Experimental investigation on mechanical behaviors and microstructure responses of the coking coal subjected to freeze-thaw cycles

Hong-fa Ma , Yan-qi Song , Jun-jie Zheng , Zhi-xin Shao , Fu-xin Shen , Chuan-peng Liu , Da-wei Yin

Journal of Central South University ›› 2023, Vol. 30 ›› Issue (8) : 2701 -2725.

PDF
Journal of Central South University ›› 2023, Vol. 30 ›› Issue (8) : 2701 -2725. DOI: 10.1007/s11771-023-5408-3
Article

Experimental investigation on mechanical behaviors and microstructure responses of the coking coal subjected to freeze-thaw cycles

Author information +
History +
PDF

Abstract

In this paper, the uniaxial compression test of coking coal with different freeze-thaw (F-T) cycles was carried out, accompanied by the monitoring of the acoustic emission (AE) system and digital image correlation (DIC) system. The results show that with the increase of F-T cycles, there is the continuous increase and obvious development of the sample mass and the pore structure respectively, causing the deterioration of mechanical properties. In addition, the AE activity of the samples gradually increased, which is more obvious in the compaction stage; furtherly, the tensile microcracks in the rock during the compression test always account for a larger proportion (except for 30 F-T cycles). For the failure characteristics, the rock sample changes from splitting tensile failure to shear failure, and the fracture surface morphology changes from rough to smooth. The damage constitutive model of coking coal subjected to the F-T effect and axial load was established, which is in good agreement with the experiment results. Finally, it is found that the initial damage of coking coal subjected to F-T cycles could be attributable to the expansion of pore and fissure space caused by the freeze of free water, the increasingly enhanced water-rock interaction and the interaction between mineral particles.

Keywords

coking coal / freeze-thaw effect / acoustic emission / microstructure / mechanical behaviors / damage constitutive model / damage mechanism

Cite this article

Download citation ▾
Hong-fa Ma, Yan-qi Song, Jun-jie Zheng, Zhi-xin Shao, Fu-xin Shen, Chuan-peng Liu, Da-wei Yin. Experimental investigation on mechanical behaviors and microstructure responses of the coking coal subjected to freeze-thaw cycles. Journal of Central South University, 2023, 30(8): 2701-2725 DOI:10.1007/s11771-023-5408-3

登录浏览全文

4963

注册一个新账户 忘记密码

References

[1]

CaiC, GaoF, LiG, et al. . Evaluation of coal damage and cracking characteristics due to liquid nitrogen cooling on the basis of the energy evolution laws [J]. Journal of Natural Gas Science and Engineering, 2016, 29: 30-36

[2]

LiB, LinH, LiS, et al. . Exploration of pore structure evolution and damage mechanism of coal under liquid nitrogen freeze-thaw cycles [J]. Fuel, 2022, 325: 124875

[3]

ZhaiC, WuS, LiuS, et al. . Experimental study on coal pore structure deterioration under freeze-thaw cycles [J]. Environmental Earth Sciences, 2017, 76(15): 507

[4]

QinL, ZhaiC, LiuS, et al. . Factors controlling the mechanical properties degradation and permeability of coal subjected to liquid nitrogen freeze-thaw [J]. Scientific Reports, 2017, 73675

[5]

ChuY, ZhangD, WangM, et al. . Experiment study on influence of liquid nitrogen freeze-thaw on pore structure of coal based on nuclear magnetic resonance technology and mercury intrusion methods [J]. Chinese Journal of Rock Mechanics and Engineering, 2022, 4191820-1831(in Chinese)

[6]

LiangY. Key technique of safe mining in low permeability and methane-rich seam group [J]. Chinese Journal of Rock Mechanics and Engineering, 2008, 27(7): 1370-1379(in Chinese)

[7]

QinL, ZhaiC, LiuS, et al. . Infrared thermal image and heat transfer characteristics of coal injected with liquid nitrogen under triaxial loading for coalbed methane recovery [J]. International Journal of Heat and Mass Transfer, 2018, 1181231-1242

[8]

