Mechanical properties of cemented coal gangue–flyash backfill under coupled effects of water pressure and chloride salt erosion

Zong-xu Li, Da-wei Yin, Hui-min Liu, Yi Tan, Xue-long Li

Journal of Central South University ›› 2024, Vol. 31 ›› Issue (5) : 1574-1591.

Journal of Central South University ›› 2024, Vol. 31 ›› Issue (5) : 1574-1591. DOI: 10.1007/s11771-024-5652-1
Article

Mechanical properties of cemented coal gangue–flyash backfill under coupled effects of water pressure and chloride salt erosion

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Abstract

In paste backfill mining, cemented coal gangue-flyash backfills (CGFB) can effectively control surface subsidence. CGFBs are subjected to water pressure and chloride ion erosion in the gob. Therefore, an improved understanding of the influence of pressurized water and chloride salt erosion on the performance of CGFB is crucial for realizing effective green mining. In this study, CGFB samples were soaked in a NaCl solution at 0, 0.5, 1.5, or 3.0 MPa for 15 d. The mechanical properties of the samples and deterioration mechanisms were investigated using uniaxial compression tests, acoustic emission tests, digital speckle strain measurements, scanning electron microscopy, and X-ray diffraction. The results show that the uniaxial compressive strength (UCS) increased and then decreased with the increase of soaking pressure. When the soaking pressure increased from 0 to 1.5 MPa, the average UCS increased by 43.5%. Then, when the soaking pressure increased from 1.5 to 3.0 MPa, the average UCS decreased by 18.9%. Moreover, water pressure promotes chloride ions into the interior of CGFB and the production of Friedel’s salt. Higher water pressures-chloride salt erosion coupling increases the porosity of CGFB, with the 3.0 MPa sample showing an 8.2% increase in porosity compared to the 0 MPa sample. Thus, internal pore cracks developed and penetrated the samples, which degraded their mechanical properties and reduced their strength and compactness.

Keywords

water pressure / chloride salt erosion / coal gangue-flyash backfill / localized deformation zone / acoustic emission signal / fracture morphology

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Zong-xu Li, Da-wei Yin, Hui-min Liu, Yi Tan, Xue-long Li. Mechanical properties of cemented coal gangue–flyash backfill under coupled effects of water pressure and chloride salt erosion. Journal of Central South University, 2024, 31(5): 1574‒1591 https://doi.org/10.1007/s11771-024-5652-1

