Weakened in-plane anisotropy of AZ31 magnesium alloy sheet induced by pre-enhanced non-basal slips during hot rolling

Chao-yang Yang , Li-fei Wang , Liang-liang Xue , Qiu-yan Huang , Da-biao Xia , Xin-wei Fu , Bo Song , Liu-wei Zheng , Hong-xia Wang , Seon-Shin Kwang

Journal of Central South University ›› 2025, Vol. 32 ›› Issue (3) : 706 -726.

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Journal of Central South University ›› 2025, Vol. 32 ›› Issue (3) : 706 -726. DOI: 10.1007/s11771-025-5856-z
Article

Weakened in-plane anisotropy of AZ31 magnesium alloy sheet induced by pre-enhanced non-basal slips during hot rolling

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Abstract

To weaken the basal texture and in-plane anisotropy of magnesium alloy, non-basal slips are pre-enhanced by pre-rolling with a single pass larger strain reduction at elevated temperatures. Then Mg alloy sheets with the thickness of 1 mm are achieved after five passes rolling at 300 °C. A double peak and disperse basal texture is generated after pre-rolling at higher temperatures when the non-basal slips are more active. So, the texture intensity of pre-rolled samples is reduced. Moreover, the distribution condition of in-grain misorientation axes (a method to analyze the activation of slips) shows that the pyramidal slip is quite active during deformation. After annealing on final rolled sheets, the texture distributions are changed and the intensity of texture reduces obviously due to static recrystallization. In particular, the r-value and in-plane anisotropy of pre-rolled samples are obviously lower than those of sample without pre-rolling.

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Chao-yang Yang, Li-fei Wang, Liang-liang Xue, Qiu-yan Huang, Da-biao Xia, Xin-wei Fu, Bo Song, Liu-wei Zheng, Hong-xia Wang, Seon-Shin Kwang. Weakened in-plane anisotropy of AZ31 magnesium alloy sheet induced by pre-enhanced non-basal slips during hot rolling. Journal of Central South University, 2025, 32(3): 706-726 DOI:10.1007/s11771-025-5856-z

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References

[1]

GaoJ-m, WangD, ZhuangD-d, et al.. Effect of laser power on microstructure and mechanical properties of laser heat conduction lap welded joint between AZ31B magnesium alloy and DP780 galvanized steel. Journal of Central South University, 2022, 29(10): 3463-3475 J]

[2]

YIN Y L, YU H L, WANG H M, et al. Tribological behaviors of AZ91D magnesium alloy under the lubrication of oil suspended synthetic magnesium silicate hydroxide nanotubes [J]. Journal of Magnesium and Alloys, 2024. DOI: https://doi.org/10.1016/j.jma.2024.01.007.

[3]

ChuC-l, WuX-q, QiuS-c, et al.. Microstructure and Gd-rich phase evolution of as-cast AZ31-xGd magnesium alloys during semi-solid isothermal heat treatment. Journal of Central South University, 2021, 28(1): 1-15 J]

[4]

JiY-f, DuanJ-r, YuanH, et al.. Effect of variable thickness cross rolling on edge crack and microstructure gradient of AZ31 magnesium alloy. Journal of Central South University, 2022, 29(4): 1124-1132 J]

[5]

ZhangY, JiangH-t, KangQ, et al.. Microstructure evolution and mechanical property of Mg-3Al alloys with addition of Ca and Gd during rolling and annealing process. Journal of Magnesium and Alloys, 2020, 8(3): 769-779 J]

[6]

ZhangW-c, LiuX-t, MaJ-f, et al.. Evolution of microstructure and mechanical properties of ZK60 magnesium alloy processed by asymmetric lowered-temperature rolling. Transactions of Nonferrous Metals Society of China, 2022, 32(9): 2877-2888 J]

[7]

