Improvement of microstructure and microhardness of AZ31 Mg alloy sheet by cross-forging-bending repeated deformation with sharply increasing temperature

Li-wei Lu , Xing-jie Liang , Min-hao Li , Yu-hui Wei , Yu-ze Xi , Min Ma , Lei Jing , Li-fei Wang , Jun Dong

Journal of Central South University ›› 2025, Vol. 32 ›› Issue (11) : 4210 -4227.

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Journal of Central South University ›› 2025, Vol. 32 ›› Issue (11) :4210 -4227. DOI: 10.1007/s11771-025-6100-6
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Improvement of microstructure and microhardness of AZ31 Mg alloy sheet by cross-forging-bending repeated deformation with sharply increasing temperature

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Abstract

In this study, AZ31 Mg alloy sheets were processed by a severe plastic deformation (SPD) technique called forging-bending repeated deformation (FBRD). The effect on the microstructure and microhardness of AZ31 Mg alloy through FBRD was investigated with increasing temperature treatment and a 90° cross route. The results reveal that the effective strain increases with the number of passes. The flow uniformity is effectively enhanced due to alterations in shear deformation direction. After four passes of deformation, the average grain size is refined by 79.3% compared to the initial specimen. The grain refinement mechanism predominantly originates from the synergistic effects of discontinuous dynamic recrystallization (DDRX), continuous dynamic recrystallization (CDRX), and twinning-induced recrystallization (TDRX). The formation of

{101¯2}
extension twins (ET) significantly contributes to coarse grain subdivision and plastic deformation coordinated. Furthermore, pyramidal <c+a> slip activation effectively enhances the plasticity of Mg alloys. By post four-pass processing, the alloy exhibits a microhardness of 81.9HV, primarily governed by fine grain strengthening and dislocation strengthening mechanisms.

Keywords

AZ31 Mg alloy sheet / forging-bending repeated deformation / microstructure / microhardness

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Li-wei Lu, Xing-jie Liang, Min-hao Li, Yu-hui Wei, Yu-ze Xi, Min Ma, Lei Jing, Li-fei Wang, Jun Dong. Improvement of microstructure and microhardness of AZ31 Mg alloy sheet by cross-forging-bending repeated deformation with sharply increasing temperature. Journal of Central South University, 2025, 32(11): 4210-4227 DOI:10.1007/s11771-025-6100-6

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References

[1]

Ding N, Du W-b, Zhu X-m, et al.. Roles of LPSO phases on dynamic recrystallization of high strain rate multi-directional free forged Mg-Gd-Er-Zn-Zr alloy and its strengthening mechanisms [J]. Materials Science and Engineering A, 2023, 864: 144590

[2]

Huang Z-q, Qi C-l, Zou J-c, et al.. Edge crack damage analysis of AZ31 magnesium alloy hot-rolled plate improved by vertical roll pre-rolling [J]. Journal of Magnesium and Alloys, 2023, 11(6): 2151-2164

[3]

Zhang L, Zhang H-g, Liu Y-z, et al.. Revealing the dynamic recrystallization mechanism, extrusion deformation mechanism, and tensile deformation behavior of Mg-6Al-1Zn-1.1Sc alloy [J]. Journal of Materials Research and Technology, 2023, 23: 5907-5922

[4]

Sun L-x, Bai J, Xue F. Evolutions of microstructure and texture of Mg-Gd alloy wires processed by cold drawing [J]. Journal of Materials Research and Technology, 2022, 21: 3961-3969

[5]

Yuan M, He C, Zhao J, et al.. Microstructure evolution and mechanical properties of the Mg-Sm-Gd-Zn-Zr alloy during extrusion [J]. Journal of Materials Research and Technology, 2021, 15: 2518-2528

[6]

Yuan Y-x, Ma A-b, Wu H-r, et al.. Optimizing microstructure and mechanical properties of biomedical Mg-Y-Zn-Mn alloy with LPSO phases by solution treatment plus equal-channel angular pressing [J]. Journal of Materials Research and Technology, 2022, 16: 968-976

[7]

Zohrevand M, Mohammadi-Zerankeshi M, Nobakht-Farin F, et al.. Degradation behavior of the as-extruded and ECAP-processed Mg-4Zn alloy by Ca addition and hydrothermal coating [J]. Journal of Materials Research and Technology, 2022, 20: 1204-1215

[8]

Bu D-h, Li T, Han X-l, et al.. Enhancing strength and ductility in back extruded WE71 magnesium alloy cylindrical parts by introduction of multi-direction forging process [J]. Journal of Rare Earths, 2023, 41(3462-470

[9]

Zhao J-q, Guo H-s, Luo T-t, et al.. Microstructure evolution and grain refinement mechanism of fine-grained Mg-Gd-Y-Zn-Zr alloy during multi-directional forging [J]. Journal of Alloys and Compounds, 2022, 928: 167199

[10]

