaborative production of clinker-free cemented iron tailings backfill material with ultra-low binder-tailing ratio [J]. Construction and Building Materials. 2023, 367: 130271.

[22]

Zhang J-q, Yang K, He Xet al. . Study on mechanical properties and damage characteristics of coal-based solid waste cemented backfill [J]. Construction and Building Materials. 2023, 368130373.

[23]

Lv H-y, Chen Y-l, Xie Q-het al. . Performance optimization and characterization of loess-slag-based geopolymer composite: A new sustainable green material for backfill [J]. Construction and Building Materials. 2022, 354129103.

[24]

Wang L-m, Cheng L, Yin S-het al. . Flocculation, dewatering and sedimentation behaviour of mine backfill slurry in deep cone thickener (DCT) [J]. Journal of Environmental Chemical Engineering. 2024, 122112168.

[25]

Zhang B, Li K-q, Cai R-jet al. . Properties of modified superfine tailings cemented paste backfill: Effects of mixing time and Al2O3 dosage [J]. Construction and Building Materials. 2024, 417135365.

[26]

Cao S, Yilmaz E, Song W-det al. . Loading rate effect on uniaxial compressive strength behavior and acoustic emission properties of cemented tailings backfill [J]. Construction and Building Materials. 2019, 213313-324.

[27]

Xiu Z-g, Wang S-h, Ji Y-cet al. . Loading rate effect on the uniaxial compressive strength (UCS) behavior of cemented paste backfill (CPB) [J]. Construction and Building Materials. 2021, 271: 121526.

[28]

Chen J, Jiang D-y, Ren Set al. . Comparison of the characteristics of rock salt exposed to loading and unloading of confining pressures [J]. Acta Geotechnica. 2016, 111221-230.

[29]

Yang P, Pang D-d, Liu Jet al. . Experiment on deformation and failure characteristics of sandstone at different unloading rates [J]. Alexandria Engineering Journal. 2023, 75: 209-219.

[30]

Liu C-y, Zhao G-m, Xu W-set al. . Experimental study on failure characteristics of single-sided unloading rock under different intermediate principal stress conditions [J]. International Journal of Mining Science and Technology. 2023, 333275-287.

[31]

Li M, Zhang J-x, Meng G-het al. . Testing and modelling creep compression of waste rocks for backfill with different lithologies [J]. International Journal of Rock Mechanics and Mining Sciences. 2020, 125: 104170.

[32]

Chen G, Ye Y-c, Yao Net al. . Experimental study on mechanical strength and acoustic emission characteristics of waste rock cemented backfill [J]. Bulletin of Engineering Geology and the Environment. 2024, 83(4): 133.

[33]

Xin L-wei. Meso-scale modeling of the influence of waste rock content on mechanical behavior of cemented tailings backfill [J]. Construction and Building Materials. 2021, 307124473.

[34]

Yan Z-p, Yin S-h, Chen Xet al. . Rheological properties and wall-slip behavior of cemented tailing-waste rock backfill (CTWB) paste [J]. Construction and Building Materials. 2022, 324126723.

[35]

Chen X-d, Wu S-x, Zhou J-kai. Influence of porosity on compressive and tensile strength of cement mortar [J]. Construction and Building Materials. 2013, 40869-874.

[36]

Xu L-l, Duan Y, Li Y-long. Porosity, gradient and impact velocity effects on compressive response of foamed concrete [J]. Construction and Building Materials. 2022, 315: 125616.

[37]

Ashrafian A, Taheri Amiri M J, Rezaie-Balf Met al. . Prediction of compressive strength and ultrasonic pulse velocity of fiber reinforced concrete incorporating nano silica using heuristic regression methods [J]. Construction and Building Materials. 2018, 190479-494.

[38]

Zhang Y, Wu K, Yang Z-xet al. . A reappraisal of the ink-bottle effect and pore structure of cementitious materials using intrusion-extrusion cyclic mercury porosimetry [J]. Cement and Concrete Research. 2022, 161: 106942.

[39]

Zhu Z-d, Huo W-w, Sun Het al. . Correlations between unconfined compressive strength, sorptivity and pore structures for geopolymer based on SEM and MIP measurements [J]. Journal of Building Engineering. 2023, 67106011.

[40]

Füredi M, Manzano C V, Marton Aet al. . Beyond the meso/macroporous boundary: Extending capillary condensation-based pore size characterization in thin films through tailored adsorptives [J]. The Journal of Physical Chemistry Letters. 2024, 1551420-1427.

[41]

Zhang A, Ge Y, Yang W-cet al. . New insight of solvent-replacement-induced damage to pores of cement stone by comparison with 1H NMR relaxometry, mercury intrusion porosimetry, and nitrogen adsorption [J]. Construction and Building Materials. 2023, 409: 133981.

