Thermal compression behavior and microstructural evolution of selective laser melted AlMgScZr high-strength aluminum alloys

Zeng-wei Zhu , Qian-li Liu , Qiu-ping Wang , Tao Jiang , Jie-ren Guan

Journal of Central South University ›› 2025, Vol. 32 ›› Issue (11) : 4260 -4280.

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Journal of Central South University ›› 2025, Vol. 32 ›› Issue (11) :4260 -4280. DOI: 10.1007/s11771-025-6114-0
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Thermal compression behavior and microstructural evolution of selective laser melted AlMgScZr high-strength aluminum alloys

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Abstract

The AlMgScZr high-strength aluminum alloy fabricated by selective laser melting (SLM) technology exhibits a “bimodal microstructure”, resulting in significant non-uniform deformation during thermal deformation. This study investigates the flow behavior of SLM-processed AlMgScZr aluminum alloy utilizing the Gleeble-1500D thermal simulation machine. The true stress–strain curves were amended based on the friction theory. Through determining the Zener-Hollomon parameters, the correlation between flow stress, deformation temperature, and strain rate during the high-temperature thermoplastic deformation of SLM-processed AlMgScZr aluminum alloy with a “bimodal microstructure” was established. In addition, the microstructural evolution during thermal deformation was analyzed. The results indicated that the predicted flow stress values obtained from the Arrhenius constitutive equation with coupled correction of thermal deformation parameters closely matched the experimental values. The correlation coefficient and the average absolute relative error of the corrected model were 0.999 and 2.766%, respectively, accurately predicting the thermoplastic deformation behavior of SLM-processed high-strength aluminum alloy with a “bimodal microstructure”. Furthermore, hot processing maps at different strains were established, identifying stable and unstable regions under different deformation conditions. Microstructural observations revealed different thermal deformation mechanisms under various deformation temperatures. Specifically, dynamic recrystallization characteristics dominated the microstructure at lower temperatures (300–360 °C), while dynamic recovery was dominant at higher temperatures (390–500 °C).

Keywords

selective laser melting / AlMgScZr high-strength aluminum alloy / thermal deformation / microstructure / constitutive model

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Zeng-wei Zhu, Qian-li Liu, Qiu-ping Wang, Tao Jiang, Jie-ren Guan. Thermal compression behavior and microstructural evolution of selective laser melted AlMgScZr high-strength aluminum alloys. Journal of Central South University, 2025, 32(11): 4260-4280 DOI:10.1007/s11771-025-6114-0

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References

[1]

Zhang J-l, Song B, Wei Q-s, et al.. A review of selective laser melting of aluminum alloys: Processing, microstructure, property and developing trends [J]. Journal of Materials Science & Technology, 2019, 35(2): 270-284

[2]

Huang W-d, Lin X. Research progress in laser solid forming of high-performance metallic components at the state key laboratory of solidification processing of China [J]. 3D Printing and Additive Manufacturing, 2014, 1(3): 156-165

[3]

GRADL P, MIRELES O R, ATSARELIS C, et al. Advancement of extreme environment additively manufactured alloys for next generation space propulsion applications [J]. Acta Astronautica, 2023. DOI: https://doi.org/10.1016/j.actaastro.2023.06.035.

[4]

Bici M, Brischetto S, Campana F, et al.. Development of a multifunctional panel for aerospace use through SLM additive manufacturing [J]. Procedia CIRP, 2018, 67: 215-220

[5]

EOS and hyperganic team up to elevate the design and performance of space propulsion components [EB/OL]. [2024-07-17]. https://www.eos.info/en-us/press-media/press-center/press-releases/eos-and-hyperganic.