OyinboS T, SinghanekaS, MatsumotoR. Exploring the basal/prismatic slip transfer at grain boundaries in magnesium: A molecular dynamic simulation. Vacuum, 2023, 212: 111995 J]

[8]

ZhangK, ShaoZ-t, RobsonJ, et al.. Achieving high ductility and strength in magnesium alloy through cryogenic-hot forming. Journal of Magnesium and Alloys, 2023, 11(9): 3130-3140 J]

[9]

XieZ-d, GuanY-j, YuX-h, et al.. Effects of ultrasonic vibration on performance and microstructure of AZ31 magnesium alloy under tensile deformation. Journal of Central South University, 2018, 25(7): 1545-1559 J]

[10]

ZhangW-c, LiuY-x, MaJ-f, et al.. Effects of bimodal basal texture on bending stress and microstructure evolution of Mg-2.6Nd-0.55Zn-0.5Zr alloys. Transactions of Nonferrous Metals Society of China, 2023, 33(3): 714-727 J]

[11]

ZhangD-d, LiuC-m, WanY-c, et al.. Microstructure and anisotropy of mechanical properties in ring rolled AZ80-Ag alloy. Journal of Central South University, 2021, 28(5): 1316-1323 J]

[12]

TianJ, LuH-h, ZhangW-g, et al.. An effective rolling process of magnesium alloys for suppressing edge cracks: Width-limited rolling. Journal of Magnesium and Alloys, 2022, 10(8): 2193-2207 J]

[13]

WangL-f, LiY-q, ZhangH, et al.. Review: Achieving enhanced plasticity of magnesium alloys below recrystallization temperature through various texture control methods. Journal of Materials Research and Technology, 2020, 9(6): 12604-12625 J]

[14]

RokhlinL L. The regularities in constitution of the ternary phase diagrams of magnesium alloys with two rare-earth metals belonging to different groups (yttrium group or cerium group). Journal of Phase Equilibria and Diffusion, 2020, 41(4): 532-537 J]

[15]

LiZ T, QiaoX G, XuC, et al.. Enhanced strength by precipitate modification in wrought Mg-Al-Ca alloy with trace Mn addition. Journal of Alloys and Compounds, 2020, 836: 154689 J]

[16]

NingF-k, LeQ-c, YanJ-s, et al.. Crimp feasibility of AZ31 magnesium alloy wide plate at warm temperatures responding to asymmetry. Journal of Magnesium and Alloys, 2022, 10(3): 797-810 J]

[17]

ShiD F, Cepeda-JiménezC M, Pérez-PradoM T. The relation between ductility at high temperature and solid solution in Mg alloys. Journal of Magnesium and Alloys, 2022, 10(1): 224-238 J]

[18]

WangW-k, ChenW-z, ZhangW-c, et al.. Weakened anisotropy of mechanical properties in rolled ZK60 magnesium alloy sheets with elevated deformation temperature. Journal of Materials Science & Technology, 2018, 34(11): 2042-2050 J]

[19]

WangL-f, PanX-h, ZhuX-x, et al.. Effect of two-step increased temperature thermal rolling on anisotropy and stretch formability of AZ31 magnesium alloy sheets. Transactions of Nonferrous Metals Society of China, 2023, 33(4): 1066-1085 J]

[20]

GongH, HeY-b, ZhangT, et al.. Modified constitutive behavior model of Mg-10Gd-3Y-0.4Zr alloy during high-temperature deformation process. Journal of Central South University, 2023, 30(8): 2458-2471 J]

[21]

HanL-y, YuY-n, WeiD-j, et al.. The synergistic and interactive effects of slip systems and dynamic recrystallization on the weakening basal texture of Mg-Y-Nd-Zr-Gd magnesium alloy. Materials & Design, 2024, 237: 112583 J]

[22]

WeiK, HuR, YinD-d, et al.. Grain size effect on tensile properties and slip systems of pure magnesium. Acta Materialia, 2021, 206: 116604 J]

[23]

