Microstructural evolution during the progressive transformation-induced plasticity effect in a Fe-0.1C-5Mn medium manganese steel

Mei Zhang , Wenhao Li , Yangfei Chen , Yang Jiang , Xiaofei Guo , Han Dong

International Journal of Minerals, Metallurgy, and Materials ›› 2025, Vol. 32 ›› Issue (2) : 369 -379.

PDF
International Journal of Minerals, Metallurgy, and Materials ›› 2025, Vol. 32 ›› Issue (2) :369 -379. DOI: 10.1007/s12613-024-2963-z
Research Article
research-article
Microstructural evolution during the progressive transformation-induced plasticity effect in a Fe-0.1C-5Mn medium manganese steel
Author information +
History +
PDF

Abstract

The microstructural evolution of a cold-rolled and intercritical annealed medium-Mn steel (Fe-0.10C-5Mn) was investigated during uniaxial tensile testing. In-situ observations under scanning electron microscopy, transmission electron microscopy, and X-ray diffraction analysis were conducted to characterize the progressive transformation-induced plasticity process and associated fracture initiation mechanisms. These findings were discussed with the local strain measurements via digital image correlation. The results indicated that Lüders band formation in the steel was limited to 1.5% strain, which was mainly due to the early-stage martensitic phase transformation of a very small amount of the less stable large-sized retained austenite (RA), which led to localized stress concentrations and strain hardening and further retardation of yielding. The small-sized RA exhibited high stability and progressively transformed into martensite and contributed to a stably extended Portevin-Le Chatelier effect. The volume fraction of RA gradually decreased from 26.8% to 8.2% prior to fracture. In the late deformation stage, fracture initiation primarily occurred at the austenite/martensite and ferrite/martensite interfaces and the ferrite phase.

Keywords

medium-Mn steel / retained austenite / progressive transformation-induced plasticity effect / local strain / fracture initiation

Cite this article

Download citation ▾
Mei Zhang, Wenhao Li, Yangfei Chen, Yang Jiang, Xiaofei Guo, Han Dong. Microstructural evolution during the progressive transformation-induced plasticity effect in a Fe-0.1C-5Mn medium manganese steel. International Journal of Minerals, Metallurgy, and Materials, 2025, 32(2): 369-379 DOI:10.1007/s12613-024-2963-z

登录浏览全文

4963

注册一个新账户 忘记密码

References

[1]

Li SS, Luo HW. Medium-Mn steels for hot forming application in the automotive industry. Int. J. Miner. Metall. Mater.. 2021, 28(5): 741

[2]

Xu H, Zhou LJ, Wang WL, Yi Y. A simple route for preparation of TRIP-assisted Si-Mn steel with excellent performance using direct strip casting. Int. J. Miner. Metall. Mater.. 2024, 31(10): 2173

[3]

Hu B, Sui H, Wen QH, Wang Z, Gramlich A, Luo HW. Review on the plastic instability of medium-Mn steels for identifying the formation mechanisms of Lüders and Portevin-Le Chatelier bands. Int. J. Miner. Metall. Mater.. 2024, 31(6): 1285

[4]

Ma Y, Zheng R, Gao ZY, et al. . Multiphase-field simulation of austenite reversion in medium-Mn steels. Int. J. Miner. Metall. Mater.. 2021, 28(5): 847

[5]

Kim MT, Park TM, Baik KH, Choi WS, Han J. Effects of cold rolling reduction ratio on microstructures and tensile properties of intercritically annealed medium-Mn steels. Mater. Sci. Eng. A. 2019, 752: 43

[6]

Cao WQ, Wang C, Shi J, Wang MQ, Hui WJ, Dong H. Microstructure and mechanical properties of Fe-0.2C-5Mn steel processed by ART-annealing. Mater. Sci. Eng. A. 2011, 528(22-23): 6661

[7]

Cai MH, Zhu WJ, Stanford N, Pan LB, Chao Q, Hodgson PD. Dependence of deformation behavior on grain size and strain rate in an ultrahigh strength-ductile Mn-based TRIP alloy. Mater. Sci. Eng. A. 2016, 653: 35

[8]

Lee S, De Cooman BC. Annealing temperature dependence of the tensile behavior of 10 pct Mn multi-phase TWIP-TRIP steel. Metall. Mater. Trans. A. 2014, 45(13): 6039

[9]

Wang YJ, Zhao S, Song RB, Hu B. Hot ductility behavior of a Fe-0.3C-9Mn-2Al medium Mn steel. Int. J. Miner. Metall. Mater.. 2021, 28(3): 422

[10]

Neog SP, Lodh A, Karmakar A, et al. . Insights into the stability of retained austenite during wear. Philos. Mag.. 2023, 103(3): 203

[11]

Zhao MJ, Jiang LH, Li CM, Huang L, Sun CY, Li JJ, Guo ZH. Flow characteristics and hot workability of a typical low-alloy high-strength steel during multi-pass deformation. Int. J. Miner. Metall. Mater.. 2024, 31(2): 323

[12]

J. Hu, X.Y. Li, Q.W. Meng, L.Y. Wang, Y.Z. Li, and W. Xu, Tailoring retained austenite and mechanical property improvement in Al-Si-V containing medium Mn steel via direct inter-critical rolling, Mater. Sci. Eng. A, 855(2022), art. No. 143904.

