Ultrasonic-assisted extraction of pectin from chaenomeles

Abstract

Ultrasound was applied for the extraction of pectin from chaenomeles. The content of pectin was evaluated by carbazole colorimetric method. Based on the results of the single factor experiment and the orthogonal tests, the optimum extraction parameters are as follows: the solid-to-liquid ratio is 1:4 g/mL, the ultrasonic power is 320 W, the ultrasonic-assisted extraction temperature is 60 °C, the ultrasonic-assisted extraction time is 50 min, and pH value is 2.0. Compared with acid hydrolyze methods, the extraction time of the present technique decreases from 70 min to 50 min, and the extraction yield increases from 1.39% to 2.61%. The results show that ultrasonic-assisted extraction is time-saving and highly efficient, so it provides a new way to extract pectin from chaenomeles.

Keywords

chaenomeles / pectin / orthogonal experiments

References

[1] WangX-feng. Industry of emerging fruits-papaya [J]. Gansu Agriculture, 200362

[2] LiY-shan. Extraction of pectin [J]. Journal of Three Gorges University: Natural Science, 2002, 24(6): 571-573

[3] TianS-d, RenH-tao. Current situation and development trend of the pectin extraction technology [J]. Food Science and Technology, 200353-55

[4] CaiH, QiuH-y, ZhangZ-yuan. Research of best technics of distilling pectin from apple peel [J]. Guangdong Chemical Industry, 2005, 7: 14-15

[5] Canteri-ScheminM H, FertonaniH C R, WaszczynskyjN, WosiackiG. Extraction of pectin from apple pomace [J]. Brazilian Archives of Biology and Technology, 2005, 3: 259-265

[6] WanL-cai. Studies on the preparation of dietary fiber and pectin from sugar beet pulp [J]. Food and Fermentation Industries, 1994, 3: 10-15

[7] LoyolaN, PavézP, LilloS. Pectin extraction from cv. pink lady (Malus pumila) apples [J]. Ciencia e Investigación Agraria, 2011, 38(3): 425-434

[8] WangC, LiLi. A study on technology of extracting pectin from lemon peel [J]. China Food Additives, 2006, 3(3): 47-49

[9] DongW, YuLong. Pectin-extracting with microwave from banana peel [J]. Studies of Trace Elements and Health, 2006, 23(1): 33-34

[10] AinaV O, MustaphaM B, MammanO A, AminaZ, HauwaH, HauwaU M S, YaganaB A. Extraction and characterization of pectin from peels of lemon (Citrus limon), grape fruit (Citrus paradisi) and sweet orange (Citrus sinensis) [J]. British Journal of Pharmacology and Toxicology, 2012, 3(6): 259-262

[11] ZhangC-s, QingX-m, LinH-j, TangY-l, HuL-fei. Study on pectin extraction conditions from pineapple peel with ultrasonic assistant technology [J]. Food Processing Technology, 2007, 28(3): 147-152

[12] WangH-b, WangF-a, PanC-dao. Study on improved pectin extraction method from orange peel [J]. Food Science, 2007, 28(2): 136-141

[13] ConstenlaD, PonceA G, LozanoJ E. Kinetic model of pectin demethylation [J]. Latin American Applied Research, 2003, 33: 91-96

[14] ChoY J, HwangJ K. Modeling the yield and intrinsic viscosity of pectin in acidic solubilization of apple pomace [J]. Journal of Food Engineering, 2000, 44(2): 85-89

[15] FertonaniH C R, ScabioA, CarneiroE B B C, SchemimM H C, NogueiraA, WosiackiG. Extraction model of low methoxyl pectin from apple pomace effects of acid concentration and time on the process and the product [J]. Food Science and Technology, 2009, 52(1): 178-185

[16] WuY-f, LiuC-chong. A study on technology of extracting pectin from chaenomeles sinensis [J]. Guangdong Chemical Industry, 2004, 8: 12-13

[17] ZhengY-qin. Study on extraction technology of pectin from yizhou chaenomeles sinensis [J]. Science, 2008, 11: 361-364

[18] YangM, LiuX-h, HeP-yi. Extracting pectin with microwave from paraya peel [J]. Processing of Agricultural Products, 2012, 8: 73-75

[19] YapoB M, KoffiK L. Extraction and characterization of highly gelling low methoxy pectin from cashew apple pomace [J]. Foods, 2014, 3: 1-12

[20] ZhaoE-f, ZhangM, LiY, XuLi. Study on extraction of pectin from carrot with ultrasonic wave [J]. China Food Additives, 2011, 6: 103-105

[21] HouM-lingFood analysis [M], 2004, Beijing, Chemical Publishing: 86-90

[22] ChenY, HuangZ-l, JiangL-h, XiongY-f, WenZ-y, ZhuH-fu. Studies on extraction of pectin in pyracantha fortuneana with ultrasonic wave [J]. China Food Additives, 2009, 6: 54-58

[23] XuW-y, HaoL-ping. Investigation on extraction technics of pectin from carrot by acidolysis [J]. Cereal and Food Industry, 2007, 14(5): 20-22

[24] YangX-j, DangBin. Optimization of pectin extraction from potato pulp and product composition analysis [J]. Food Science, 2011, 32(4): 25-30