SuS, GaoF, CaiC, et al. . Experimental study on coal permeability and cracking characteristics under LN2 freeze-thaw cycles [J]. Journal of Natural Gas Science and Engineering, 2020, 83: 103526

[9]

McdanielB W, GrundmannS R, KendrickW D, et al. . Field applications of cryogenic nitrogen as a hydraulic-fracturing fluid [C]. 1997 SPE Annual Technical Conference and Exhibition, 1997, San Antonio, Texas, SPE: 38-3950

[10]

QiaoC, SongZ, WangY, et al. . Fractures and acoustic emission features of non-persistent jointed rocks subjected to freeze-thaw-compression load: Experimental insights [J]. Rock Mechanics and Rock Engineering, 2022, 55(1): 109-123

[11]

SongY, MaH, LiuJ, et al. . Experimental investigation on the damage characteristics of freeze-thaw limestone by the uniaxial compression and acoustic emission monitoring tests [J]. Chinese Journal of Rock Mechanics and Engineering, 2022, 41(S1): 2603-2614(in Chinese)

[12]

WangY, SongZ, MaoT, et al. . Macro-meso fracture and instability behaviors of hollow-cylinder granite containing fissures subjected to freeze-thaw-fatigue loads [J]. Rock Mechanics and Rock Engineering, 2022, 55(7): 4051-4071

[13]

QiaoC, LiC, WangY, et al. . Experimental study on failure of central rock bridge under freeze-thaw cycle [J]. Chinese Journal of Rock Mechanics and Engineering, 2020, 39(06): 1094-1103(in Chinese)

[14]

MaH, SongY, YangJ, et al. . Experimental investigation on physical-mechanical behaviors and macro-micro-structural responses of lignite subjected to freeze-thaw cycles [J]. Natural Resources Research, 2023, 32(2): 543-566

[15]

MomeniA, AbdilorY, KhanlariG R, et al. . The effect of freeze-thaw cycles on physical and mechanical properties of granitoid hard rocks [J]. Bulletin of Engineering Geology and the Environment, 2016, 75(4): 1649-1656

[16]

KhanlariG, SahamiehR Z, AbdilorY. The effect of freeze-thaw cycles on physical and mechanical properties of Upper Red Formation sandstones, central part of Iran [J]. Arabian Journal of Geosciences, 2015, 8(8): 5991-6001

[17]

HuangS, LiuQ, ChengA, et al. . A fully coupled thermo-hydro-mechanical model including the determination of coupling parameters for freezing rock [J]. International Journal of Rock Mechanics and Mining Sciences, 2018, 103: 205-214

[18]

ZhouJ, TangY. Experimental inference on dual-porosity aggravation of soft clay after freeze-thaw by fractal and probability analysis [J]. Cold Regions Science and Technology, 2018, 153: 181-196

[19]

AbdolghanizadehK, HosseiniM, SaghafiyazdiM. Effect of freezing temperature and number of freeze-thaw cycles on mode I and mode II fracture toughness of sandstone [J]. Theoretical and Applied Fracture Mechanics, 2020, 105: 102428

[20]

HuangS, HeY, YuS, et al. . Experimental investigation and prediction model for UCS loss of unsaturated sandstones under freeze-thaw action [J]. International Journal of Mining Science and Technology, 2022, 32(1): 41-49

[21]

LiuY, CaiY, HuangS, et al. . Effect of water saturation on uniaxial compressive strength and damage degree of clay-bearing sandstone under freeze-thaw [J]. Bulletin of Engineering Geology and the Environment, 2020, 79(4): 2021-2036

[22]

DeprezM, DeK T, DeS G, et al. . A review on freeze-thaw action and weathering of rocks [J]. Earth-Science Reviews, 2020, 203103143

[23]

NiuC, ZhuZ, ZhouL, et al. . Study on the microscopic damage evolution and dynamic fracture properties of sandstone under freeze-thaw cycles [J]. Cold Regions Science and Technology, 2021, 191103328

[24]

WangY, ZhangB, LiB, et al. . A strain-based fatigue damage model for naturally fractured marble subjected to freeze-thaw and uniaxial cyclic loads [J]. International Journal of Damage Mechanics, 2021, 30(10): 1594-1616

