Multi-Scale Pore Structure Heterogeneity in Tuff Reservoirs Investigated with Multi-Experimental Method and Fractal Dimensions in Chang 7 Formation, Southern Ordos Basin

Hao Lu, Qing Li, Dali Yue, Dongdong Xia, Shenghe Wu, Lang Wen, Yu He

Journal of Earth Science ›› 2024, Vol. 35 ›› Issue (2) : 666-686. DOI: 10.1007/s12583-023-1857-8
Petroleum Geology

Multi-Scale Pore Structure Heterogeneity in Tuff Reservoirs Investigated with Multi-Experimental Method and Fractal Dimensions in Chang 7 Formation, Southern Ordos Basin

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Abstract

The tight tuff reservoir is an unusual type of unconventional reservoir with strong heterogeneity. However, there is a lack of research on the microscopic pore structure that causes the heterogeneity of tuff reservoirs. Using the Chang 7 Formation in Ordos Basin, China as a case study, carbon-dioxide gas adsorption, nitrogen gas adsorption and high-pressure mercury injection are integrated to investigate the multi-scale pore structure characteristics of tuff reservoirs. Meanwhile, the fractal dimension is introduced to characterize the complexity of pore structure in tuff reservoirs. By this multi-experimental method, the quantitative characterizations of the full-range pore size distribution of four tuff types were obtained and compared in the size ranges of micropores, mesopores and macropores. Fractal dimension curves derived from full-range pores are divided into six segments as D1, D2, D3, D4, D5 and D6 corresponding to fractal characteristics of micropores, smaller mesopores, larger mesopores, smaller macropores, medium macropores and larger macropores, respectively. The macropore volume, average macropore radius and fractal dimension D5 significantly control petrophysical properties. The larger macropore volume, average macropore radius and D5 correspond to favorable pore structure and good reservoir quality, which provides new indexes for the tuff reservoir evaluation. This study enriches the understanding of the heterogeneity of pore structures and contributes to unconventional oil and gas exploration and development.

Keywords

tuff reservoir / pore structure / carbon-dioxide gas adsorption / nitrogen gas adsorption / high-pressure mercury injection / fractal dimension / petroleum geology

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Hao Lu, Qing Li, Dali Yue, Dongdong Xia, Shenghe Wu, Lang Wen, Yu He. Multi-Scale Pore Structure Heterogeneity in Tuff Reservoirs Investigated with Multi-Experimental Method and Fractal Dimensions in Chang 7 Formation, Southern Ordos Basin. Journal of Earth Science, 2024, 35(2): 666‒686 https://doi.org/10.1007/s12583-023-1857-8