Zhao X, Li S-c, Zheng Y-s, et al.. The microstructure evolution, texture weakening mechanism and mechanical properties of AZ80 Mg alloy processed by repetitive upsetting-extrusion with reduced deformation temperature [J]. Journal of Alloys and Compounds, 2021, 883: 160871

[11]

Fan Y-t, Lu L-w, Zhou T, et al.. Improvement of the microstructure and microhardness of AQ80 magnesium alloy by repeated upsetting-extrusion [J]. Metals and Materials International, 2023, 29(10): 3052-3065

[12]

Zheng L-w, Zhang X-p, Wang H-x, et al.. Synergistic effect of LPSO and eutectic phase on mechanical properties of Mg-Gd-Nd-Zn-Zr alloy during equal channel angular pressing [J]. Journal of Materials Research and Technology, 2021, 15: 2459-2470

[13]

Cui C, Zhang W-c, Chen W-z, et al.. Microstructure, texture evolution and yield strength symmetry improvement of as-extruded ZK60 Mg alloy via multi-directional impact forging [J]. Journal of Magnesium and Alloys, 2022, 10(102745-2760

[14]

Krajňák T, Minárik P, Gubicza J, et al.. Influence of equal channel angular pressing routes on texture, microstructure and mechanical properties of extruded AX41 magnesium alloy [J]. Materials Characterization, 2017, 123: 282-293

[15]

Li Q-z, Jiao X. Exploration of equal channel angular pressing routes for efficiently achieving ultrafine microstructure in magnesium [J]. Materials Science and Engineering A, 2018, 733: 179-189

[16]

Meng Y-z, Yu J-m, Yu H-s, et al.. Effect of variable temperature repetitive upsetting-extrusion on microstructure and texture of Mg-Gd-Y-Zr alloy [J]. Procedia Manufacturing, 2020, 50: 822-830

[17]

Huang C, Liu C-m, Jiang S-n, et al.. Enhanced age-hardening response and mechanical properties of the Mg-Gd-Y-Zn-Zr alloy by trace Ag addition [J]. Journal of Alloys and Compounds, 2021, 874: 159825

[18]

Huang Y, Langdon T G. Advances in ultrafine-grained materials [J]. Materials Today, 2013, 16(3): 85-93

[19]

Yamashita A, Horita Z, Langdon T G. Improving the mechanical properties of magnesium and a magnesium alloy through severe plastic deformation [J]. Materials Science and Engineering A, 2001, 300(12142-147

[20]

Chen H, Yang Y-m, Hu F-p, et al.. Improvement of severe plastic deformation realized by several passes rotary swaging in the microstructure and properties of Mg-0.6Mn-0.5Al-0.5Zn-0.4Ca alloy [J]. Materials Science and Engineering A, 2023, 865: 144629

[21]

Che B, Lu L-w, Kang W, et al.. Hot deformation behavior and processing map of a new type Mg-6Zn-1Gd-1Er alloy [J]. Journal of Alloys and Compounds, 2021, 862: 158700

[22]

Lin B-y, Zhang H, Meng Y-p, et al.. Deformation behavior, microstructure evolution, and dynamic recrystallization mechanism of an AZ31 Mg alloy under high-throughput gradient thermal compression [J]. Materials Science and Engineering A, 2022, 847: 143338

[23]

Feng Y-h, Qian L-y, Sun C-y, et al.. Twinning, dynamic recrystallization, and texture evolution in as-solution AZ80 Mg alloy during hot compression [J]. Journal of Materials Research and Technology, 2023, 25: 5159-5173

[24]

Lu L-w, Liu X-y, Shi D-f, et al.. Effect of twinning behavior on dynamic recrystallization during extrusion of AZ31Mg alloy [J]. JOM, 2019, 71(4): 1566-1573

[25]

Zhang H, Yang M-x, Hou M-j, et al.. Effect of pre-existing {101¯2}\documentclass[12pt]{minimal}\usepackage{amsmath}\usepackage{wasysym}\usepackage{amsfonts}\usepackage{amssymb}\usepackage{amsbsy}\usepackage{mathrsfs}\usepackage{upgreek}\setlength{\oddsidemargin}{-69pt}\begin{document}$$\{10\bar{1}2\}$$\end{document} extension twins on mechanical properties, microstructure evolution and dynamic recrystallization of AZ31 Mg alloy during uniaxial compression [J]. Materials Science and Engineering A, 2019, 744: 456-470

[26]

Son H W, Hyun S K. Dislocation characteristics and dynamic recrystallization in hot deformed AM30 and AZ31 alloys [J]. Journal of Magnesium and Alloys, 2022, 10(12): 3495-3505

[27]

Xu W-l, Yu J-m, Jia L-c, et al.. Deformation behavior of Mg-13Gd-4Y-2Zn-0.5Zr alloy on the basis of LPSO kinking, dynamic recrystallization and twinning during compression-torsion [J]. Materials Characterization, 2021, 178: 111215

[28]

