Microstructure and texture evolutions of 310S austenitic stainless steel after cryogenic rolling and subsequent annealing: X-ray and electron backscatter diffraction studies

Abstract

The present work aims to study the microstructure and texture evolutions of thermomechanically processed 310S austenitic stainless steel. The material was cryo-rolled at 20%, 50% and 90% thickness reduction, followed by annealing at 1023, 1223 and 1323 K for 5, 15 and 30 min, respectively. After a 20% thickness reduction, strain-induced α′-martensite was seen along with deformation twinning within the austenite grains. The volume fraction of the deformation twinning was higher than that of α′-martensite. By increasing deformation from 50% to 90%, the volume fraction of α′-martensite went from 11% to 69%, and twinning was replaced by martensite. Brass, Goss, and S components were the dominant textures in the austenite phase after deformation, while the main texture components in α′-martensite were R-Cu, R-cube, F, and E. Brass component was further increased by increasing the thickness reduction in contrast to the Goss component. During annealing, martensite to austenite reversion and recrystallization occurred in the deformed austenite, which resulted in an increase in the volume fractions of the Goss and Brass recrystallization components. However, the annealing texture of the alloy was found to be approximately the same as the cryo-rolling texture. The kinetics of martensite reversion at 1223 K for 5 min was much faster than that at 1023 K. An equiaxed microstructure was not detected at 1023 K for 5 min due to incomplete martensite reversion and primary recrystallization. The optimum annealing temperature for obtaining an ultrafine grain structure was 1023 K for 15 min. Recrystallization and tangible grain growth swiftly occurred at 1173 K and 1273 K.

Keywords

310S stainless steel / deformation / annealing / electron backscattered diffraction / microstructure / texture

References

[1] YeganehM, Khosravi-BigdeliI, EskandariM, et al. . Corrosion inhibition of l-methionine amino acid as a green corrosion inhibitor for stainless steel in the H₂SO₄ solution [J]. Journal of Materials Engineering and Performance, 2020, 29(6): 3983-3994

[2] EskandariM, Mohtadi-BonabM A, YeganehM, et al. . High-strain-rate deformation behaviour of new high-Mn austenitic steel during impact shock-loading [J]. Materials Science and Technology, 2019, 35(1): 77-88

[3] MoghadasS M J, YeganehM, ZareeS R A, et al. . Influence of low temperature heat treatment on microstructure, corrosion resistance and biological performance of 316L stainless steel manufactured by selective laser melting [J]. CIRP Journal of Manufacturing Science and Technology, 2023, 40: 68-74

[4] SalehiM, YeganehM, HeidariR B, et al. . Comparison of the microstructure, corrosion resistance, and hardness of 321 and 310S austenitic stainless steels after thermo-mechanical processing [J]. Materials Today Communications, 2022, 31: 103638

[5] GOYAL A, KAPOOR H, JAYAHARI L, et al. Experimental investigation to analyze the mechanical and microstructure properties of 310SS performed by TIG welding [J]. Advances in Materials Science and Engineering, 2022: 1–11. DOI: https://doi.org/10.1155/2022/1231843.

[6] LiuZ, LuJ-q, SuH-z, et al. . On the role of mechanical deformation in the environmental degradation of 310S stainless steels in supercritical carbon dioxide [J]. Corrosion Science, 2022, 207110537

[7] SunH-y, SunY-d, ZhangR-q, et al. . Study on hot workability and optimization of process parameters of a modified 310 austenitic stainless steel using processing maps [J]. Materials & Design, 2015, 67165-172

[8] CHRISTIAN J, GIRTON L D, GRUNER J. The effects of cold rolling on the mechanical properties of type 310 stainless steel at room and cryogenic temperatures [J]. Characterization of Minerals, Metals, and Materials, 1962: 127–133.