References

[]
Brunauer S, Deming L S, Deming W E, et al.. On a Theory of the van Der Waals Adsorption of Gases. Journal of the American Chemical Society, 1940, 62(7): 1723-1732,
CrossRef Google scholar
[]
Chen C C, Huang Z L, Chen X, et al.. The Formation Conditions of the Upper Carboniferous Near-Source Tuff Tight Oil Reservoir in Santanghu Basin, Xinjiang Province. Geol. Bull. China, 2018, 37(1): 83-92 (in Chinese with English Abstract)
[]
Chen X, Liu J T, Long F, et al.. Practical Experience and Understanding of Exploration and Development of Permian Tight Tuff Reservoir in the Santanghu Basin. China Pet. Explor., 2019, 24(6): 771-780 (in Chinese with English Abstract)
[]
Clarkson C R, Solano N, Bustin R M, et al.. Pore Structure Characterization of North American Shale Gas Reservoirs Using USANS/SANS, Gas Adsorption, and Mercury Intrusion. Fuel, 2013, 103: 606-616,
CrossRef Google scholar
[]
Donaldson E C, Kendall R F, Baker B A, et al.. Surface-Area Measurement of Geologic Materials. Soc. Pet. Eng. AIME J., 1975, 15(2): 111-116,
CrossRef Google scholar
[]
Dong S Q, Zeng L B, Che X H, et al.. Application of Artificial Intelligence in Fracture Identification Using Well Logs in Tight Reservoirs. Earth Science, 2023, 48(7): 2443-2461 (in Chinese with English Abstract)
[]
Dou W C, Liu L F, Wu K J, et al.. Diagenetic Heterogeneity, Pore Throats Characteristic and Their Effects on Reservoir Quality of the Upper Triassic Tight Sandstones of Yanchang Formation in Ordos Basin, China. Marine and Petroleum Geology, 2018, 98: 243-257,
CrossRef Google scholar
[]
Gong L, Cheng Y Q, Gao S, et al.. Fracture Connectivity Characterization and Its Controlling Factors in Lower Jurassic Tight Sandstone Reservoirs of Eastern Kuqa Foreland Basin. Earth Science, 2023, 48(7): 2475-2488 (in Chinese with English Abstract)
[]
Guo X B, Huang Z L, Zhao L B, et al.. Pore Structure and Multi-Fractal Analysis of Tight Sandstone Using MIP, NMR and NMRC Methods: A Case Study from the Kuqa Depression, China. Journal of Petroleum Science and Engineering, 2019, 178: 544-558,
CrossRef Google scholar
[]
Hay R L, Sheppard R A. Occurrence of Zeolites in Sedimentary Rocks: An Overview. Natural Zeolites Occurrence Properties & Applications, 2001, 45(1): 217-234,
CrossRef Google scholar
[]
He C, Ji L M, Wu Y D, et al.. Characteristics of Hydrothermal Sedimentation Process in the Yanchang Formation, South Ordos Basin, China: Evidence from Element Geochemistry. Sedimentary Geology, 2016, 345: 33-41,
CrossRef Google scholar
[]
Huang W B, Lu S F, Hersi O S, et al.. Reservoir Spaces in Tight Sandstones: Classification, Fractal Characters, and Heterogeneity. Journal of Natural Gas Science and Engineering, 2017, 46: 80-92,
CrossRef Google scholar
[]
Jaroniec M. Evaluation of the Fractal Dimension from a Single Adsorption Isotherm. Langmuir, 1995, 11(6): 2316-2317,
CrossRef Google scholar
[]
Jiang Y Q, Liu Y Q, Yang Z, et al.. Characteristics and Origin of Tuff-Type Tight Oil in Jimusaer Sag, Junggar Basin, NW China. Petroleum Exploration and Development, 2015, 42(6): 810-818,
CrossRef Google scholar
[]
Kolata D R, Frost J K, Huff W D. Chemical Correlation of K-Bentonite Beds in the Middle Ordovician Decorah Subgroup, Upper Mississippi Valley. Geology, 1987, 15(3): 208-211,
CrossRef Google scholar
[]
Lai J, Wang G W, Wang Z Y, et al.. A Review on Pore Structure Characterization in Tight Sandstones. Earth-Science Reviews, 2018, 177: 436-457,