References

[1]
ChenS-j, YinD-w, CaoF-w, et al. . An overview of integrated surface subsidence-reducing technology in mining areas of China. Natural Hazards, 2016, 81(2): 1129-1145 J]
CrossRef Google scholar
[2]
MaJ-b, YinD-w, JiangN, et al. . Application of a superposition model to evaluate surface asymmetric settlement in a mining area with thick bedrock and thin loose layer. Journal of Cleaner Production, 2021, 314: 128075 J]
CrossRef Google scholar
[3]
EkerH. Investigation of the usability of industrial mining wastes in agriculture. Frontiers in Environmental Science, 2023, 111248188 J]
CrossRef Google scholar
[4]
BeheraS K, MishraD P, SinghP, et al. . Utilization of mill tailings, fly ash and slag as mine paste backfill material: Review and future perspective. Construction and Building Materials, 2021, 309125120 J]
CrossRef Google scholar
[5]
YinD-w, ChenS-j, LiB, et al. . Bed separation backfill to reduce surface cracking due to mining under thick and hard conglomerate: A case study. Royal Society Open Science, 2019, 6(8): 190880 J]
CrossRef Google scholar
[6]
KrzysztofS. 3D numerical modelling of the application of cemented paste backfill on displacements around strip excavations. Energies, 2021, 14227750-7750 J]
CrossRef Google scholar
[7]
EkerH, BascetinA. The study of strength behaviour of zeolite in cemented paste backfill. Geomechanics and Engineering, 2022, 29(4): 421-434[J]
[8]
BeheraS, GhoshC, MishraD, et al. . Strength development and microstructural investigation of lead-zinc mill tailings based paste backfill with fly ash as alternative binder. Cement and Concrete Composites, 2020, 109103553 J]
CrossRef Google scholar
[9]
ThompsonB D, BawdenW F, GrabinskyM W. In situ measurements of cemented paste backfill at the Cayeli Minec. Canadian Geotechnical Journal, 2012, 49(7): 755-772 J]
CrossRef Google scholar
[10]
ChenS-m, XiangZ-g, EkerH. Curing stress influences the mechanical characteristics of cemented paste backfill and its damage constitutive model. Buildings, 2022, 12(10): 1607 J]
CrossRef Google scholar
[11]
GolikV, GabaraevO, KudryaA. Sublevel stoping with cemented paste backfill in weak rock mass zones. Journal of Mining Science, 2023, 5861002-1009 J]
CrossRef Google scholar
[12]
AliehS, AhmadJ, KhodadadiA. A review of additives used in the cemented paste tailings: Environmental aspects and application. Journal of Environmental Management, 2021, 289112501[J]
[13]
HelinskiM, FaheyM, FourieA. Behavior of cemented paste backfill in two mine stopes: Measurements and modeling. Journal of Geotechnical and Geoenvironmental Engineering, 2011, 137(2): 171-182 J]
CrossRef Google scholar
[14]
LibosI, CuiL. Time- and temperature-dependence of compressive and tensile behaviors of polypropylene fiber-reinforced cemented paste backfill. Frontiers of Structural and Civil Engineering, 2021, 15(4): 1025-1037 J]
CrossRef Google scholar
[15]
DalcéJ, LiL, YangP-yu. Experimental study of uniaxial compressive strength (UCS) distribution of hydraulic backfill associated with segregation. Minerals, 2019, 9(3): 147 J]
CrossRef Google scholar
[16]
ChakilamS, CuiLiang. Effect of polypropylene fiber content and fiber length on the saturated hydraulic conductivity of hydrating cemented paste backfill. Construction and Building Materials, 2020, 262120854 J]
CrossRef Google scholar
[17]
NIROSHAN N, SIVAKUGAN N, VEENSTRA L R. Laboratory study on strength development in cemented paste backfills [J]. Journal of Materials in Civil Engineering, 2017, 29(7). DOI: https://doi.org/10.1061/(ASCE)MT.1943-5533.0001848.
[18]
JafariM, GrabinskyM. Effect of hydration on failure surface evolution of low sulfide content cemented paste backfill. International Journal of Rock Mechanics and Mining Sciences, 2021, 144104749 J]
CrossRef Google scholar
[19]
MashifanaT, SitholeT. Clean production of sustainable backfill material from waste gold tailings and slag. Journal of Cleaner Production, 2021, 3082021127357 J]
CrossRef Google scholar
[20]
HefniM, AhmedH, OmarE S, et al. . The potential reuse of Saudi mine tailings in mine backfill: A path towards sustainable mining in Saudi Arabia. Sustainability, 2021, 13116204 J]
CrossRef Google scholar
[21]
KlemettiT, DykeV M, TuluI, et al. . A case study of the stability of a non-typical bleeder entry system at a U. S. longwall mine. International Journal of Mining Science and Technology, 2020, 30125-31 J]
CrossRef Google scholar
[22]
SilvisM J, HasenfusJ G, HainesM A. Bulking based porosity method to predict floodable volume of longwall gob. Mining, Metallurgy Exploration, 2021, 38(5): 1845-1859 J]
