Microstructure and mechanical properties of aged Mg-Gd-Y-Zr-Ag alloy sheets processed by different rolling routes

Yu-ting Zhu , Han Chen , Zhi-yong Chen , Yu-xiang Han , Shu-nong Jiang , Yong-hao Gao , Ying-chun Wan , Chu-ming Liu

Journal of Central South University ›› 2025, Vol. 32 ›› Issue (8) : 2809 -2822.

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Journal of Central South University ›› 2025, Vol. 32 ›› Issue (8) : 2809 -2822. DOI: 10.1007/s11771-025-6039-7
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Microstructure and mechanical properties of aged Mg-Gd-Y-Zr-Ag alloy sheets processed by different rolling routes

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Abstract

Microstructure and mechanical properties of aged Mg-10Gd-2Y-0.4Zr-0.4Ag alloy sheets prepared by different rolling routes were investigated. The results showed that the cross rolling aged (CRA) sheet possesses larger grain size than unidirectional rolling aged (URA) sheet due to the occurrence of dynamic recovery during rolling which reduces the dislocation density and delays dynamic recrystallization (DRX). The URA sheet has basal texture and RD-favored texture while CRA sheet has multiple-peak texture. Both sheets precipitate β′ phase and CRA sheet exhibits a stronger aging response. The CRA sheet has higher yield strength and tensile strength than URA sheet, with reduced yield strength anisotropy but increased tensile strength anisotropy. Taking into account different strengthening mechanisms, although the finer grain size of URA sheet enhances grain boundary strengthening, CRA sheet is more responsive to aging, leading to superior aging-precipitated phase strengthening and consequently higher yield strength.

Keywords

Mg-Gd-Y-Zr-Ag alloy / rolling routes / aging precipitation / microstructure / strengthening mechanism

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Yu-ting Zhu, Han Chen, Zhi-yong Chen, Yu-xiang Han, Shu-nong Jiang, Yong-hao Gao, Ying-chun Wan, Chu-ming Liu. Microstructure and mechanical properties of aged Mg-Gd-Y-Zr-Ag alloy sheets processed by different rolling routes. Journal of Central South University, 2025, 32(8): 2809-2822 DOI:10.1007/s11771-025-6039-7

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References

[1]

PanC-j, LiuX-h, HongQ-x, et al.. Recent advances in surface endothelialization of the magnesium alloy stent materials [J]. Journal of Magnesium and Alloys, 2023, 11(1): 48-77.

[2]

WangG G, WeilerJ P. Recent developments in high-pressure die-cast magnesium alloys for automotive and future applications [J]. Journal of Magnesium and Alloys, 2023, 11(1): 78-87.

[3]

SongJ-f, ChenJ, XiongX-m, et al.. Research advances of magnesium and magnesium alloys worldwide in 2021 [J]. Journal of Magnesium and Alloys, 2022, 10(4): 863-898.

[4]

LiuH-x, LiC-x, XieJ-l, et al.. Effect of Sm content on microstructure and properties of extruded Mg-6Al-2Sr alloy [J]. Journal of Central South University, 2024, 31(1): 59-71.

[5]

TangJ-w, ChenL, BaoY-h, et al.. Investigation on corrosion behaviors of Mg-Zn-Al-Sn-Mn alloy treated by solution and artificial aging [J]. Journal of Central South University, 2023, 30(10): 3197-3210.

[6]

BiG-l, XuZ-c, JiangJ, et al.. High-speed impact behavior and microstructure evolution of anExtruded Mg-7Sn-5Zn-3Al alloy [J]. Journal of Materials Engineering and Performance, 2020, 29(10): 6427-6438.

[7]

TianA-q, XuX-h, SunL, et al.. Effects of interrupted ageing and asymmetric rolling on microstructures, mechanical properties, and intergranular corrosion behavior of Al-Mg-Si-Zn alloy [J]. Journal of Central South University, 2022, 29(3): 821-835.

[8]

WangK, WangX-w, DangC, et al.. Microstructure evolution and mechanical properties of high-strength Mg-Gd-Y-Zn-Mn alloy processed by asymmetric hot rolling [J]. Journal of Materials Research and Technology, 2023, 24: 2907-2917.

[9]

HanY-x, ChenS-y, WanY-c, et al.. Microstructure, texture evolution and mechanical anisotropy of Mg-Gd-Y-Zn-Zr alloy sheets produced by unidirectional and cross rolling [J]. Materials Science and Engineering A, 2024, 893146127.

[10]

TangW-q, HuangS-y, LiD-y, et al.. Mechanical anisotropy and deep drawing behaviors of AZ31 magnesium alloy sheets produced by unidirectional and cross rolling [J]. Journal of Materials Processing Technology, 2015, 215: 320-326.