[9] LebanM B, VončinaM, KosecT, et al. . Comparison of cycling high temperature corrosion at 650 °C in the presence of NaCl of various austenitic stainless steels [J]. High Temperature Corrosion of Materials, 2023, 99(1): 63-77

[10] SomaniM C, JuntunenP, KarjalainenL P, et al. . Enhanced mechanical properties through reversion in metastable austenitic stainless steels [J]. Metallurgical and Materials Transactions A, 2009, 40(3): 729-744

[11] ChowdhuryS G, SahuP, MahatoB, et al. HaldarA, SuwasS, BhattacharjeeD, et al. . Evolution of recrystallization texture in AISI300 series austenitic stainless steels after cold rolling to large strain [C]. Microstructure and Texture in Steels, 2009, London, Springer: 361378

[12] YilmazS O, TekerT, BatmazY O, et al. . Effect of thermomechanical processing on the mechanical properties of CuZn10 alloy [J]. Materials Testing, 2022, 64(7): 1026-1032

[13] ShakhovaI, DudkoV, BelyakovA, et al. . Effect of large strain cold rolling and subsequent annealing on microstructure and mechanical properties of an austenitic stainless steel [J]. Materials Science and Engineering A, 2012, 545: 176-186

[14] LeeJ C, NohY, KimN S, et al. . Effect of texture and temperature on strain-induced martensitic transformation in 304 austenitic stainless steel [J]. Steel Research International, 2023, 94(2): 2200243

[15] PunL, SoaresG C, IsakovM, et al. . Effects of strain rate on strain-induced martensite nucleation and growth in 301LN metastable austenitic steel [J]. Materials Science and Engineering A, 2022, 831: 142218

[16] XuD-m, WanX-l, YuJ-x, et al. . Effect of cold deformation on microstructures and mechanical properties of austenitic stainless steel [J]. Metals, 2018, 87522

[17] GhoshS K, MallickP, ChattopadhyayP P. Effect of reversion of strain induced martensite on microstructure and mechanical properties in an austenitic stainless steel [J]. Journal of Materials Science, 2011, 46103480-3487

[18] diS A, BarteriM, KennyJ M. Effects of grain size on the properties of a low nickel austenitic stainless steel [J]. Journal of Materials Science, 2003, 38(23): 4725-4733

[19] EskandariM, YeganehM, MotamediM. Investigation in the corrosion behaviour of bulk nanocrystalline 316L austenitic stainless steel in NaCl solution [J]. Micro & Nano Letters, 2012, 7(4): 380

[20] EskandariM, NajafizadehA, KermanpurA, et al. . Potential application of nanocrystalline 301 austenitic stainless steel in lightweight vehicle structures [J]. Materials & Design, 2009, 3093869-3872

[21] TiamiyuA A, SzpunarJ A, OdeshiA G, et al. . Development of ultra-fine-grained structure in AISI 321 austenitic stainless steel [J]. Metallurgical and Materials Transactions A, 2017, 48(12): 5990-6012

[22] FuX-q, JiY-c, ChengX-q, et al. . Effect of grain size and its uniformity on corrosion resistance of rolled 316L stainless steel by EBSD and TEM [J]. Materials Today Communications, 2020, 25101429

[23] NezakatM, AkhianiH, SabetS M, et al. . Electron backscatter and X-ray diffraction studies on the deformation and annealing textures of austenitic stainless steel 310S [J]. Materials Characterization, 2017, 123115-127

[24] NezakatM, AkhianiH, HoseiniM, et al. . Effect of thermo-mechanical processing on texture evolution in austenitic stainless steel 316L [J]. Materials Characterization, 2014, 98: 10-17

[25] KorznikovaG, MironovS, KonkovaT, et al. . EBSD characterization of cryogenically rolled type 321 austenitic stainless steel [J]. Metallurgical and Materials Transactions A, 2018, 49(12): 6325-6336

[26] TiamiyuA A, OdeshiA G, SzpunarJ A. Austenitic reversion of cryo-rolled Ti-stabilized austenitic stainless steel: High-resolution EBSD investigation [J]. Journal of Materials Engineering and Performance, 2018, 27(2): 889-904

[27] OdnobokovaM, BelyakovA, EnikeevN, et al. . Annealing behavior of a 304L stainless steel processed by large strain cold and warm rolling [J]. Materials Science and Engineering A, 2017, 689: 370-383