[6]

Spierings A B, Dawson K, Heeling T, et al.. Microstructural features of Sc- and Zr-modified Al-Mg alloys processed by selective laser melting [J]. Materials & Design, 2017, 115: 52-63

[7]

Spierings A B, Dawson K, Kern K, et al.. SLM-processed Sc- and Zr- modified Al-Mg alloy: Mechanical properties and microstructural effects of heat treatment [J]. Materials Science and Engineering A, 2017, 701: 264-273

[8]

Wang Z-h, Lin X, Kang N, et al.. Laser powder bed fusion of high-strength Sc/Zr-modified Al-Mg alloy: Phase selection, microstructural/mechanical heterogeneity, and tensile deformation behavior [J]. Journal of Materials Science & Technology, 2021, 95: 40-56

[9]

Li X, Liu Y-z, Tan C-l, et al.. Laser powder bed fusion of a novel crack-free Al-Mg-Sc-Zr alloy: Printability, microstructure characterization and mechanical performance [J]. Optics & Laser Technology, 2023, 162: 109281

[10]

Xue D, Wei W, Shi W, et al.. Dislocation evolution and induced precipitation on corrosion resistance of a novel Al-Mg-Zn-Er-Zr alloy during hot compression [J]. Rare Metals, 2023, 42(7): 2371-2380

[11]

Guan J-r, Wang Q-P. The effect of a remelting treatment scanning strategy on the surface morphology, defect reduction mechanism, and mechanical properties of a selective laser-melted Al-based alloy [J]. Journal of Materials Science, 2022, 57(219807-9817

[12]

Wang Q-p, Zhu Z-w, Guan J-r, et al.. The influence mechanisms of re-fused scanning on the surface roughness, microstructural evolution and mechanical properties of laser powder bed fusion processed AlMgScZr alloy [J]. Optics & Laser Technology, 2024, 177: 111060

[13]

Wang J-h, Liu T, Luo L-s, et al.. Selective laser melting of high-strength TiB2/AlMgScZr composites: Microstructure, tensile deformation behavior, and mechanical properties [J]. Journal of Materials Research and Technology, 2022, 16: 786-800

[14]

NASA’s innovative rocket nozzle paves way for deep space missions-NASA [EB/OL]. [2025-05-11]. https://www.nasa.gov/centers-and-facilities/marshall/nasas-innovative-rocket-nozzle-paves-way-for-deep-space-missions/.

[15]

Lei C, Wang Q-d, Ebrahimi M, et al.. Hot deformation behavior and processing maps of an As-cast Al-5Mg-3Zn-1Cu (wt%) alloy [J]. Materials, 2023, 16(11): 4093

[16]

Khomutov M G, Pozdniakov A V, Churyumov A Y, et al.. Flow stress modelling and 3D processing maps of Al4.5Zn4.5Mg1Cu0.12Zr alloy with different scandium contents [J]. Applied Sciences, 2021, 11(104587

[17]

Xia Y-x, Shu X-d, Zhang Q-d, et al.. Modified Arrhenius constitutive model and simulation verification of 2A12-T4 aluminum alloy during hot compression [J]. Journal of Materials Research and Technology, 2023, 26: 1325-1340

[18]

Harikrishna K, Bhowmik A, Davidson M J, et al.. Evaluation of constitutive equations for modeling and characterization of microstructure during hot deformation of sintered Al-Zn-Mg alloy [J]. Journal of Materials Research and Technology, 2024, 28: 1523-1537

[19]

Hamed M. Simple physically-based constitutive equations for hot deformation of 2024 and 7075 aluminum alloys [J]. Transactions of Nonferrous Metals Society of China, 2015, 25(51614-1618

[20]

Shi D-j, Zhang F, He Z-y, et al.. Constitutive equation and dynamic recovery mechanism of high strength cast Al-Cu-Mn alloy during hot deformation [J]. Materials Today Communications, 2022, 33: 104199

[21]

Zhang Z-w, Liu R-x, Li D-y, et al.. Investigation on deformation behaviors and dynamic recrystallization mechanism of spray formed Al-Zn-Mg-Cu alloy under hot compression [J]. Journal of Materials Research and Technology, 2024, 28: 4401-4416

[22]

Wang M-h, Wei K, Li X-j, et al.. Constitutive modeling for high temperature flow behavior of a high-strength manganese brass [J]. Journal of Central South University, 2018, 25(7): 1560-1572

[23]

Jiang J-y, Jiang F, Huang H-f, et al.. Hot deformation analysis and microstructure evolution of Al-Mg-Mn-Sc-Zr alloy by isothermal compression [J]. Journal of Alloys and Compounds, 2021, 858: 157655