CrossRef Google scholar
[23]
MkadmiE N, AubertinM, LiL. Effect of drainage and sequential filling on the behavior of backfill in mine stopes. Canadian Geotechnical Journal, 2014, 51(1): 1-15 J]
CrossRef Google scholar
[24]
SunY-j, ZhangL, XuZ-m, et al. . Multi-field action mechanism and research progress of coal mine water quality formation and evolution. Journal of China Coal Society, 2022, 47(1): 423-437[J]
[25]
QIN Wei. Study on hydraulic connection and seepage law of goaf groups in coal mine underground reservoir [J]. Geofluids, 2022: 4316878. DOI: https://doi.org/10.1155/2022/4316878.
[26]
ChenS-j, DuZ-w, ZhangZ, et al. . Effects of chloride on the early mechanical properties and microstructure of gangue-cemented paste backfill. Construction and Building Materials, 2020, 235117504 J]
CrossRef Google scholar
[27]
DuZ-w, ChenS-j, YinD-w, et al. . Experimental study of stability of paste backfill under chloride erosion environment. Journal of China University of Mining & Technology, 2021, 50(3): 532-538[J]
[28]
OuyangS-y, HuangY-l, WuL-w, et al. . Effects of chlorides on setting time, hydration heat and hydration products of fresh slurry of cemented paste backfill. Case Studies in Construction Materials, 2022, 17e01462 J]
CrossRef Google scholar
[29]
WangS, WangF, YinD-w, et al. . Experimental study on mechanical properties of paste backfill with flue-gas desulphurisation gypsum under combined action of dry-wet cycles and chloride erosion. Minerals, 2021, 11(8): 882 J]
CrossRef Google scholar
[30]
FenauxM, ReyesE, GálvezJ, et al. . Modelling the transport of chloride and other ions in cement-based materials. Cement and Concrete Composites, 2019, 9733-42 J]
CrossRef Google scholar
[31]
CostaD A, FenauxM, FernándezJ, et al. . Modelling of chloride penetration into non-saturated concrete: Case study application for real marine offshore structures. Construction and Building Materials, 2013, 43217-224 J]
CrossRef Google scholar
[32]
BernalJ, FenauxM, MoraguesA, et al. . Study of chloride penetration in concretes exposed to high-mountain weather conditions with presence of deicing salts. Construction and Building Materials, 2016, 127: 971-983 J]
CrossRef Google scholar
[33]
TranB, PhamD, LocM, et al. . An adaptive approach for the chloride diffusivity of cement-based materials. Computers and Concrete, 2019, 23(2): 145-153[J]
[34]
XuG-z, fanK-g, WangK, et al. . Paste backfill corrosion mechanisms in chloride and sulfate environments. Minerals, 2022, 12(5): 551 J]
CrossRef Google scholar
[35]
WangP-g, MoR, LiS, et al. . A chemo-damage-transport model for chloride ions diffusion in cement-based materials: Combined effects of sulfate attack and temperature. Construction and Building Materials, 2021, 288: 123121 J]
CrossRef Google scholar
[36]
SHI Cai-jun, YUAN Qiang, HE Fu-qiang, et al. Transport and interactions of chlorides in cement-based materials [M]. CRC Press, 2019. (in Chinese)
[37]
WangX-g, ShiC-j, HeF-q, et al. . Chloride binding and its effects on microstructure of cement-based materials. Journal of the Chinese Ceramic Society, 2013, 412187-198[J]
[38]
YoonI, NamJ. New experiment recipe for chloride penetration in concreteunder water pressure. Computers and Concrete, 2016, 17(2): 189-199 J]
CrossRef Google scholar
[39]
OuY-l, XuM-j, ChenD-q, et al. . Effect of reverse water pressure on chloride penetration within finite concrete during drying-wetting cycles. Ocean Engineering, 2022, 257111606 J]
CrossRef Google scholar
[40]
XiaoL-f, ChenD-q, JiangM-j, et al. . Experimental and numerical analysis of chloride transport in finite concrete under reverse water pressure. Construction and Building Materials, 2021, 304124576 J]
CrossRef Google scholar
[41]
MaZ-m, ZhaoT-j, ZhaoY-di. Effects of hydrostatic pressure on chloride ion penetration into concrete. Magazine of Concrete Research, 2016, 68(17): 877-886 J]
CrossRef Google scholar
[42]
FuQ, BuM-x, ZhangZ-r, et al. . Chloride ion transport performance of lining concrete under coupling the action of flowing groundwater and loading. Cement and Concrete Composites, 2021, 123104166 J]
CrossRef Google scholar
[43]
LiZ-x, YinD-w, JiangN, et al. . Deformation and failure characteristics of bimaterial samples consisting of sandstone and cemented coal gangue – fly ash backfill under uniaxial loading. Minerals, 2022, 12(12): 1546-1546 J]
CrossRef Google scholar
[44]
