Microstructure, mechanical properties and deformation mechanisms of an Al-Mg alloy processed by the cyclical continuous expanded extrusion and drawing approach

Ruiqing Lu , Long Zhang , Shuwei Zheng , Dingfa Fu , Jie Teng , Jianchun Chen , Guodong Zhao , Fulin Jiang , Hui Zhang

International Journal of Minerals, Metallurgy, and Materials ›› 2022, Vol. 29 ›› Issue (1) : 108 -118.

PDF
International Journal of Minerals, Metallurgy, and Materials ›› 2022, Vol. 29 ›› Issue (1) : 108 -118. DOI: 10.1007/s12613-021-2342-y
Article

Microstructure, mechanical properties and deformation mechanisms of an Al-Mg alloy processed by the cyclical continuous expanded extrusion and drawing approach

Author information +
History +
PDF

Abstract

Al—Mg alloys are an important class of non-heat treatable alloys in which Mg solute and grain size play essential role in their mechanical properties and plastic deformation behaviors. In this work, a cyclical continuous expanded extrusion and drawing (CCEED) process was proposed and implemented on an Al—3Mg alloy to introduce large plastic deformation. The results showed that the continuous expanded extrusion mainly improved the ductility, while the cold drawing enhanced the strength of the alloy. With the increased processing CCEED passes, the multi-pass cross shear deformation mechanism progressively improved the homogeneity of the hardness distributions and refined grain size. Continuous dynamic recrystallization played an important role in the grain refinement of the processed Al—3Mg alloy rods. Besides, the microstructural evolution was basically influenced by the special thermomechanical deformation conditions during the CCEED process.

Keywords

Al—Mg alloy / plastic processing / microstructure / mechanical properties / dynamic recrystallization

Cite this article

Download citation ▾
Ruiqing Lu, Long Zhang, Shuwei Zheng, Dingfa Fu, Jie Teng, Jianchun Chen, Guodong Zhao, Fulin Jiang, Hui Zhang. Microstructure, mechanical properties and deformation mechanisms of an Al-Mg alloy processed by the cyclical continuous expanded extrusion and drawing approach. International Journal of Minerals, Metallurgy, and Materials, 2022, 29(1): 108-118 DOI:10.1007/s12613-021-2342-y

登录浏览全文

4963

注册一个新账户 忘记密码

References

[1]

McQueen HJ, Spigarelli S, Kassner ME, Evangelista E. Hot Deformation and Processing of Aluminum Alloys, 2011, Boca Raton, CRC Press

[2]

Estrin Y, Vinogradov A. Extreme grain refinement by severe plastic deformation: A wealth of challenging science. Acta Mater., 2013, 61(3): 782.

[3]

Kuzmina M, Ponge D, Raabe D. Grain boundary segregation engineering and austenite reversion turn embrittlement into toughness: Example of a 9 wt.% medium Mn steel. Acta Mater., 2015, 86, 182.

[4]

Huang CQ, Liu JX, Jia XD. Effect of thermal deformation parameters on the microstructure, texture, and microhardness of 5754 aluminum alloy. Int. J. Miner. Metall. Mater., 2019, 26(9): 1140.

[5]

Valiev RZ, Korznikov AV, Mulyukov RR. Structure and properties of ultrafine-grained materials produced by severe plastic deformation. Mater. Sci. Eng. A, 1993, 168(2): 141.

[6]

Sabirov I, Enikeev NA, Murashkin MY, Valiev RZ. Bulk Nanostructured Materials with Multifunctional Properties, 2015, Cham, Springer

[7]

G. Faraji, H.S. Kim, and H.T. Kashi, Severe Plastic Deformation Methods: Processing and Properties, Elsevier, 2018.

[8]

R. Kalsar, D. Yadav, A. Sharma, H.G. Brokmeier, J. May, H.W. Höppel, W. Skrotzki, and S. Suwas, Effect of Mg content on microstructure, texture and strength of severely equal channel angular pressed aluminium-magnesium alloys, Mater. Sci. Eng. A, 797(2020), art. No. 140088.

[9]

Radetić T, Popović M, Romhanji E, Verlinden B. The effect of ECAP and Cu addition on the aging response and grain substructure evolution in an Al—4.4wt.% Mg alloy. Mater. Sci. Eng. A, 2010, 527(3): 634.

[10]

Romero-Reséndiz L, Flores-Rivera A, Figueroa IA, Braham C, Reyes-Ruiz C, Alfonso I, González G. Effect of the initial ECAP passes on crystal texture and residual stresses of 5083 aluminum alloy. Int. J. Miner. Metall. Mater., 2020, 27(6): 801.

[11]

Yang ZJ, Wang KK, Yang Y. Optimization of ECAP—RAP process for preparing semisolid billet of 6061 aluminum alloy. Int. J. Miner. Metall. Mater., 2020, 27(6): 792.

[12]

Deschamps A, de Geuser F, Horita Z, Lee S, Renou G. Precipitation kinetics in a severely plastically deformed 7075 aluminium alloy. Acta Mater., 2014, 66, 105.

[13]

Bazarnik P, Huang Y, Lewandowska M, Langdon TG. Structural impact on the Hall—Petch relationship in an Al—5Mg alloy processed by high-pressure torsion. Mater. Sci. Eng. A, 2015, 626, 9.

[14]

Liu HS, Zhang B, Zhang GP. Microstructures and mechanical properties of Al/Mg alloy multilayered composites produced by accumulative roll bonding. J. Mater. Sci. Technol., 2011, 27(1): 15.

[15]

Sheikh H. Role of shear banding on the microtexture of an Al—Mg alloy processed by hot/high strain rate accumulative roll bonding. Scripta Mater., 2011, 64(6): 556.