[24]

Li B, Pan Q-l, Yin Z-M. Microstructural evolution and constitutive relationship of Al-Zn-Mg alloy containing small amount of Sc and Zr during hot deformation based on Arrhenius-type and artificial neural network models [J]. Journal of Alloys and Compounds, 2014, 584: 406-416

[25]

Wang L, Liu F, Cheng J J, et al.. Arrhenius-type constitutive model for high temperature flow stress in a nickel-based corrosion-resistant alloy [J]. Journal of Materials Engineering and Performance, 2016, 25(4): 1394-1406

[26]

Li B, Chu Z J, Du Y, et al.. Hot deformation behavior and dynamic recrystallization kinetics of a novel Sc and Zr modified ultra-high-strength Al-Zn-Mg-Cu alloy [J]. Journal of Materials Engineering and Performance, 2020, 29(12): 7774-7784

[27]

Xu C-l, Huang J-w, Jiang F-q, et al.. Dynamic recrystallization and precipitation behavior of a novel Sc, Zr alloyed Al-Zn-Mg-Cu alloy during hot deformation [J]. Materials Characterization, 2022, 183: 111629

[28]

Wang Z-h, Lin X, Wang J-f, et al.. Remarkable strength-impact toughness conflict in high-strength Al-Mg-Sc-Zr alloy fabricated via laser powder bed fusion additive manufacturing [J]. Additive Manufacturing, 2022, 59: 103093

[29]

Huang G-q, Shen T, Li B. Microstructural evolution modelling and low-stress fatigue performance of bimodal-structured Al-Mg-Sc-Zr alloy produced by laser powder bed fusion additive manufacturing [J]. Virtual and Physical Prototyping, 2024, 19: e2346287

[30]

Ebrahimi R, Najafizadeh A. A new method for evaluation of friction in bulk metal forming [J]. Journal of Materials Processing Technology, 2004, 152(2): 136-143

[31]

Zhang X, Wang X-x, Zhang D-K. Investigation into constitutive equation and hot compression deformation behavior of 6061 Al alloy [J]. Technical Gazette, 2019, 26(51376-1382

[32]

Jonas J J, Sellars C M, Mcg Tegart W J. Strength and structure under hot-working conditions [J]. Metallurgical Reviews, 1969, 14(1): 1-24

[33]

Medina S F, Hernandez C A. General expression of the Zener-Hollomon parameter as a function of the chemical composition of low alloy and microalloyed steels [J]. Acta Materialia, 1996, 44(1): 137-148

[34]

Wang L, Liu F, Cheng J J, et al.. Hot deformation characteristics and processing map analysis for nickel-based corrosion resistant alloy [J]. Journal of Alloys and Compounds, 2015, 623: 69-78

[35]

Chakravartty J K, Prasad Y V R K, Asundi M K. Processing map for hot working of alpha-zirconium [J]. Metallurgical Transactions A, 1991, 22(4): 829-836

[36]

Prasad Y V R K. Recent advances in the science of mechanical processing [J]. Indian Journal of Technology, 2024, 28: 435-451

[37]

Deng Y, Zhu X-w, Lai Y, et al.. Effects of Zr/(Sc+ Zr) microalloying on dynamic recrystallization, dislocation density and hot workability of Al - Mg alloys during hot compression deformation [J]. Transactions of Nonferrous Metals Society of China, 2023, 33(3): 668-682

[38]

Prasad Y V R K, Rao K P, Sasidhara S. Hot Working Guide: A Compendium of Processing Maps, 20152nd EditionMaterials Park OH, ASM Int.

[39]

Tao C-c, Zhou G, Huang H-j, et al.. Research on energy dissipation and dynamic recrystallization microstructure evolution behavior of NiTi alloy during hot deformation [J]. Materials Characterization, 2024, 208: 113673

[40]

Wang Q-p, Zhou R-f, Guan J-r, et al.. The deformation compatibility and recrystallisation behaviour of the alloy CuSn10P1 [J]. Materials Characterization, 2021, 174: 110940

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