[13]

Wang XG, Huang MX. Temperature dependence of Lüders strain and its correlation with martensitic transformation in a medium Mn transformation-induced plasticity steel. J. Iron Steel Res. Int.. 2017, 24(11): 1073

[14]

Callahan M, Hubert O, Hild F, Perlade A, Schmitt JH. Coincidence of strain-induced TRIP and propagative PLC bands in medium Mn steels. Mater. Sci. Eng. A. 2017, 704: 391

[15]

Liu WQ, Lian JH. Stress-state dependence of dynamic strain aging: Thermal hardening and blue brittleness. Int. J. Miner. Metall. Mater.. 2021, 28(5): 854

[16]

Sun BH, Vanderesse N, Fazeli F, et al. . Discontinuous strain-induced martensite transformation related to the Portevin-Le Chatelier effect in a medium manganese steel. Scripta Mater.. 2017, 133: 9

[17]

Yang F, Luo HW, Pu EX, Zhang SL, Dong H. On the characteristics of Portevin-Le Chatelier bands in cold-rolled 7Mn steel showing transformation-induced plasticity. Int. J. Plast.. 2018, 103: 188

[18]

Tang LP, Wei PF, Hu ZL, Pang Q. Microstructure and mechanical properties stability of pre-hardening treatment in Al-Cu alloys for pre-hardening forming process. Int. J. Miner. Metall. Mater.. 2024, 31(3): 539

[19]

F. Yang, J. Zhou, Y. Han, P. Liu, H.W. Luo, and H. Dong, A novel cold-rolled medium Mn steel with an ultra-high product of tensile strength and elongation, Mater. Lett., 258(2020), art. No. 126804.

[20]

Yan S, Li TL, Liang TS, Chen JQ, Zhao Y, Liu XH. By controlling recrystallization degree: A plain medium Mn steel overcoming Lüders deformation and low yield-to-tensile ratio simultaneously. Mater. Sci. Eng. A. 2019, 758: 79

[21]

Wang HS, Zhang YX, Yuan G, et al. . Significance of cold rolling reduction on Lüders band formation and mechanical behavior in cold-rolled intercritically annealed medium-Mn steel. Mater. Sci. Eng. A. 2018, 737: 176

[22]

Li ZC, Ding H, Misra RDK, Cai ZH. Deformation behavior in cold-rolled medium-manganese TRIP steel and effect of pre-strain on the Lüders bands. Mater. Sci. Eng. A. 2017, 679: 230

[23]

J. Wu, Y. Hovanski, and M. Miles, Digital image correlation characterization and formability analysis of aluminum alloy TWB during forming, Materials, 15(2022), No. 15, art. No. 5291.

[24]

Wang T, Hu J, Misra RDK. Microstructure evolution and strain behavior of a medium Mn TRIP/TWIP steel for excellent combination of strength and ductility. Mater. Sci. Eng. A. 2019, 753: 99

[25]

Sun BH, Fazeli F, Scott C, Brodusch N, Gauvin R, Yue S. The influence of silicon additions on the deformation behavior of austenite-ferrite duplex medium manganese steels. Acta Mater.. 2018, 148: 249

[26]

Gibbs PJ, De Moor E, Merwin MJ, Clausen B, Speer JG, Matlock DK. Austenite stability effects on tensile behavior of manganese-enriched-austenite transformation-induced plasticity steel. Metall. Mater. Trans. A. 2011, 42(12): 3691

[27]

Wang C, Cao WQ, Shi J, Huang CX, Dong H. Deformation microstructures and strengthening mechanisms of an ultrafine grained duplex medium-Mn steel. Mater. Sci. Eng. A. 2013, 562: 89

[28]

Wang XG, Wang L, Huang MX. Kinematic and thermal characteristics of Lüders and Portevin-Le Châtelier bands in a medium Mn transformation-induced plasticity steel. Acta Mater.. 2017, 124: 17

[29]

Seo EJ, Kim JK, Cho L, Mola J, Oh CY, De Cooman BC. Micro-plasticity of medium Mn austenitic steel: Perfect dislocation plasticity and deformation twinning. Acta Mater.. 2017, 135: 112

[30]

M. Zhang, W.J. Wang, B.D. Zhang, Q.Y. Cen, and J. Liu, Influence of pre-straining on the low-cycle fatigue performance of Fe-0.1C-5Mn medium manganese steel, Int. J. Fatigue, 165(2022), art. No. 107186.

[31]

Steineder K, Krizan D, Schneider R, Béal C, Sommitsch C. On the microstructural characteristics influencing the yielding behavior of ultra-fine grained medium-Mn steels. Acta Mater.. 2017, 139: 39

[32]

Sun BH, Palanisamy D, Ponge D, et al. . Revealing fracture mechanisms of medium manganese steels with and without delta-ferrite. Acta Mater.. 2019, 164: 683

[33]

Narasimha Rao BV, Thomas G. Structure-property relations and the design of Fe-4Cr-C base structural steels for high strength and toughness. Metall. Trans. A. 1980, 11(3): 441

[34]

De Moor E, Matlock DK, Speer JG, Merwin MJ. Austenite stabilization through manganese enrichment. Scripta Mater.. 2011, 64(2): 185

[35]

Talonen J, Hänninen H, Nenonen P, Pape G. Effect of strain rate on the strain-induced γ → α′-martensite transformation and mechanical properties of austenitic stainless steels. Metall. Mater. Trans. A. 2005, 36(2): 421

RIGHTS & PERMISSIONS

University of Science and Technology Beijing

PDF

0

Accesses

0

Citation

Detail

Sections
Recommended

/