Unveiling the cellular microstructure–property relations in martensitic stainless steel via laser powder bed fusion
Lingzhi Wu , Cong Zhang , Dil Faraz Khan , Ruijie Zhang , Yongwei Wang , Xue Jiang , Haiqing Yin , Xuanhui Qu , Geng Liu , Jie Su
International Journal of Minerals, Metallurgy, and Materials ›› 2024, Vol. 31 ›› Issue (11) : 2476 -2487.
Unveiling the cellular microstructure–property relations in martensitic stainless steel via laser powder bed fusion
Laser powder bed fusion (LPBF) is a widely recognized additive manufacturing technology that can fabricate complex components rapidly through layer-by-layer formation. However, there is a paucity of research on the effect of laser scanning speed on the cellular microstructure and mechanical properties of martensitic stainless steel. This study systematically investigated the influence of laser scanning speed on the cellular microstructure and mechanical properties of a developed Fe11Cr8Ni5Co3Mo martensitic stainless steel produced by LPBF. The results show that increasing the laser scanning speed from 400 to 1000 mm/s does not lead to a noticeable change in the phase fraction, but it reduces the average size of the cellular microstructure from 0.60 to 0.35 µm. The scanning speeds of 400 and 1000 mm/s both had adverse effects on performances of sample, resulting in inadequate fusion and keyhole defects respectively. The optimal scanning speed for fabricating samples was determined to be 800 mm/s, which obtained the highest room temperature tensile strength and elongation, with the ultimate tensile strength measured at (1088.3 ± 2.0) MPa and the elongation of (16.76 ± 0.10)%. Furthermore, the mechanism of the evolution of surface morphology, defects, and energy input were clarified, and the relationship between cellular microstructure size and mechanical properties was also established.
| [1] |
|
| [2] |
H.L. Cheng, X.C. Luo, and X. Wu, Recent research progress on additive manufacturing of high-strength low-alloy steels: Focusing on the processing parameters, microstructures and properties, Mater. Today Commun., 36(2023), art. No. 106616. |
| [3] |
|
| [4] |
M. Simonelli, Z.Y. Zou, P. Barriobero-Vila, and Y.Y. Tse, The development of ultrafine grain structure in an additively manufactured titanium alloy via high-temperature microscopy, Materialia, 30(2023), art. No. 101856. |
| [5] |
|
| [6] |
J.L. Cann, A. De Luca, D.C. Dunand, et al., Sustainability through alloy design: Challenges and opportunities, Prog. Mater. Sci., 117(2021), art. No. 100722. |
| [7] |
|
| [8] |
J.R. Lee, M.S. Lee, H. Chae, et al., Effects of building direction and heat treatment on the local mechanical properties of direct metal laser sintered 15–5 PH stainless steel, Mater. Charact., 167(2020), art. No. 110468. |
| [9] |
G. Liu, J. Su, A. Wang, et al., A novel Fe–Cr–Ni–Co–Mo maraging stainless steel with enhanced strength and cryogenic toughness: Role of austenite with core-shell structures, Mater. Sci. Eng. A, 863(2023), art. No. 144537. |
| [10] |
D.H. Liu, J. Su, A. Wang, et al., Tailoring the microstructure and mechanical properties of FeCrNiCoMo maraging stainless steel after laser melting deposition, Mater. Sci. Eng. A, 840(2022), art. No. 142931. |
| [11] |
L.Z. Wu, D.F. Khan, C. Zhang, et al., Microstructure and mechanical characterization of additively manufactured Fe11Cr8Ni5Co3Mo martensitic stainless steel, Mater. Charact., 203(2023), art. No. 113106. |
| [12] |
|
| [13] |
|
| [14] |
G.Q. Dai, M.H. Xue, Y.H. Guo, et al., Gradient microstructure and strength-ductility synergy improvement of 2319 aluminum alloys by hybrid additive manufacturing, J. Alloys Compd., 968(2023), art. No. 171781. |
| [15] |
M.W. Vaughan, M. Elverud, J. Ye, et al., Development of a process optimization framework for fabricating fully dense advanced high strength steels using laser directed energy deposition, Addit. Manuf., 67(2023), art. No. 103489. |
| [16] |
|
| [17] |
|
| [18] |
|
| [19] |
Q. Chen, L.Y. Xu, L. Zhao, K.D. Hao, and Y.D. Han, Effect of scanning speed on microstructure and mechanical properties of as-printed Ti–22Al–25Nb intermetallic by laser powder bed fusion, Mater. Sci. Eng. A, 885(2023), art. No. 145652. |
| [20] |
|
| [21] |
|
| [22] |
M. Sanjari, A. Hadadzadeh, H. Pirgazi, et al., Selective laser melted stainless steel CX: Role of built orientation on microstructure and micro-mechanical properties, Mater. Sci. Eng. A, 786(2020), art. No. 139365. |