[28] ChowdhuryS G, DasS, RavikumarB, et al. . Textural development in AISI 316 stainless steel during cold rolling and annealing [J]. Materials Science Forum, 2002, 408–412: 1371-1376

[29] JiaoW-c, LiH-b, FengH, et al. . Effect of high nitrogen addition on microstructure and mechanical properties of as-cast M42 high speed steel [J]. ISIJ International, 2020, 60(3): 564-572

[30] WangX-b, LiuC-b, QinY-m, et al. . Effect of tempering temperature on microstructure and mechanical properties of nanostructured bainitic steel [J]. Materials Science and Engineering A, 2022, 832: 142357

[31] SohrabiM J, NaghizadehM, MirzadehH. Deformation-induced martensite in austenitic stainless steels: A review [J]. Archives of Civil and Mechanical Engineering, 2020, 20(4): 124

[32] ShenY F, LiX X, SunX, et al. . Twinning and martensite in a 304 austenitic stainless steel [J]. Materials Science and Engineering A, 2012, 552514-522

[33] FengZ-x, ZecevicM, KnezevicM. Stressassisted (γ → α′) and strain-induced (γ → εs → α′) phase transformation kinetics laws implemented in a crystal plasticity model for predicting strain path sensitive deformation of austenitic steels [J]. International Journal of Plasticity, 2021, 136102807

[34] BrofmanP J, AnsellG S. On the effect of carbon on the stacking fault energy of austenitic stainless steels [J]. Metallurgical Transactions A, 1978, 9(6): 879-880

[35] RhodesC G, ThompsonA W. The composition dependence of stacking fault energy in austenitic stainless steels [J]. Metallurgical Transactions A, 1977, 8(12): 1901-1906

[36] SunG-s, ZhaoM-m, DuL-x, et al. . Significant effects of grain size on mechanical response characteristics and deformation mechanisms of metastable austenitic stainless steel [J]. Materials Characterization, 2022, 184111674

[37] AmininejadA, JamaatiR, HosseinipourS J. Achieving superior strength and high ductility in AISI 304 austenitic stainless steel via asymmetric cold rolling [J]. Materials Science and Engineering A, 2019, 767138433

[38] JamaatiR, ToroghinejadM R. Effect of stacking fault energy on deformation texture development of nanostructured materials produced by the ARB process [J]. Materials Science and Engineering A, 2014, 598263-276

[39] EskandariM, Zarei-HanzakiA, Mohtadi-BonabM A, et al. . Grain-orientation-dependent of γ-ε-α′ transformation and twinning in a super-high-strength, high ductility austenitic Mn-steel [J]. Materials Science and Engineering A, 2016, 674: 514-528

[40] EskandariM, KermanpurA, NajafizadehA. Formation of nano-grained structure in a 301 stainless steel using a repetitive thermo-mechanical treatment [J]. Materials Letters, 2009, 63(16): 1442-1444

[41] diS A, SalvatoriI, KennyJ M. Effects of martensite formation and austenite reversion on grain refining of AISI 304 stainless steel [J]. Journal of Materials Science, 2002, 37(21): 4561-4565

[42] KumarB R, SinghA K, DasS, et al. . Cold rolling texture in AISI 304 stainless steel [J]. Materials Science and Engineering A, 2004, 364(1–2): 132-139

[43] EskandariM, NajafizadehA, KermanpurA. Effect of strain-induced martensite on the formation of nanocrystalline 316L stainless steel after cold rolling and annealing [J]. Materials Science and Engineering A, 2009, 519(1–2): 46-50

[44] EskandariM, KermanpurA, NajafizadehA. Formation of nanocrystalline structure in 301 stainless steel produced by martensite treatment [J]. Metallurgical and Materials Transactions A, 2009, 40(9): 2241-2249

[45] RezaeiH A, GhazaniM S, EghbaliB. Effect of post deformation annealing on the microstructure and mechanical properties of cold rolled AISI 321 austenitic stainless steel [J]. Materials Science and Engineering A, 2018, 736: 364-374