CrossRef Google scholar
[]
Law B E, Curtis J B. Introduction to Unconventional Petroleum Systems. AAPG Bulletin, 2002, 86: 1851-1852
[]
Li A, Ding W L, Jiu K, et al.. Investigation of the Pore Structures and Fractal Characteristics of Marine Shale Reservoirs Using NMR Experiments and Image Analyses: A Case Study of the Lower Cambrian Niutitang Formation in Northern Guizhou Province, South China. Marine and Petroleum Geology, 2018, 89: 530-540,
CrossRef Google scholar
[]
Li B, Guo Y J, Wu J P, et al.. Study on Main Controlling Factors of Tuff Tight Reservoir Development in Tengyi Submember of Anan Sag, Erlian Basin. Abstract Book of Sedimentology and Unconventional Resources, 2015 China National Sedimentology Congress 298-299 (in Chinese with English Abstract)
[]
Li K W. Analytical Derivation of Brooks-Corey Type Capillary Pressure Models Using Fractal Geometry and Evaluation of Rock Heterogeneity. Journal of Petroleum Science and Engineering, 2010, 73(1/2): 20-26,
CrossRef Google scholar
[]
Li P, Zheng M, Bi H, et al.. Pore Throat Structure and Fractal Characteristics of Tight Oil Sandstone: A Case Study in the Ordos Basin, China. Journal of Petroleum Science and Engineering, 2017, 149: 665-674,
CrossRef Google scholar
[]
Li Q, Lu H, Li J S, et al.. Characteristics and Formation Mechanism of the Tight Tuff Reservoirs of the Upper Triassic Chang 7 Member in the Southern Ordos Basin, China. Marine and Petroleum Geology, 2022, 139: 105625,
CrossRef Google scholar
[]
Li Q, Wu S H, Xia D L, et al.. Major and Trace Element Geochemistry of the Lacustrine Organic-Rich Shales from the Upper Triassic Chang 7 Member in the Southwestern Ordos Basin, China: Implications for Paleoenvironment and Organic Matter Accumulation. Marine and Petroleum Geology, 2020, 111: 852-867,
CrossRef Google scholar
[]
Li T J, Huang Z L, Zhao J, et al.. Pore Structure Characteristics and Their Influencing Factors: A Case Study from the Middle Jurassic Mixed Siliciclastic Carbonate Rocks, Turpan-Hami Basin, Northwest China. Journal of Petroleum Science and Engineering, 2021, 203: 108611,
CrossRef Google scholar
[]
Li X B, Liu H Q, Pan S X, et al.. Subaqueous Sandy Mass-Transport Deposits in Lacustrine Facies of the Upper Triassic Yanchang Formation, Ordos Basin, Central China. Marine and Petroleum Geology, 2018, 97: 66-77,
CrossRef Google scholar
[]
Liu F, Zhu X, Li Y, et al.. Sedimentary Facies Analysis and Depositional Model of Gravity-Flow Deposits of the Yanchang Formation, Southwestern Ordos Basin, NW China. Australian Journal of Earth Sciences, 2016, 63(7): 885-902,
CrossRef Google scholar
[]
Liu M, Xie R H, Guo J F, et al.. Characterization of Pore Structures of Tight Sandstone Reservoirs by Multifractal Analysis of the NMR T 2 Distribution. Energy & Fuels, 2018, 32(12): 12218-12230,
CrossRef Google scholar
[]
Liu X H, Wang W W, Feng M Y, et al.. Hydrothermal Process and Duration of Carboniferous Altered Tuff Reservoir in Well Dixi 14 Area of Kelameili Gas Field (Junggar Basin), NW China. Earth Science, 2022, 47(5): 1694-1710 (in Chinese with English Abstract)
[]
Loucks R G, Reed R M, Ruppel S C, et al.. Spectrum of Pore Types and Networks in Mudrocks and a Descriptive Classification for Matrix-Related Mudrock Pores. AAPG Bulletin, 2012, 96(6): 1071-1098,
CrossRef Google scholar
[]