[25]

WangY, ZhangB, GaoS H, et al. . Investigation on the effect of freeze-thaw on fracture mode classification in marble subjected to multi-level cyclic loads [J]. Theoretical and Applied Fracture Mechanics, 2021, 111102847

[26]

LiJ, ZhouK, LiuW, et al. . NMR research on deterioration characteristics of microscopic structure of sandstones in freeze-thaw cycles [J]. Transactions of Nonferrous Metals Society of China, 2016, 26(11): 2997-3003

[27]

ParkJ, HyunC U, ParkH D. Changes in microstructure and physical properties of rocks caused by artificial freeze-thaw action [J]. Bulletin of Engineering Geology and the Environment, 2015, 74(2): 555-565

[28]

Seyed MousaviS Z, TavakoliH, MoarefvandP, et al. . Assessing the effect of freezing-thawing cycles on the results of the triaxial compressive strength test for calc-schist rock [J]. International Journal of Rock Mechanics and Mining Sciences, 2019, 123104090

[29]

ZhangH, MengX, YangG. A study on mechanical properties and damage model of rock subjected to freeze-thaw cycles and confining pressure [J]. Cold Regions Science and Technology, 2020, 174103056

[30]

WalbertC, EslamiJ, BeaucourA L, et al. . Evolution of the mechanical behaviour of limestone subjected to freeze-thaw cycles [J]. Environmental Earth Sciences, 2015, 74(7): 6339-6351

[31]

HanT, ShiJ, CaoX. Fracturing and damage to sandstone under coupling effects of chemical corrosion and freeze-thaw cycles [J]. Rock Mechanics and Rock Engineering, 2016, 49(11): 4245-4255

[32]

DengH, YuS, DengJ, et al. . Experimental investigation on energy mechanism of freezing-thawing treated sandstone under uniaxial static compression [J]. KSCE Journal of Civil Engineering, 2019, 23(5): 2074-2082

[33]

LuY, LiX, ChanA. Damage constitutive model of single flaw sandstone under freeze-thaw and load [J]. Cold Regions Science and Technology, 2019, 15920-28

[34]

ZhengH, FengX, ChenZ, et al. . ISRM suggested method for reporting rock laboratory test data in electronic format [J]. Rock Mechanics and Rock Engineering, 2014, 47(1): 221-254

[35]

NicholsonD T, NicholsonF H. Physical deterioration of sedimentary rocks subjected to experimental freeze-thaw weathering [J]. Earth Surface Processes and Landforms, 2000, 25(12): 1295-1307

[36]

MaH, ChenS, SongY, et al. . Experimental investigation into the effects of composition and microstructure on the tensile properties and failure characteristics of different gypsum rocks [J]. Scientific Reports, 2021, 11: 14517

[37]

MaQ, MaD, YaoZ. Influence of freeze-thaw cycles on dynamic compressive strength and energy distribution of soft rock specimen [J]. Cold Regions Science and Technology, 2018, 15310-17

[38]

LiuQ. Analysis of mechanism of rock failure due to freeze-thaw cycling and mechanical testing study on frozen-thawed rocks [J]. Chinese Journal of Rock Mechanics and Engineering, 2005, 24(17): 3076-3082(in Chinese)

[39]

MaH, SongY, ChenS, et al. . Experimental investigation on the mechanical behavior and damage evolution mechanism of water-immersed gypsum rock [J]. Rock Mechanics and Rock Engineering, 2021, 54(9): 4929-4948

[40]

DuK, LiX, TaoM, et al. . Experimental study on acoustic emission (AE) characteristics and crack classification during rock fracture in several basic lab tests [J]. International Journal of Rock Mechanics and Mining Sciences, 2020, 133104411

[41]

LiX, ChenS, LiuS, et al. . AE waveform characteristics of rock mass under uniaxial loading based on Hilbert-Huang transform [J]. Journal of Central South University, 2021, 28(6): 1843-1856

[42]