YIN Da-wei, DING Yi-song, JIANG Ning, et al. Mechanical properties and damage characteristics of coal samples under water immersion pressure [J]. Lithosphere, 2022(1): 1278783. DOI: https://doi.org/10.2113/2022/1278783.
[45]
LiF-x, YinD-w, ZhuC, et al. . Effects of kaolin addition on mechanical properties for cemented coal gangue-fly ash backfill under uniaxial loading. Energies, 2021, 14(12): 3693-3693 J]
CrossRef Google scholar
[46]
LiP, SunJ-l, CaiM-f, et al. . Acoustic emission behavior of rock materials containing two preexisting flaws and an opening subjected to uniaxial compression: insights into self-similarity, chaotic, and fractal features. Journal of Materials Research and Technology, 2022, 201786-1801 J]
CrossRef Google scholar
[47]
YinD-w, ChenS-j, GeY, et al. . Mechanical properties of rock-coal bi-material samples with different lithologies under uniaxial loading. Journal of Materials Research and Technology, 2021, 10: 322-338 J]
CrossRef Google scholar
[48]
YinD-w, ChenS-j, SunX, et al. . Effects of interface angles on properties of rock-cemented coal gangue-fly ash backfill bi-materials. Geomechanics and Engineering, 2021, 24(1): 81-89[J]
[49]
JiangN, LvK, GaoZ-y, et al. . Experimental study on mechanical properties of single fracture-hole red sandstone. Frontiers in Earth Science, 2023, 10: 1083689 J]
CrossRef Google scholar
[50]
WuJ-n, YangX-b, SongY-m, et al. . Study on a new inversion method for non-uniform distribution of rock material parameters. Bulletin of Engineering Geology and the Environment, 2022, 81(7): 280 J]
CrossRef Google scholar
[51]
GuG H, AhnS Y, KimY, et al. . Determining reliable wide-strain-range equivalent stress-strain curves using 3D digital image correlation. Journal of Materials Research and Technology, 2022, 192822-2830 J]
CrossRef Google scholar
[52]
LiF-x, YinD-w, WangF, et al. . Effects of combination mode on mechanical properties of bi-material samples consisting of rock and coal. Journal of Materials Research and Technology, 2022, 192156-2170 J]
CrossRef Google scholar
[53]
LiX-l, ChenS-j, LiuS-m, et al. . AE waveform characteristics of rock mass under uniaxial loading based on hilbert-huang transform. Journal of Central South University, 2021, 28(6): 1843-1856 J]
CrossRef Google scholar
[54]
YinD-w, WangF, ZhangJ-c, et al. . Experimental study on the short-term uniaxial creep characteristics of sandstone-coal composite samples. Minerals, 2021, 11(12): 1398 J]
CrossRef Google scholar
[55]
LiuC, ShiB, ZhouJ, et al. . Quantification and characterization of microporosity by image processing, geometric measurement and statistical methods: Application on SEM images of clay materials. Applied Clay Science, 2011, 54197-106 J]
CrossRef Google scholar
[56]
YooJ H, LeeH S, IsmailM A. An analytical study on the water penetration and diffusion into concrete under water pressure. Construction and Building Materials, 2010, 25(1): 99-108 J]
CrossRef Google scholar
[57]
LiC-b, MaB-g, TanH-b, et al. . Effect of triisopropanolamine on chloride binding of cement paste with ground-granulated blast furnace slag. Construction and Building Materials, 2020, 256: 119494 J]
CrossRef Google scholar
[58]
YaziciH, DenizE, BaradanB. The effect of autoclave pressure, temperature and duration time on mechanical properties of reactive powder concrete. Construction and Building Materials, 2013, 4253-63 J]
CrossRef Google scholar
[59]
MustaphaE J, ZhengJ, LiLi. Experimental study of the evolution of pore water pressure and total stresses during and after the deposition of slurried backfill. Geomechanics and Engineering, 2021, 26(5): 499-512[J]
[60]
changhyuckL, GyuyongK, GyeongtaeK, et al. . Evaluation of chloride-ion diffusion characteristics of wave power marine concrete structures. Materials, 2021, 14(19): 5675-5675 J]
CrossRef Google scholar
[61]
AhmadH, RezaK, HocineS, et al. . Investigation of leakage and self-healing of direct tension cracks under sustained loading and high-water pressure. Construction and Building Materials, 2020, 267120879[J]

Foundation item: Projects(52274128, 51904167, 52174159) supported by the National Natural Science Foundation of China; Project supported by the Taishan Scholars Project Special Fund of Shandong Province, China; Project(KCF2204) supported by the Open Fund for the Henan Key Laboratory for Green and Efficient Mining & Comprehensive Utilization of Mineral Resources, China; Project(22KF01) supported by the Open Fund for the State Key Laboratory of Mining Response and Disaster Prevention and Control in Deep Coal Mines, China

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