ZhuY-z, HouD-w, LiQ-z. Quasi in situ EBSD analysis of twinning-detwinning and slip behaviors in textured AZ31 magnesium alloy subjected to compressivetensile loading. Journal of Magnesium and Alloys, 2022, 10(4): 956-964 J]

[24]

PanX-h, WangL-f, LuP-b, et al.. Unveiling the planar deformation mechanisms for improved formability in pre-twinned AZ31 Mg alloy sheet at warm temperature. Journal of Magnesium and Alloys, 2023, 11(12): 4659-4678 J]

[25]

SuhB C, KimJ H, BaeJ H, et al.. Effect of Sn addition on the microstructure and deformation behavior of Mg-3Al alloy. Acta Materialia, 2017, 124: 268-279 J]

[26]

WuW, WangL-f, HuangG-s, et al.. Effect of multi-pass continuous screw twist extrusion process on microstructure evolution, texture, and mechanical properties of AZ31 magnesium alloy. Materials Today Communications, 2023, 34: 105508 J]

[27]

MirzadehH. Grain refinement of magnesium alloys by dynamic recrystallization (DRX): A review. Journal of Materials Research and Technology, 2023, 25: 7050-7077 J]

[28]

LiZ-c, WuG-q, YuJ-m, et al.. Influence of strain rate on grain refinement and texture evolution under complex shear stress conditions. Journal of Magnesium and Alloys, 2023, 11(7): 2558-2584 J]

[29]

HuJ-l, WuX-j, BoH, et al.. Dislocation density model and microstructure of 7A85 aluminum alloy during thermal deformation. Journal of Central South University, 2021, 28(10): 2999-3007 J]

[30]

HaoM-j, ChengW-l, WangL-f, et al.. Texture evolution induced by twinning and dynamic recrystallization in dilute Mg-1Sn-1Zn-1Al alloy during hot compression. Journal of Magnesium and Alloys, 2020, 8(3): 899-909 J]

[31]

SunD, JiangS-y, ZhangY-q, et al.. Discontinuous dynamic recrystallization of TiNb alloys: Experiment and cellular automaton simulation. Journal of Central South University, 2023, 30(9): 2890-2905 J]

[32]

DuH-q, LiF, HuoP-d, et al.. Microstructure evolution and ductility improvement mechanisms of magnesium alloy in interactive alternating forward extrusion. Transactions of Nonferrous Metals Society of China, 2022, 32(8): 2557-2568 J]

[33]

LiangM-j, ZhengJ, LiuH, et al.. Microstructure and mechanical properties of AZ31 alloy prepared by cyclic expansion extrusion with asymmetrical extrusion cavity. Transactions of Nonferrous Metals Society of China, 2022, 32(1): 122-133 J]

[34]

LiH, ZengQ-h, YangP-f, et al.. Towards understanding twinning behavior near fracture surface in magnesium. Journal of Materials Science & Technology, 2020, 43: 230-237 J]

[35]

XieB-c, ZhangB-y, NingY-q, et al.. Mechanisms of DRX nucleation with grain boundary bulging and subgrain rotation during the hot working of nickel-based superalloys with columnar grains. Journal of Alloys and Compounds, 2019, 786: 636-647 J]

[36]

GuoP-c, LiuX, ZhuB-w, et al.. The microstructure evolution and deformation mechanism in a casting AM80 magnesium alloy under ultra-high strain rate loading. Journal of Magnesium and Alloys, 2022, 10(11): 3205-3216 J]

[37]

SongB, WangM, ShiR-l, et al.. Promoting hybrid twins structure to reduce yield asymmetry of rolled AZ31 plates by combining side-rolling and torsion. Journal of Magnesium and Alloys, 2023, 11(6): 2096-2105 J]

[38]

HuZ-q, GuoC-f, LiH-m. Influence of AZ31 sheet treated by cryogenic on punch shearing. Journal of Central South University, 2019, 26(6): 1582-1591 J]

