Temperature influence on fracture behavior in clay-rich mudstone: A comprehensive experimental study

Abdel Kareem Alzo’ubi , Mahmoud Alneasan

Journal of Central South University ›› 2025, Vol. 32 ›› Issue (11) : 4463 -4485.

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Journal of Central South University ›› 2025, Vol. 32 ›› Issue (11) :4463 -4485. DOI: 10.1007/s11771-025-6115-z
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Temperature influence on fracture behavior in clay-rich mudstone: A comprehensive experimental study

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Abstract

This study investigates the fracture behavior of clay-rich mudstone under varying temperature and pressure conditions, which is crucial for the safety of geological structures. It focuses on three fracture types: pure mode I tensile fractures, pure mode II tensile fractures, and shear fractures, examining specimens at room temperature (RT) and after thermal treatments at 250 and 500 °C. The findings reveal that increasing temperatures makes the mudstone more brittle, enhancing fracture velocity, toughness, load-bearing capacity, roughness, and the fracture process zone (FPZ) radius. Notably, tensile fractures induced under pure mode II displayed the highest velocities, while shear fractures exhibited the lowest velocities, smoothest surfaces, and greatest resistance to failure. The application of a confining pressure of 4 MPa significantly improved shear fracture toughness by 119.7%, 98.5% and 71.9% at RT, 250 °C and 500 °C, respectively, and reduced roughness by 8.2%, 22.4% and 30.4%. This research offers a novel, comprehensive view of how temperature and pressure impact fractures in mudstone sensitive to temperature due to its high clay content and water affinity. The findings provide valuable insights applicable to geothermal energy, oil and gas exploration, and underground construction, thereby enhancing the understanding of fracture mechanics in geological contexts.

Keywords

pure mode I tensile fractures / pure mode II tensile fractures / shear fractures / temperature / fracture speed / fracture process zone

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Abdel Kareem Alzo’ubi, Mahmoud Alneasan. Temperature influence on fracture behavior in clay-rich mudstone: A comprehensive experimental study. Journal of Central South University, 2025, 32(11): 4463-4485 DOI:10.1007/s11771-025-6115-z

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References

[1]

Zhang X-p, Jiang Y-j, Du Y, et al.. Influence of joint spacing and rock characteristics on the toppling stability of cut rock slope through a simplified limit equilibrium method [J]. Journal of Central South University, 2024, 31(8): 2694-2702

[2]

Wu X-k, Zhao G-m, Meng X-r, et al.. Load-bearing characteristics and energy evolution of fractured rock masses after granite and sandstone grouting [J]. Journal of Central South University, 2024, 31(8): 2810-2825

[3]

Kravchuk M, Chemenda A I, Ambre J. Spatial arrangements and clustering of opening-mode fractures in experimental models of layered rocks [J]. Journal of Structural Geology, 2025, 196: 105392

[4]

Li X, Konietzky H, Li X-b, et al.. Failure pattern of brittle rock governed by initial microcrack characteristics [J]. Acta Geotechnica, 2019, 14(5): 1437-1457

[5]

Ma X, Wang G-l, Hu D-w, et al.. Hydraulic fracturing of granite under real-time high temperature and true triaxial stress [J]. Journal of Central South University, 2023, 30(1243-256

[6]

Ding R, Sun Q, Jia H-l, et al.. Experimental study on the compressive strength and AE characteristics of high-temperature-treated and LN2-cooled sandstone [J]. International Journal of Geomechanics, 2024, 24(4): 04024040

[7]

Occhiena C, Pirulli M. Analysis of climatic influences on slope microseismic activity and rockfalls: Case study of the Matterhorn peak (northwestern Alps) [J]. Journal of Geotechnical and Geoenvironmental Engineering, 2012, 138(81012-1021

[8]

Feng C-c, Wang Z-l, Wang J-g, et al.. A thermo-mechanical damage constitutive model for deep rock considering brittleness-ductility transition characteristics [J]. Journal of Central South University, 2024, 31(7): 2379-2392