Lu H, Li Q, Yue D L, et al.. Study on Optimal Selection of Porosity Logging Interpretation Methods for Chang 73 Segment of the Yanchang Formation in the Southwestern Ordos Basin, China. Journal of Petroleum Science and Engineering, 2021, 198: 108153,
CrossRef Google scholar
[]
Lu H, Xia D D, Li Q, et al.. Quantitative Characterization and Differences of the Pore Structure in Lacustrine Siliceous Shale and Argillaceous Shale: A Case Study of the Upper Triassic Yanchang Formation Shales in the Southern Ordos Basin, China. Energy & Fuels, 2021, 35(19): 15525-15544,
CrossRef Google scholar
[]
Lyu W Y, Zeng L B, Zhang B J, et al.. Influence of Natural Fractures on Gas Accumulation in the Upper Triassic Tight Gas Sandstones in the Northwestern Sichuan Basin, China. Marine and Petroleum Geology, 2017, 83: 60-72,
CrossRef Google scholar
[]
Ma J, Huang Z L, Liang S J, et al.. Geochemical and Tight Reservoir Characteristics of Sedimentary Organic-Matter-Bearing Tuff from the Permian Tiaohu Formation in the Santanghu Basin, Northwest China. Marine and Petroleum Geology, 2016, 73: 405-418,
CrossRef Google scholar
[]
Ma J, Liu G H, Huang Z L, et al.. Tight Tuff Reservoir Characteristics and Its Controlling Factors: A Comparative Study of the Permian Tiaohu Formation and Carboniferous Haerjiawu Formation in the Santanghu Basin, NW China. Journal of Petroleum Science and Engineering, 2020, 187: 106808,
CrossRef Google scholar
[]
Mandelbrot B B, Wheeler J A. The Fractal Geometry of Nature. American Journal of Physics, 1983, 51(3): 286-287,
CrossRef Google scholar
[]
Pan Y S, Huang Z L, Li T J, et al.. Pore Structure Characteristics and Evaluation of Lacustrine Mixed Fine-Grained Sedimentary Rocks: A Case Study of the Lucaogou Formation in the Malang Sag, Santanghu Basin, Western China. Journal of Petroleum Science and Engineering, 2021, 201: 108545,
CrossRef Google scholar
[]
Pfeifer P, Wu Y, Cole M, et al.. Multilayer Adsorption on a Fractally Rough Surface. Physical Review Letters, 1989, 62(17): 1997-2000,
CrossRef Google scholar
[]
Qin S, Wang R, Shi W Z, et al.. Diverse Effects of Intragranular Fractures on Reservoir Properties, Diagenesis, and Gas Migration: Insight from Permian Tight Sandstone in the Hangjinqi Area, North Ordos Basin. Marine and Petroleum Geology, 2022, 137: 105526,
CrossRef Google scholar
[]
Qiu X W, Liu C Y, Mao G Z, et al.. Late Triassic Tuff Intervals in the Ordos Basin, Central China: Their Depositional, Petrographic, Geochemical Characteristics and Regional Implications. Journal of Asian Earth Sciences, 2014, 80: 148-160,
CrossRef Google scholar
[]
Rouquerol J, Avnir D, Fairbridge C W, et al.. Recommendations for the Characterization of Porous Solids (Technical Report). Pure and Applied Chemistry, 1994, 66(8): 1739-1758,
CrossRef Google scholar
[]
Shamim A, Nosheen S, Yang X Y. Genesis of Tuff Interval and Its Uranium Enrichment in Upper Triassic of Ordos Basin, NW China. Acta Geochimica, 2018, 37(1): 32-46,
CrossRef Google scholar
[]
Shao X H, Pang X Q, Li Q W, et al.. Pore Structure and Fractal Characteristics of Organic-Rich Shales: A Case Study of the Lower Silurian Longmaxi Shales in the Sichuan Basin, SW China. Marine and Petroleum Geology, 2017, 80: 192-202,
CrossRef Google scholar
[]
Sing K S W. Reporting Physisorption Data for Gas/Solid Systems with Special Reference to the Determination of Surface Area and Porosity (Recommendations 1984). Pure and Applied Chemistry, 1985, 57(4): 603-619,
CrossRef Google scholar
[]