[39]

ChapuisA, DriverJ H. Temperature dependency of slip and twinning in plane strain compressed magnesium single crystals. Acta Materialia, 2011, 59(5): 1986-1994 J]

[40]

LiuY-x, LiY-x, ZhuQ-c, et al.. Twin recrystallization mechanisms in a high strain rate compressed Mg-Zn alloy. Journal of Magnesium and Alloys, 2021, 9(2): 499-504 J]

[41]

YinG-m, FengZ-y, ZhaoZ-l, et al.. Microstructure and creep properties of Al/Mg/Al composite clad plates. Journal of Central South University, 2023, 30(9): 2867-2877 J]

[42]

LiuD, LiuZ-y, WangE. Improving single pass reduction during cold rolling by controlling initial texture of AZ31 magnesium alloy sheet. Transactions of Nonferrous Metals Society of China, 2018, 28(2): 244-250 J]

[43]

MalikA, WangY-w, NazeerF, et al.. Effect of pre-straining on twinning, texture and mechanical behavior of magnesium alloys A—Review. Journal of Materials Research and Technology, 2020, 9(6): 14478-14499 J]

[44]

SongD-h, ZhouT, TuJ, et al.. Improved stretch formability of AZ31 sheet via texture control by introducing a continuous bending channel into equal channel angular rolling. Journal of Materials Processing Technology, 2018, 259: 380-386 J]

[45]

GuoF, PeiR-s, JiangL-y, et al.. The role of recrystallization and grain growth in optimizing the sheet texture of magnesium alloys with calcium addition during annealing. Journal of Magnesium and Alloys, 2020, 8(1): 252-268 J]

[46]

HanX-z, HuL, JiaD-y, et al.. Role of unusual double-peak texture in significantly enhancing cold rolling formability of AZ31 magnesium alloy sheet. Transactions of Nonferrous Metals Society of China, 2023, 33(8): 2351-2364 J]

[47]

LiuB-s, XueL-k, LiR-g, et al.. Plasticity damage behavior caused by compression twins and double twins in rolled WE43 magnesium alloys. Materials Letters, 2023, 350: 134877 J]

[48]

ElsayedF R, SasakiT T, MendisC L, et al.. Compositional optimization of Mg-Sn-Al alloys for higher age hardening response. Materials Science and Engineering A, 2013, 566: 22-29 J]

[49]

NarayanJ. Recent progress in thin film epitaxy across the misfit scale (2011 Acta Gold Medal Paper). Acta Materialia, 2013, 61(8): 2703-2724 J]

[50]

WenK, LiX-w, XiongB-q, et al.. Influence of minor Sc additions on grain refinement and microstructure characteristics of a high Zn-containing Al-Zn-Mg-Cu-Zr alloy. Journal of Central South University, 2022, 29(3): 780-794 J]

[51]

GuiY-w, OuyangL-x, CuiY-j, et al.. Grain refinement and weak-textured structures based on the dynamic recrystallization of Mg-9.80Gd-3.78Y-1.12Sm-0.48Zr alloy. Journal of Magnesium and Alloys, 2021, 9(2): 456-466 J]

[52]

FanZ, GaoF, WangY, et al.. Grain refinement of Mg-alloys by native MgO particles: An overview. Journal of Magnesium and Alloys, 2022, 10(11): 2919-2945 J]

[53]

ShiB-d, YangC, PengY, et al.. Anisotropy of wrought magnesium alloys: A focused overview. Journal of Magnesium and Alloys, 2022, 10(6): 1476-1510 J]

[54]

PanX-h, WangL-f, XueL-l, et al.. Dynamic recrystallization, twinning behaviors and mechanical response of pre-twinned AZ31 Mg alloy sheet along various strain paths at warm temperature. Journal of Materials Research and Technology, 2022, 19: 1627-1649 J]

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