[9]

Shan J-t, Wu Y-m, Yang X-L. Three-dimensional stability of two-step slope with crack considering temperature effect on unsaturated soil [J]. Journal of Central South University, 2025, 32(3): 1060-1079

[10]

Ju Y, Xing D-y, Ren Z-y, et al.. Optical quantification and characterization of 3D stress fields and plastic zones around arch tunnel models using stress freezing and 3D printing techniques [J]. International Journal of Rock Mechanics and Mining Sciences, 2025, 189: 106088

[11]

Yu Z-y, Shen S-w, Li M, et al.. An improved rock damage model from a cyclic temperature-triaxial loading experiment for compressed air energy storage Caverns [J]. Engineering Geology, 2025, 344: 107857

[12]

Pan J-l, Feng Z-m, Zhang Y, et al.. Experimental study on evaluation of porosity, thermal conductivity, UCS, and elastic modulus of granite after thermal and chemical treatments by using P-wave velocity [J]. Geoenergy Science and Engineering, 2023, 230: 212184

[13]

Ren J-f, Liu X-j, Xiong J, et al.. Experimental study on the acoustic wave propagation characteristics of bedding shales under changes in temperature and pressure [J]. Natural Gas Industry B, 2023, 10(5): 407-418

[14]

Zhang P, Wang C, Gao Z, et al.. Combined effects of high temperature and lithology on the tensile mechanical damage and fracture surface morphology of reservoir rocks [J]. Bulletin of Engineering Geology and the Environment, 2024, 83(6226

[15]

Justo J, Castro J. Mechanical properties of 4 rocks at different temperatures and fracture assessment using the strain energy density criterion [J]. Geomechanics for Energy and the Environment, 2021, 25: 100212

[16]

Jiang T-q, Chen B, Zhang Q-s, et al.. Thermal stimulation mechanical response and shear dilatation predictive model improvement of granite fractures in an enhanced geothermal system [J]. Journal of Materials Research and Technology, 2024, 28: 4334-4349

[17]

Guo T-y, Wong L N Y, Wu Z-J. Microcracking behavior transition in thermally treated granite under mode I loading [J]. Engineering Geology, 2021, 282: 105992

[18]

Feng Y-j, Su H-j, Yu L-y, et al.. Mixed mode I–II fracture mechanism of sandstone samples after thermal treatment: Insights from optical monitoring and thermal analysis [J]. Theoretical and Applied Fracture Mechanics, 2023, 125: 103883

[19]

Rezaee H, Noorian-Bidgoli M. Numerical and experimental investigation of the influence of temperature and grain size on the fracture behavior of rock [J]. Journal of Rock Mechanics and Geotechnical Engineering, 2025, 17(21102-1119

[20]

Zhou M, He F-f, Zhang W-y, et al.. Effect of high temperature on the mixed mode I-II fracture characteristics of hot-dry rock [J]. Engineering Fracture Mechanics, 2024, 303: 110141

[21]

Hasanzadeh Samani F, Behnia M. Investigating the impact of thermal treatment on fracture toughness and sub-critical crack growth parameters under mode II loading [J]. Theoretical and Applied Fracture Mechanics, 2024, 134: 104694

[22]

Li X, Xu Y, Zhan Z-f, et al.. Influence of thermal treatment on dynamic mode II fracture properties of rocks using the short core in compression (SCC) method [J]. Theoretical and Applied Fracture Mechanics, 2022, 119: 103383

[23]

Liu L-m, He H-l, Dyck M, et al.. Modeling thermal conductivity of clays: A review and evaluation of 28 predictive models [J]. Engineering Geology, 2021, 288: 106107

[24]

Sun W-j, Wei Z-f, Sun D-a, et al.. Evaluation of the swelling characteristics of bentonite-sand mixtures [J]. Engineering Geology, 2015, 199: 1-11

[25]