LiuX, HanM, HeW, et al. . A new b value estimation method in rock acoustic emission testing [J]. Journal of Geophysical Research: Solid Earth, 2020, 125(12): e2020JB019658

[43]

ChenS, YinD, JiangN, et al. . Mechanical properties of oil shale-coal composite samples [J]. International Journal of Rock Mechanics and Mining Sciences, 2019, 123104120

[44]

GanY, WuS, RenY, et al. . Evaluation indexes of granite splitting failure based on RA and AF of AE parameters [J]. Chinese Journal of Rock and Soil Mechanics, 2020, 4172324-2332(in Chinese)

[45]

SouliotiD, BarkoulaN M, PaipetisA, et al. . Acoustic emission behavior of steel fibre reinforced concrete under bending [J]. Construction and Building Materials, 2009, 23(12): 3532-3536

[46]

OhnoK, OhtsuM. Crack classification in concrete based on acoustic emission [J]. Construction and Building Materials, 2010, 24(12): 2339-2346

[47]

GutenbergB, RichterC F. Magnitude and energy of earthquakes [J]. Nature, 1955, 176(4486): 795

[48]

FuB, ZhouZ, WangH, et al. . Precursor information study on acoustic emission characteristics of marble under uniaxial cyclic loading-unloading [J]. Journal of China Coal Society, 2016, 4181946-1953(in Chinese)

[49]

ChenS, YinD, JiangN, et al. . Simulation study on effects of loading rate on uniaxial compression failure of composite rock-coal layer [J]. Geomechanics and Engineering, 2019, 17(4): 333-342(in Chinese)

[50]

ChenS, DuZ, ZhangZ, et al. . Effects of chloride on the early mechanical properties and microstructure of gangue-cemented paste backfill [J]. Construction and Building Materials, 2020, 235117504

[51]

ZhouH W, LiuZ L, ZhongJ C, et al. . NMRI online observation of coal fracture and pore structure evolution under confining pressure and axial compressive loads: A novel approach [J]. Energy, 2022, 261125297

[52]

XiaoP, LiD, ZhaoG, et al. . Mechanical properties and failure behavior of rock with different flaw inclinations under coupled static and dynamic loads [J]. Journal of Central South University, 2020, 27(10): 2945-2958

[53]

GaoM, ZhangJ, LiS, et al. . Calculating changes in fractal dimension of surface cracks to quantify how the dynamic loading rate affects rock failure in deep mining [J]. Journal of Central South University, 2020, 27(10): 3013-3024

[54]

HaimsonB, ChangC. A new true triaxial cell for testing mechanical properties of rock, and its use to determine rock strength and deformability of Westerly granite [J]. International Journal of Rock Mechanics and Mining Sciences, 2000, 37(1–2): 285-296

[55]

FanZ, XieH, RenL, et al. . Anisotropy in shear-sliding fracture behavior of layered shale under different normal stress conditions [J]. Journal of Central South University, 2022, 29(11): 3678-3694

[56]

YanJ. Experimental research on mechanical properties of deep marble under different initial damage levels and unloading paths [J]. Chinese Journal of Rock Mechanics and Engineering, 2012, 31(8): 1686-1697(in Chinese)

[57]

BianK, LiuJ, ZhangW, et al. . Mechanical behavior and damage constitutive model of rock subjected to water-weakening effect and uniaxial loading [J]. Rock Mechanics and Rock Engineering, 2019, 52(1): 97-106

[58]

XiaoP, ChenY, DuX, et al. . Study on the mechanical properties of sandstone under freeze-thaw cycles and study of Meso-damage constitutive model [J]. Chinese Journal of Geotechnical Engineering, 2023, 45(4): 805-815(in Chinese)

[59]

YinD, XuQ. Investigating the damage evolution of sandstone using electrical impedance spectroscopy [J]. International Journal of Rock Mechanics and Mining Sciences, 2021, 144104817

[60]

WeibullW. A statistical distribution function of wide applicability [J]. Journal of Applied Mechanics, 1951, 18(3): 293-297

AI Summary AI Mindmap
PDF

202

Accesses

0

Citation

Detail

Sections
Recommended

AI思维导图

/