[11]

LinX, ChenZ-y, ShaoJ-b, et al.. Deformation mechanism, orientation evolution and mechanical properties of annealed cross-rolled Mg-Zn-Zr-Y-Gd sheet during tension [J]. Journal of Magnesium and Alloys, 2023, 11(7): 2340-2350.

[12]

HuZ, ChenZ-y, XiongJ-y, et al.. Microstructure and mechanical properties of Mg-6.75%Zn-0.57%Zr-0.4%Y-0.18%Gd sheets by unidirectional and cross rolling [J]. Materials Science and Engineering A, 2016, 662: 519-527.

[13]

XieJ-s, ZhangJ-h, YouZ-h, et al.. Towards developing Mg alloys with simultaneously improved strength and corrosion resistance via RE alloying [J]. Journal of Magnesium and Alloys, 2021, 9(1): 41-56.

[14]

StanfordN, ShaG, XiaJ H, et al.. Solute segregation and texture modification in an extruded magnesium alloy containing gadolinium [J]. Scripta Materialia, 2011, 65(10): 919-921.

[15]

PangH, BaoJ, LiQ-a, et al.. Effect of Sm on microstructures and mechanical properties of Mg-Gd(-Sm) -Zr alloys by hot extrusion and aging treatment [J]. Journal of Materials Research and Technology, 2022, 19: 3877-3893.

[16]

ZhaoY, LiH, JingC-j, et al.. Improving tensile properties and corrosion resistance of Mg-Zn-Ca-Mn alloy via Gd addition [J]. Intermetallics, 2023, 162108000.

[17]

QinH, YangG-y, KanZ-y, et al.. Effect of substituting Gd with 3 wt% Nd on high temperature creep behaviors of peak-aged Mg-10Gd-0.4Zr casting Mg alloy [J]. Journal of Materials Research and Technology, 2023, 25: 5781-5794.

[18]

Jafari NodooshanH R, LiuW-c, WuG-h, et al.. Effect of Gd content on microstructure and mechanical properties of Mg-Gd-Y-Zr alloys under peak-aged condition [J]. Materials Science and Engineering A, 2014, 615: 79-86.

[19]

AnsariN, SarveshaR, LeeS Y, et al.. Influence of yttrium addition on recrystallization, texture and mechanical properties of binary Mg-Y alloys [J]. Materials Science and Engineering A, 2020, 793139856.

[20]

LeeY C, DahleA K, StjohnD H. The role of solute in grain refinement of magnesium [J]. Metallurgical and Materials Transactions A, 2000, 31(11): 2895-2906.

[21]

HuangC, LiuC-m, JiangS-n, et al.. Enhanced age-hardening response and mechanical properties of the Mg-Gd-Y-Zn-Zr alloy by trace Ag addition [J]. Journal of Alloys and Compounds, 2021, 874159825.

[22]

ZhangD-d, LiuC-m, JiangS-n, et al.. Effects of trace Ag on the dynamic recrystallization and mechanical properties of Mg-Gd-Y-Zr alloy [J]. Materials Science and Engineering A, 2023, 880145377.

[23]

WuL, LiY, ChenJ-w, et al.. Rare earth modified reduced graphene oxide reinforced AgCuTi composite brazing filler for brazing C/C composites [J]. Journal of Central South University, 2024, 31(5): 1398-1411.

[24]

LiZ-h, ZhangJ-h, XiaoT-x, et al.. Regulating microstructure and improving precipitation hardening response of fine-grained Mg-RE-Ag hot-extruded alloy by extreme short-time heat treatment [J]. Materials Science and Engineering A, 2024, 892146059.

[25]

ZhangY, ZhuY-m, RongW, et al.. On the precipitation in an Ag-containing Mg-Gd-Zr alloy [J]. Metallurgical and Materials Transactions A, 2018, 49(2): 673-694.

[26]

SunJ-p, XuB-q, YangZ-q, et al.. Achieving excellent ductility in high-strength Mg-10.6Gd-2Ag alloy via equal channel angular pressing [J]. Journal of Alloys and Compounds, 2020, 817152688.

[27]

ChenH, HanY-x, LiuC-m, et al.. Effect of unidirectional rolling and cross-rolling on microstructure and mechanical anisotropy of Mg-Gd-Y-Ag-Zr plates [J]. Journal of Alloys and Compounds, 2023, 960170680.

[28]

HussainM, RaoP N, SinghD, et al.. Insight to the evolution of nano precipitates by cryo rolling plus warm rolling and their effect on mechanical properties in Al6061 alloy [J]. Materials Science and Engineering A, 2021, 811141072.

[29]

KubinL P, MortensenA. Geometrically necessary dislocations and strain-gradient plasticity: A few critical issues [J]. Scripta Materialia, 2003, 48(2): 119-125.