Alibrahim B, Garoushi A H B, Uygar E. The role of calcium-based additives in bentonite stabilization: A comparative evaluation [J]. Arabian Journal for Science and Engineering, 2025, 50(118425-8438

[26]

Rimi A, Zarhloule Y, Barkaoui A E, et al.. Towards a de-carbonized energy system in north-eastern Morocco: Prospective geothermal resource [J]. Renewable and Sustainable Energy Reviews, 2012, 16(4): 2207-2216

[27]

Chong K P, Kuruppu M D. New specimen for fracture toughness determination for rock and other materials [J]. International Journal of Fracture, 1984, 26(2): R59-R62

[28]

Alneasan M, Behnia M, Bagherpour R. Analytical and numerical investigations of dynamic crack propagation in brittle rocks under mixed mode loading [J]. Construction and Building Materials, 2019, 222: 544-555

[29]

Alneasan M, Behnia M, Bagherpour R. Applicability of the classical fracture mechanics criteria to predict the crack propagation path in rock under compression [J]. European Journal of Environmental and Civil Engineering, 2020, 24(11): 1761-1784

[30]

Alneasan M, Behnia M, Bagherpour R. Frictional crack initiation and propagation in rocks under compressive loading [J]. Theoretical and Applied Fracture Mechanics, 2018, 97: 189-203

[31]

Jung Y, Park E, Kim H. Determination of mode II toughness of granite by using SCC test [C]. Rock Mechanics and Rock Engineering: From the Past to the Future, 2016, Cappadocia, Turkey, CRC Press

[32]

Xu Y, Yao W, Zhao G-l, et al.. Evaluation of the short core in compression (SCC) method for measuring mode II fracture toughness of rocks [J]. Engineering Fracture Mechanics, 2020, 224: 106747

[33]

Yao W, Xu Y, Wang C-l, et al.. Dynamic Mode I fracture behavior of rocks under hydrostatic pressure using the short core in compression (SCC) method [J]. International Journal of Mining Science and Technology, 2021, 31(5): 927-937

[34]

Alneasan M, Alzo’ubi A K, Okasha N. A comprehensive study for the effect of sample geometry and lateral pressure on shear fractures using the short core in compression (SCC) method [J]. European Journal of Mechanics-A/Solids, 2023, 100: 104988

[35]

Yin T-b, Zhang S-s, Li X-b, et al.. A numerical estimate method of dynamic fracture initiation toughness of rock under high temperature [J]. Engineering Fracture Mechanics, 2018, 204: 87-102

[36]

Folk R L. Petrology of sedimentary rocks [M], 1980

[37]

Xiang L, Liu X-d, Liu P-h, et al.. Research insights of argillaceous-based site for high-level radioactive waste disposal in China [J]. Journal of Radioanalytical and Nuclear Chemistry, 2025, 334(1795-805

[38]

Li X, Chen L, Zhu X-m, et al.. Geothermal reservoir characteristics of SYYD-1 well and energy efficiency analysis after geothermal transformation [J]. Geothermics, 2024, 118: 102921

[39]

Ma J, Zhang Y-l, Lv J-k, et al.. Experimental study on permeability characteristics of mudstone under high temperature overburden condition [J]. Processes, 2023, 11(10): 2828

[40]

Jun J, Liang W. Investigation of the pore structure characteristics and fluid components of Quaternary mudstone biogas reservoirs: A case study of the Qaidam Basin in China [J]. Scientific Reports, 2024, 14(126512

[41]

Alneasan M, Behnia M. Strain rate effects on the crack propagation speed under different loading modes (I, II and I/II): Experimental investigations [J]. Engineering Fracture Mechanics, 2021, 258: 108118

[42]

Poliakov A N B, Dmowska R, Rice J R. Dynamic shear rupture interactions with fault bends and off-axis secondary faulting [J]. Journal of Geophysical Research: Solid Earth, 2002, 107(B11ESE6-1-18