| [23] |
J.W. Liu, Y.N. Song, C.Y. Chen, et al., Effect of scanning speed on the microstructure and mechanical behavior of 316L stainless steel fabricated by selective laser melting, Mater. Des., 186(2020), art. No. 108355. |
| [24] |
G.N. Nigon, O. Burkan Isgor, and S. Pasebani, The effect of annealing on the selective laser melting of 2205 duplex stainless steel: Microstructure, grain orientation, and manufacturing challenges, Opt. Laser Technol., 134(2021), art. No. 106643. |
| [25] |
P.F. Jiang, C.H. Zhang, S. Zhang, J.B. Zhang, J. Chen, and H.T. Chen, Additive manufacturing of novel ferritic stainless steel by selective laser melting: Role of laser scanning speed on the formability, microstructure and properties, Opt. Laser Technol., 140(2021), art. No. 107055. |
| [26] |
T.H. Hsu, P.C. Huang, M.Y. Lee, et al., Effect of processing parameters on the fractions of martensite in 17–4 PH stainless steel fabricated by selective laser melting, J. Alloys Compd., 859(2021), art. No. 157758. |
| [27] |
A. Hamada, M. Jaskari, T. Gundgire, and A. Järvenpää, Enhancement and underlying fatigue mechanisms of laser powder bed fusion additive-manufactured 316L stainless steel, Mater. Sci. Eng. A, 873(2023), art. No. 145021. |
| [28] |
|
| [29] |
|
| [30] |
|
| [31] |
J. Song, Q. Tang, Q.X. Feng, et al., Effect of remelting processes on the microstructure and mechanical behaviours of 18Ni-300 maraging steel manufactured by selective laser melting, Mater. Charact., 184(2022), art. No. 111648. |
| [32] |
|
| [33] |
T. Rautio, A. Hamada, J. Kumpula, A. Järvenpää, and T. Allam, Enhancement of electrical conductivity and corrosion resistance by silver shell–copper core coating of additively manufactured AlSi10Mg alloy, Surf. Coat. Technol., 403(2020), art. No. 126426. |
| [34] |
|
| [35] |
|
| [36] |
|
| [37] |
W.Q. Guo, B. Feng, Y. Yang, et al., Effect of laser scanning speed on the microstructure, phase transformation and mechanical property of NiTi alloys fabricated by LPBF, Mater. Des., 215(2022), art. No. 110460. |
| [38] |
R. Esmaeilizadeh, A. Keshavarzkermani, U. Ali, et al., Customizing mechanical properties of additively manufactured Hastelloy X parts by adjusting laser scanning speed, J. Alloys Compd., 812(2020), art. No. 152097. |
| [39] |
|
| [40] |
|
| [41] |
|
| [42] |
|
| [43] |
|
| [44] |
|
| [45] |
J.Q. Zhang, M.J. Wang, L.H. Niu, et al., Effect of process parameters and heat treatment on the properties of stainless steel CX fabricated by selective laser melting, J. Alloys Compd., 877(2021), art. No. 160062. |
| [46] |
S. Afkhami, V. Javaheri, E. Dabiri, H. Piili, and T. Björk, Effects of manufacturing parameters, heat treatment, and machining on the physical and mechanical properties of 13Cr10Ni1.7Mo2Al0.4Mn0.4Si steel processed by laser powder bed fusion, Mater. Sci. Eng. A, 832(2022), art. No. 142402. |
| [47] |
|
| [48] |
|
| [49] |
|
| [50] |
|
| [51] |
|
| [52] |
D.C. Kong, C.F. Dong, S.L. Wei, et al., About metastable cellular structure in additively manufactured austenitic stainless steels, Addit. Manuf., 38(2021), art. No. 101804. |
| [53] |
|
| [54] |
|
| [55] |
|
| [56] |
|
| [57] |
D.M. Li, X. Zhang, R.X. Qin, J.X. Xu, D.Y. Yue, and B.Z. Chen, Influence of processing parameters on AlSi10Mg lattice structure during selective laser melting: Manufacturing defects, thermal behavior and compression properties, Opt. Laser Technol., 161(2023), art. No. 109182. |
| [58] |
|
| [59] |
|
| [60] |
|
| [61] |
J. Kwon, Y.T. Choi, E.S. Kim, et al., Effect of cell characteristics on mechanical properties of AlSi10Mg alloy fabricated by laser powder bed fusion, Mater. Sci. Eng. A, 901(2024), art. No. 146537. |
| [62] |
W.S. Tang, X.Q. Yang, C.B. Tian, and C. Gu, Effect of rotation speed on microstructure and mechanical anisotropy of Al-5083 alloy builds fabricated by friction extrusion additive manufacturing, Mater. Sci. Eng. A, 860(2022), art. No. 144237. |
| [63] |
|
| [64] |
|
| [65] |
|
| [66] |
|
| [67] |
|
| [68] |
|
| [69] |
|
| [70] |
|
| [71] |
|
| [72] |
|
| [73] |
P. Peng, K.S. Wang, W. Wang, et al., Relationship between microstructure and mechanical properties of friction stir processed AISI 316L steel produced by selective laser melting, Mater. Charact., 163(2020), art. No. 110283. |
| [74] |
|
| [75] |
|
| [76] |
|
| [77] |
|
/
| 〈 |
|
〉 |