Song G-s, Zhang S-h, Zheng L, et al.. Twinning, grain orientation and texture variation of AZ31 Mg alloy during compression by EBSD tracing [J]. Journal of Alloys and Compounds, 2011, 509(22): 6481-6488

[29]

Ma Q, Li B, Marin E B, et al.. Twinning-induced dynamic recrystallization in a magnesium alloy extruded at 450 °C [J]. Scripta Materialia, 2011, 65(9823-826

[30]

Zhang L, Yuan S, Wang J-h, et al.. Hot deformation behavior, processing map, microstructure evolution and dynamic recrystallization mechanism of Mg-5Al-0.6Sc alloy [J]. Journal of Alloys and Compounds, 2022, 922: 166244

[31]

Liu X-y, Le T-h, Yuan S, et al.. The microstructure and quasi-static compression properties at elevated temperatures of the aged vacuum die-casting Mg-4Al-4(La, Ce) alloy [J]. Journal of Materials Research and Technology, 2023, 23: 4293-4306

[32]

Zhu Y-z, Hou D-w, Li Q-Z. Quasi in situ EBSD analysis of twinning-detwinning and slip behaviors in textured AZ31 magnesium alloy subjected to compressive-tensile loading [J]. Journal of Magnesium and Alloys, 2022, 10(4): 956-964

[33]

Zhang D-d, Liu C-m, Jiang S-n, et al.. Effects of dynamic recrystallization mechanisms on texture evolution in Mg-Gd-Y-Zr-Ag alloy during hot compression [J]. Journal of Alloys and Compounds, 2023, 944: 169190

[34]

Pan X-h, Wang L-f, Li Y-q, et al.. Twinning and dynamic recrystallization behaviors during inchoate deformation of pre-twinned AZ31 Mg alloy sheet at elevated temperatures [J]. Journal of Alloys and Compounds, 2022, 917: 165495

[35]

Zhou S-b, Tang A-t, Liu T-t, et al.. Ductility enhancement by activating non-basal slip in as-extruded Mg alloys with dilute Sc addition [J]. Journal of Materials Research and Technology, 2023, 22: 3362-3374

[36]

Hao M-j, Cheng W-l, Wang L-f, et al.. Texture evolution induced by twinning and dynamic recrystallization in dilute Mg-1Sn-1Zn-1Al alloy during hot compression [J]. Journal of Magnesium and Alloys, 2020, 8(3): 899-909

[37]

Zhu S Q, Yan H G, Chen J H, et al.. Feasibility of high strain-rate rolling of a magnesium alloy across a wide temperature range [J]. Scripta Materialia, 2012, 67(4): 404-407

[38]

Woo S K, Pei R-s, Al-Samman T, et al.. Plastic instability and texture modification in extruded Mg-Mn-Nd alloy [J]. Journal of Magnesium and Alloys, 2022, 10(1): 146-159

[39]

Shahri Z, Zarei-Hanzaki A, Abedi H R, et al.. An investigation to the hot deformation characteristics of AZ31 alloy through continuous cooling compression testing method [J]. Materials & Design, 2012, 36: 470-476

[40]

Fan Y-t, Lu L-w, Zhao H-l, et al.. Effect of deformation temperatures on microstructure of AQ80 magnesium alloy under repeated upsetting-extrusion [J]. Acta Metallurgica Sinica (English Letters), 2023, 36(10): 1649-1664

[41]

Wang Q-h, Jiang B, Tang A-t, et al.. Formation of the elliptical texture and its effect on the mechanical properties and stretch formability of dilute Mg-Sn-Y sheet by Zn addition [J]. Materials Science and Engineering A, 2019, 746: 259-275

[42]

Zhou T-s, Liu Z-h, Yang D-l, et al.. High ductility in solution-treated Mg-Sc-Yb-Mn-Zr alloy mediated bydislocations [J]. Journal of Alloys and Compounds, 2021, 873: 159880

[43]

Jebelli A A, Fereshteh-Saniee F. Superior combined strength and elongation by conducting elevated temperature constrained groove pressing on Al-Mg-Mn sheets [J]. Materials Chemistry and Physics, 2023, 307: 128090

[44]

Zhong L-p, Wang Y-j, Dou Y-C. On the improved tensile strength and ductility of Mg: Sn: Zn: Mn alloy processed by aging prior to extrusion [J]. Journal of Magnesium and Alloys, 2019, 7(4): 637-647

[45]

Yu H-h, Xin Y-c, Wang M-y, et al.. Hall-petch relationship in Mg alloys: A review [J]. Journal of Materials Science & Technology, 2018, 34(2248-256

[46]

Yang Z-q, Ma A-b, Liu H, et al.. Managing strength and ductility in AZ91 magnesium alloy through ECAP combined with prior and post aging treatment [J]. Materials Characterization, 2019, 152: 213-222

[47]

Starink M J, Cheng X-y, Yang S-F. Hardening of pure metals by high-pressure torsion: A physically based model employing volume-averaged defect evolutions [J]. Acta Materialia, 2013, 61(1): 183-192

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