[46] PadilhaA F, PlautR L, RiosP R. Annealing of cold-worked austenitic stainless steels [J]. ISIJ International, 2003, 43(2): 135-143

[47] YangS W, SpruiellJ E. Cold-worked state and annealing behaviour of austenitic stainless steel [J]. Journal of Materials Science, 1982, 17(3): 677-690

[48] DonadilleC, ValleR, DervinP, et al. . Development of texture and microstructure during cold-rolling and annealing of F.C.C. alloys: Example of an austenitic stainless steel [J]. Acta Metallurgica, 1989, 37(6): 1547-1571

[49] WeiF-a, WangJ-h, ShiB, et al. . Effect of annealing time on bimodal microstructures and tensile properties of Mg-6Sn-3Al-Zn alloy [J]. Materials Research Express, 2020, 7(10): 106504

[50] EskandariM, Mohtadi-BonabM A, BasuR, et al. . Preferred crystallographic orientation development in nano/ultrafine-grained 316L stainless steel during martensite to austenite reversion [J]. Journal of Materials Engineering and Performance, 2015, 242644-653

[51] ShirdelM, MirzadehH, ParsaM H. Enhanced mechanical properties of microalloyed austenitic stainless steel produced by martensite treatment [J]. Advanced Engineering Materials, 2015, 17(8): 1226-1233

[52] NaikS N, WalleyS M. The Hall-Petch and inverse Hall-Petch relations and the hardness of nanocrystalline metals [J]. Journal of Materials Science, 2020, 55(7): 2661-2681

[53] LiH-b, JiangZ-h, ZhangZ-r, et al. . Effect of grain size on mechanical properties of nickel-free high nitrogen austenitic stainless steel [J]. Journal of Iron and Steel Research, International, 2009, 16(1): 58-61

[54] TakakiS, KawasakiK, KimuraY. Mechanical properties of ultra fine grained steels [J]. Journal of Materials Processing Technology, 2001, 117(3): 359-363

[55] PetchN J. The cleavage strength of polycrystals [J]. Journal of Iron and Steel Institute, 1953, 174(1): 25-28

[56] HallE O. The deformation and ageing of mild steel: III discussion of results [J]. Proceedings of the Physical Society Section B, 1951, 64(9): 747-753

[57] AnwarM S, MeliniaR K, PradistiM G, et al. . Effect of prior austenite grain-size on the annealing twin density and hardness in the austenitic stainless steel [J]. International Journal of Technology, 2021, 12(6): 1149

[58] HuangJ-x, YeX-n, GuJ-q, et al. . Enhanced mechanical properties of type AISI301LN austenitic stainless steel through advanced thermo mechanical process [J]. Materials Science and Engineering A, 2012, 532: 190-195

[59] ChenX H, LuJ, LuL, et al. . Tensile properties of a nanocrystalline 316L austenitic stainless steel [J]. Scripta Materialia, 2005, 52(10): 1039-1044

[60] HugE, PrasathB R, MonnetI, et al. . Impact of the nanostructuration on the corrosion resistance and hardness of irradiated 316 austenitic stainless steels [J]. Applied Surface Science, 2017, 3921026-1035

[61] TiamiyuA A, EduokU, SzpunarJ A, et al. . Corrosion behavior of metastable AISI 321 austenitic stainless steel: Investigating the effect of grain size and prior plastic deformation on its degradation pattern in saline media [J]. Scientific Reports, 2019, 9(1): 1-18

[62] RoyB, KumarR, DasJ. Effect of cryorolling on the microstructure and tensile properties of bulk nano-austenitic stainless steel [J]. Materials Science and Engineering A, 2015, 631: 241-247

[63] NaghizadehM, MirzadehH. Effects of grain size on mechanical properties and work-hardening behavior of AISI 304 austenitic stainless steel [J]. Steel Research International, 2019, 90(10): 1900153

[64] KheiriS, MirzadehH, NaghizadehM. Tailoring the microstructure and mechanical properties of AISI 316L austenitic stainless steel via cold rolling and reversion annealing [J]. Materials Science and Engineering A, 2019, 75990-96