[42]

Liu K-q, Yang X-s, Zhang Het al. . Pore connectivity of oil well cement in the early hydration stage by in situ electrical resistivity measurements and low-field nuclear magnetic resonance [J]. Construction and Building Materials. 2021, 303124448.

[43]

Hu K, Liu Y-f, Zhang Qet al. . From micropores to macropores: Investigating pore characteristics of Longmaxi Shale in the Sichuan Basin [J]. Energy & Fuels. 2024, 3853961-3981.

[44]

Ouellet S, Bussière B, Aubertin Met al. . Microstructural evolution of cemented paste backfill: Mercury intrusion porosimetry test results [J]. Cement and Concrete Research. 2007, 37121654-1665.

[45]

Zeng L, Zhu J-y, Zhao Yet al. . Pore structure characteristics and permeability analysis of natural anhydrite with various water/anhydrite ratios based on mercury intrusion porosimetry [J]. Construction and Building Materials. 2023, 398: 132422.

[46]

Yang J-w, Cui Y-j, Mokni Net al. . Microstructural investigation into the damage behaviour of MX80 bentonite pellet under wetting/drying path using mercury intrusion porosimetry (MIP) and micro-computed tomography (μCT) [J]. Engineering Geology. 2023, 322107168.

[47]

Wang J-l, Wang X-y, Ding S-qet al. . Micro-nano scale pore structure and fractal dimension of ultra-high performance cementitious composites modified with nanofillers [J]. Cement and Concrete Composites. 2023, 141105129.

[48]

Mohan M K, Rahul A V, van Stappen J Fet al. . Assessment of pore structure characteristics and tortuosity of 3D printed concrete using mercury intrusion porosimetry and X-ray tomography [J]. Cement and Concrete Composites. 2023, 140105104.

[49]

Gao R-g, Wang W-j, Xiong Xet al. . Effect of curing temperature on the mechanical properties and pore structure of cemented backfill materials with waste rock-tailings [J]. Construction and Building Materials. 2023, 409133850.

[50]

Qin H, Cao S, Yilmaz E. Mechanical, energy evolution, damage and microstructural behavior of cemented tailings-rock fill considering rock content and size effects [J]. Construction and Building Materials. 2024, 411134449.

[51]

Standard for test methods of concrete physical and mechanical properties: GB/T 50081-2019[S]. (in Chinese)

[52]

Standard test method for determination of pore volume and pore volume distribution of soil and rock by mercury intrusion porosimetry: ASTM, D 4404-10 [S].

[53]

Zhou Y, Yin S-h, Zhao Ket al. . Understanding the static rate dependence of early fracture behavior of cemented paste backfill using digital image correlation and acoustic emission techniques [J]. Engineering Fracture Mechanics. 2023, 283109209.

[54]

Awoyera P O, Akinmusuru J O, Dawson A Ret al. . Microstructural characteristics, porosity and strength development in ceramic-laterized concrete [J]. Cement and Concrete Composites. 2018, 86224-237.

[55]

Hou D-w, Li D-y, Hua P-cet al. . Statistical modelling of compressive strength controlled by porosity and pore size distribution for cementitious materials [J]. Cement and Concrete Composites. 2019, 96: 11-20.

[56]

Yu X-z, Liu H, Fan X-let al. . Research on the permeability and pore structure distribution characteristics of high-performance mortar for surface treatment of bridge piers and columns [J]. Buildings. 2024, 14(3): 811.

[57]

Hu J-h, Ren Q-f, Ma S-wet al. . Macroscopic and microscopic trans-scale characteristics of pore structure of mine grouting materials [J]. Transactions of Nonferrous Metals Society of China. 2019, 2951067-1081.

[58]

Li Y, Fu J-x, Wang Ket al. . Influence of shell ash on pore structure and mechanical characteristics of cemented tailings backfill [J]. Construction and Building Materials. 2024, 411: 134473.

[59]

Chen S-m, Yilmaz E, Xiang Z-get al. . Curing conditions effect on pore structure, compressive strength and elastic modulus of cementitious tailings backfills [J]. Powder Technology. 2023, 422118458.

[60]

Richard T, Dagrain F, Poyol Eet al. . Rock strength determination from scratch tests [J]. Engineering Geology. 2012, 147–14891-100.

[61]

Qi C-c, Zheng J-s, Yang X-yet al. . Application of deep neural network in the strength prediction of cemented paste backfill based on a global dataset [J]. Construction and Building Materials. 2023, 391131827.

RIGHTS & PERMISSIONS

Central South University

PDF

0

Accesses

0

Citation

Detail

Sections
Recommended

/