[43]

Zhang J, Little D N, Grajales J, et al.. Use of semicircular bending test and cohesive zone modeling to evaluate fracture resistance of stabilized soils [J]. Transportation Research Record: Journal of the Transportation Research Board, 2017, 2657(167-77

[44]

Ayatollahi M R, Aliha M R M. Wide range data for crack tip parameters in two disc-type specimens under mixed mode loading [J]. Computational Materials Science, 2007, 38(4660-670

[45]

Erdogan F, Sih G C. On the crack extension in plates under plane loading and transverse shear [J]. Journal of Basic Engineering, 1963, 85(4): 519-525

[46]

Sih G C. Strain-energy-density factor applied to mixed mode crack problems [J]. International Journal of Fracture, 1974, 10(3): 305-321

[47]

Palaniswamy K. Crack propagation under general inplane loading [D], 1972, Pasadena, USA, California Institute of Technology

[48]

Whittaker B N, Singh R, Sun G-X. Rock fracture mechanics: Principles, design and applications [M], 2011, Amsterdam, Elsevier

[49]

Bao X-k, Tao M, Zhao J-C. Study of mixed mode fracture toughness and fracture trajectories in gypsum interlayers in corrosive environment [J]. Royal Society Open Science, 2018, 5(1): 171374

[50]

Smith D J, Ayatollahi M R, Pavier M J. The role of 7-stress in brittle fracture for linear elastic materials under mixed-mode loading [J]. Fatigue & Fracture of Engineering Materials & Structures, 2001, 24(2137-150

[51]

Ayatollahi M R, Rashidi Moghaddam M, Berto F. A generalized strain energy density criterion for mixed mode fracture analysis in brittle and quasi-brittle materials [J]. Theoretical and Applied Fracture Mechanics, 2015, 79: 70-76

[52]

Alneasan M, Behnia M. An experimental investigation on tensile fracturing of brittle rocks by considering the effect of grain size and mineralogical composition [J]. International Journal of Rock Mechanics and Mining Sciences, 2021, 137: 104570

[53]

Whitehouse D J. Surfaces and their measurement [M], 2002

[54]

Akhavan A, Shafaatian S M H, Rajabipour F. Quantifying the effects of crack width, tortuosity, and roughness on water permeability of cracked mortars [J]. Cement and Concrete Research, 2012, 42(2): 313-320

[55]

Su X-p, Zhou L, Li H-l, et al.. Effect of mesoscopic structure on hydro-mechanical properties of fractures [J]. Environmental Earth Sciences, 2020, 79(6146

[56]

Alzo’ubi A. Fracture mechanisms of open offset rock joints under uniaxial loading [D], 2001, Irbid, Jordan, Jordan University of Science and Technology

[57]

Bear J. Dynamics of fluids in porous media [J]. Soil Science, 2022, 120: 162-163

[58]

Cook D. Calcined clay, shale and other soils [M]. Cement Replacement Materials, 1986, London, UK, Surrey University Press

[59]

Kuruppu M D, Obara Y, Ayatollahi M R, et al.. ISRM-suggested method for determining the mode I static fracture toughness using semi-circular bend specimen [J]. Rock Mechanics and Rock Engineering, 2014, 47(1267-274

[60]

Dou Z-h, Gao T-y, Zhao Z-h, et al.. The role of water lubrication in critical state fault slip [J]. Engineering Geology, 2020, 271: 105606

[61]

Chu P, Xie H-p, Chen C-c, et al.. Fracture behavior and fracture surface roughness of high-temperature granite subjected to liquid nitrogen and water cooling [J]. Engineering Fracture Mechanics, 2024, 300: 109987

[62]

Chen C-c, Chu P, Xie H-p, et al.. Fracture behavior of high-temperature granite subjected to liquid nitrogen cooling: Semi-circular bending test and crack evolution analysis [J]. Theoretical and Applied Fracture Mechanics, 2023, 128: 104100

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