Smith R K, Tremallo R L, Lofgren G E. Growth of Megaspherulites in a Rhyolitic Vitrophyre. American Mineralogist, 2001, 86(5/6): 589-600,
CrossRef Google scholar
[]
Song Z Z, Liu G D, Yang W W, et al.. Multi-Fractal Distribution Analysis for Pore Structure Characterization of Tight Sandstone—A Case Study of the Upper Paleozoic Tight Formations in the Longdong District, Ordos Basin. Marine and Petroleum Geology, 2018, 92: 842-854,
CrossRef Google scholar
[]
Su X C, Gong L, Fu X F, et al.. Fracture Distribution Characteristics and Effectiveness Evaluation of Tight Sandstone Reservoir of Chang 7 Member in Sanbian Area, Ordos Basin. Earth Science, 2023, 48(7): 2601-2613 (in Chinese with English Abstract)
[]
Thomas Kalan H P, Sitorus M E. Jatibarang Field, Geologic Study of Volcanic Reservoir for Horizontal Well Proposal. Indonesian Petroleum Association, 23rd Annual Convention Proceedings, 1994, 1: 229-244
[]
Tomaru H, Lu Z L, Fehn U, et al.. Origin of Hydrocarbons in the Green Tuff Region of Japan: 129I Results from Oil Field Brines and Hot Springs in the Akita and Niigata Basins. Chemical Geology, 2009, 264(1/2/3/4): 221-231,
CrossRef Google scholar
[]
Torabi A, Fossen H, Braathen A. Insight into Petrophysical Properties of Deformed Sandstone Reservoirs. AAPG Bulletin, 2013, 97(4): 619-637,
CrossRef Google scholar
[]
Wan X F, Liu C C, Zhao D F, et al.. Hotspot and Development Trend of Shale Oil Research. Earth Science, 2023, 48(2): 793-813 (in Chinese with English Abstract)
[]
Wang C, Wang Q X, Chen G J, et al.. Petrographic and Geochemical Characteristics of the Lacustrine Black Shales from the Upper Triassic Yanchang Formation of the Ordos Basin, China: Implications for the Organic Matter Accumulation. Marine and Petroleum Geology, 2017, 86: 52-65,
CrossRef Google scholar
[]
Wang F Y, Yang K, You J X, et al.. Analysis of Pore Size Distribution and Fractal Dimension in Tight Sandstone with Mercury Intrusion Porosimetry. Results in Physics, 2019, 13: 102283,
CrossRef Google scholar
[]
Wang J, Cao Y C, Liu K Y, et al.. Fractal Characteristics of the Pore Structures of Fine-Grained, Mixed Sedimentary Rocks from the Jimsar Sag, Junggar Basin: Implications for Lacustrine Tight Oil Accumulations. Journal of Petroleum Science and Engineering, 2019, 182: 106363,
CrossRef Google scholar
[]
Wang L, Yin R, Sima L Q, et al.. Insights into Pore Types and Wettability of a Shale Gas Reservoir by Nuclear Magnetic Resonance: Longmaxi Formation, Sichuan Basin, China. Energy & Fuels, 2018, 32(9): 9289-9303,
CrossRef Google scholar
[]
Wang N J. . Characteristics and Controlling Factors of Volcanic Reservoirs in Cenozoic Group Qikou Depression, 2012 Xi’an Northwest University (in Chinese with English Abstract)
[]
Wang R, Shi W Z, Xie X Y, et al.. Clay Mineral Content, Type, and Their Effects on Pore Throat Structure and Reservoir Properties: Insight from the Permian Tight Sandstones in the Hangjinqi Area, North Ordos Basin, China. Marine and Petroleum Geology, 2020, 115: 104281,
CrossRef Google scholar
[]
Wang W R, Yue D L, Eriksson K A, et al.. Quantification and Prediction of Pore Structures in Tight Oil Reservoirs Based on Multifractal Dimensions from Integrated Pressure- and Rate-Controlled Porosimetry for the Upper Triassic Yanchang Formation, Ordos Basin, China. Energy & Fuels, 2020, 34(4): 4366-4383,
CrossRef Google scholar
[]