[30]

LiX-q, RenL, LeQ-c, et al.. Reducing the yield asymmetry in Mg-5Li-3Al-2Zn alloy by hot-extrusion and multi-pass rolling [J]. Journal of Magnesium and Alloys, 2021, 9(3): 937-949.

[31]

QiX-x, LiY-x, XuX-y, et al.. Enhancing strength-ductility synergy in a Mg–Gd–Y–Zr alloy at sub-zero temperatures via high dislocation density and shearable precipitates [J]. Journal of Materials Science & Technology, 2023, 166: 123-132.

[32]

LiuH, GaoY, LiuJ Z, et al.. A simulation study of the shape of β′ precipitates in Mg-Y and Mg-Gd alloys [J]. Acta Materialia, 2013, 61(2): 453-466.

[33]

JinX-z, XuW-c, ShanD-b, et al.. Mechanism of high-strength and ductility of Mg-RE alloy fabricated by low-temperature extrusion and aging treatment [J]. Materials & Design, 2021, 199109384.

[34]

ShenJ-y, ZhangL-y, SunY, et al.. An exceptional ductility of AZ31 magnesium alloy sheet achieved by consecutive multi-pass cooperative lowered-temperature rolling [J]. Materials Science and Engineering A, 2022, 831142343.

[35]

WuW, WangL-f, HuangG-s, et al.. Effect of multi-pass continuous screw twist extrusion process on microstructure evolution, texture, and mechanical properties of AZ31 magnesium alloy [J]. Materials Today Communications, 2023, 34105508.

[36]

ShiB Q, ZhangR D, ShangX L, et al.. Reducing mechanical anisotropy by formation of symmetrical ring-like texture via final-pass heavy reduction rolling in Mg alloy [J]. Journal of Materials Research and Technology, 2023, 24: 4315-4328.

[37]

YaoY, LiuC-m, WanY-c, et al.. Microstructure, texture and mechanical anisotropy of Mg-Gd-Y-Zr sheets processed via different rolling routes and reductions [J]. Materials Characterization, 2020, 161110120.

[38]

YangZ-q, MaA-b, XuB-q, et al.. Development of a high-strength Mg-11Gd-2Ag (wt%) alloy sheet with extra-low anisotropy [J]. Materials Science and Engineering A, 2021, 811141084.

[39]

LuJ W, YinD D, HuangG H, et al.. Plastic anisotropy and deformation behavior of extruded Mg-Y sheets at elevated temperatures [J]. Materials Science and Engineering A, 2017, 700: 598-608.

[40]

ChiY Q, ZhengM Y, XuC, et al.. Effect of ageing treatment on the microstructure, texture and mechanical properties of extruded Mg-8.2Gd-3.8Y-1Zn-0.4Zr (wt%) alloy [J]. Materials Science and Engineering A, 2013, 565: 112-117.

[41]

XuC, ZhengM Y, WuK, et al.. Effect of ageing treatment on the precipitation behaviour of Mg-Gd-Y-Zn-Zr alloy [J]. Journal of Alloys and Compounds, 2013, 550: 50-56.

[42]

XuC, NakataT, QiaoX G, et al.. Ageing behavior of extruded Mg-8.2Gd-3.8Y-1.0Zn-0.4Zr (wt.%) alloy containing LPSO phase and γ′ precipitates [J]. Scientific Reports, 2017, 743391.

[43]

JiZ K, QiaoX G, HuC Y, et al.. Effect of aging treatment on the microstructure, fracture toughness and fracture behavior of the extruded Mg-7Gd-2Y-1Zn-0.5Zr alloy [J]. Materials Science and Engineering A, 2022, 849143514.

[44]

HuangK, MarthinsenK, ZhaoQ-l, et al.. The double-edge effect of second-phase particles on the recrystallization behaviour and associated mechanical properties of metallic materials [J]. Progress in Materials Science, 2018, 92: 284-359.

[45]

KwakT Y, KimW J. Mechanical properties and Hall-Petch relationship of the extruded Mg-Zn-Y alloys with different volume fractions of icosahedral phase [J]. Journal of Alloys and Compounds, 2019, 770: 589-599.

[46]

CuiX-f, FuW, FangD-q, et al.. Mechanical properties and deformation mechanisms of a novel finegrained Mg-Gd-Y-Ag-Zr-Ce alloy with high strength-ductility synergy [J]. Journal of Materials Science & Technology, 2021, 66: 64-73.

[47]

SomekawaH, OsawaY, SinghA, et al.. Effect of precipitate volume fraction on fracture toughness of extruded Mg-Zn alloys [J]. Journal of Materials Research, 2008, 23(4): 1128-1135.

[48]

WangF, DangN, ChenJ, et al.. The microstructural features and strengthening mechanisms of Mg-Al-Zn-Ca- (RE) extruded alloys having high-volume fractions of second-phase particles [J]. Materials Science and Engineering A, 2023, 868144765.

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