Wang X X, Hou J G, Song S H, et al.. Combining Pressure-Controlled Porosimetry and Rate-Controlled Porosimetry to Investigate the Fractal Characteristics of Full-Range Pores in Tight Oil Reservoirs. Journal of Petroleum Science and Engineering, 2018, 171: 353-361,
CrossRef Google scholar
[]
Wei W, Zhu X M, He M W, et al.. Original Sediment Composition of the Lower Cretaceous Lacustrine Tight-Oil Mudstone and Influences on Diagenesis and Organic Matter Content, the Erennaoer Sag in Erlian Basin, NE China. Marine and Petroleum Geology, 2018, 94: 131-143,
CrossRef Google scholar
[]
Wen J. . Reservoir Characteristics of Tuff Tight Oil Reservoirs in ma 56 Block of Santanghu Basin and Research on the Geological Mechanism of Enhanced Oil Recovery, 2019 Chengdu Chengdu University of Technology in Chinese with English Abstract)
[]
Wu H, Zhang C L, Ji Y L, et al.. An Improved Method of Characterizing the Pore Structure in Tight Oil Reservoirs: Integrated NMR and Constant-Rate-Controlled Porosimetry Data. Journal of Petroleum Science and Engineering, 2018, 166: 778-796,
CrossRef Google scholar
[]
Xi Z D, Tang S H, Wang J, et al.. Pore Structure and Fractal Characteristics of Niutitang Shale from China. Minerals, 2018, 8(4): 163,
CrossRef Google scholar
[]
Xian B Z, Wang J H, Gong C L, et al.. Classification and Sedimentary Characteristics of Lacustrine Hyperpycnal Channels: Triassic Outcrops in the South Ordos Basin, Central China. Sedimentary Geology, 2018, 368: 68-82,
CrossRef Google scholar
[]
Xie W D, Wang M, Wang X Q, et al.. Nano-Pore Structure and Fractal Characteristics of Shale Gas Reservoirs: A Case Study of Longmaxi Formation in Southeastern Chongqing, China. Journal of Nanoscience and Nanotechnology, 2021, 21(1): 343-353,
CrossRef Google scholar
[]
Yang R, He S, Yi J Z, et al.. Nano-Scale Pore Structure and Fractal Dimension of Organic-Rich Wufeng-Longmaxi Shale from Jiaoshiba Area, Sichuan Basin: Investigations Using FE-SEM, Gas Adsorption and Helium Pycnometry. Marine and Petroleum Geology, 2016, 70: 27-45,
CrossRef Google scholar
[]
Yang Y T, Li W, Ma L. Tectonic and Stratigraphic Controls of Hydrocarbon Systems in the Ordos Basin: A Multicycle Cratonic Basin in Central China. AAPG Bulletin, 2005, 89(2): 255-269,
CrossRef Google scholar
[]
Zeng L B, Ma S J, Tian H, et al.. Research Progress of Natural Fractures in Organic Rich Shale. Earth Science, 2023, 48(7): 2427-2442 (in Chinese with English Abstract)
[]
Zhang K, Liu R, Liu Z J, et al.. Influence of Volcanic and Hydrothermal Activity on Organic Matter Enrichment in the Upper Triassic Yanchang Formation, Southern Ordos Basin, Central China. Marine and Petroleum Geology, 2020, 112: 104059,
CrossRef Google scholar
[]
Zhang Z, Xu G S, Yuan H F, et al.. Characteristics and Controlling Factors of Carboniferous Volcanic Reservoir in Hashan Area of Junggar Basin. Journal of Northeast Petroleum University, 2013, 37(4): 39-46 120 (in Chinese with English Abstract)
[]
Zheng H, Sun X M, Wang J P, et al.. Devitrification Pores and Their Contribution to Volcanic Reservoirs: A Case Study in the Hailar Basin, NE China. Marine and Petroleum Geology, 2018, 98: 718-732,
CrossRef Google scholar
[]
Zheng H, Sun X M, Zhu D F, et al.. Characteristics and Factors Controlling Reservoir Space in the Cretaceous Volcanic Rocks of the Hailar Basin, NE China. Marine and Petroleum Geology, 2018, 91: 749-763,
CrossRef Google scholar

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