[16]

Yang XH, Wang DG, Wu ZG, Yi JH, Ni S, Du Y, Song M. A coupled EBSD/TEM study of the microstructural evolution of multi-axial compressed pure Al and Al—Mg alloy. Mater. Sci. Eng. A, 2016, 658, 16.

[17]

Valiev RZ, Estrin Y, Horita Z, Langdon TG, Zehetbauer MJ, Zhu YT. Fundamentals of superior properties in bulk NanoSPD materials. Mater. Res. Lett., 2016, 4(1): 1.

[18]

Gao WL, Xu J, Teng J, Lu Z. Microstructure characteristics and mechanical properties of a 2A66 Al—Li alloy processed by continuous repetitive upsetting and extrusion. J. Mater. Res., 2016, 31(16): 2506.

[19]

Chu H S, Liu K S, Yeh J W. An in situ composite of Al (graphite, Al4C3) produced by reciprocating extrusion. Mater. Sci. Eng. A, 2000, 277(1–2): 25.

[20]

Huang JY, Zhu YT, Jiang H, Lowe TC. Microstructures and dislocation configurations in nanostructured Cu processed by repetitive corrugation and straightening. Acta Mater., 2001, 49(9): 1497.

[21]

Utsunomiya H, Hatsuda K, Sakai T, Saito Y. Continuous grain refinement of aluminum strip by conshearing. Mater. Sci. Eng. A, 2004, 372(1–2): 199.

[22]

Murashkin M, Medvedev A, Kazykhanov V, Krokhin A, Raab G, Enikeev N, Valiev RZ. Enhanced mechanical properties and electrical conductivity in ultrafine-grained Al 6101 alloy processed via ECAP—Conform. Metals, 2015, 5(4): 2148.

[23]

Etherington C. Conform—A new concept for the continuous extrusion forming of metals. J. Eng. Ind., 1974, 96(3): 893.

[24]

Peng DS, Yao BQ, Zuo TY. The experimental simulation of deformation behavior of metals in the conform process. J. Mater. Process. Technol., 1992, 31(1–2): 85.

[25]

Zhang H, Yan QQ, Li LX. Microstructures and tensile properties of AZ31 magnesium alloy by continuous extrusion forming process. Mater. Sci. Eng. A, 2008, 486(1–2): 295.

[26]

Raab GJ, Valiev RZ, Lowe TC, Zhu YT. Continuous processing of ultrafine grained Al by ECAP—Conform. Mater. Sci. Eng. A, 2004, 382(1–2): 30.

[27]

Derakhshan JF, Parsa MH, Jafarian HR. Microstructure and mechanical properties variations of pure aluminum subjected to one pass of ECAP—Conform process. Mater. Sci. Eng. A, 2019, 747, 120.

[28]

Xu C, Schroeder S, Berbon PB, Langdon TG. Principles of ECAP—Conform as a continuous process for achieving grain refinement: Application to an aluminum alloy. Acta Mater., 2010, 58(4): 1379.

[29]

Azushima A, Kopp R, Korhonen A, Yang DY, Micari F, Lahoti GD, Groche P, Yanagimoto J, Tsuji N, Rosochowski A, Yanagida A. Severe plastic deformation (SPD) processes for metals. CIRP Ann., 2008, 57(2): 716.

[30]

Stolyarov VV, Zhu YT, Lowe TC, Valiev RZ. Microstructure and properties of pure Ti processed by ECAP and cold extrusion. Mater. Sci. Eng. A, 2001, 303(1–2): 82.

[31]

Park KT, Lee HJ, Lee CS, Nam WJ, Shin DH. Enhancement of high strain rate superplastic elongation of a modified 5154 Al by subsequent rolling after equal channel angular pressing. Scripta. Mater., 2004, 51(6): 479.

[32]

Park KT, Lee HJ, Lee CS, Shin DH. Effect of post-rolling after ECAP on deformation behavior of ECAPed commercial Al—Mg alloy at 723 K. Mater. Sci. Eng. A, 2005, 393(1–2): 118.

[33]

Lu RQ, Zheng SW, Teng J, Hu JM, Fu DF, Chen JC, Zhao GD, Jiang FL, Zhang H. Microstructure, mechanical properties and deformation characteristics of Al—Mg—Si alloys processed by a continuous expansion extrusion approach. J. Mater. Sci. Technol., 2021, 80, 150.

[34]

F.L. Jiang, S. Takaki, T. Masumura, R. Uemori, H. Zhang, and T. Tsuchiyama, Nonadditive strengthening functions for cold-worked cubic metals: Experiments and constitutive modeling, Int. J. Plast., 129(2020), art. No. 102700.

[35]

Zhou F, Liao XZ, Zhu YT, Dallek S, Lavernia EJ. Microstructural evolution during recovery and recrystallization of a nanocrystalline Al—Mg alloy prepared by cryogenic ball milling. Acta Mater., 2003, 51(10): 2777.

[36]

Chaudhuri A, Behera AN, Sarkar A, Kapoor R, Ray RK, Suwas S. Hot deformation behaviour of Mo-TZM and understanding the restoration processes involved. Acta Mater., 2019, 164, 153.

[37]

Kapoor R, Reddy GB, Sarkar A. Discontinuous dynamic recrystallization in α-Zr. Mater. Sci. Eng. A, 2018, 718, 104.

[38]

Sakai T, Belyakov A, Kaibyshev R, Miura H, Jonas JJ. Dynamic and post-dynamic recrystallization under hot, cold and severe plastic deformation conditions. Prog. Mater. Sci., 2014, 60, 130.

[39]

Morris DG, Muñoz-Morris MA. Microstructure of severely deformed Al—3Mg and its evolution during annealing. Acta Mater., 2002, 50(16): 4047.

[40]

Huang K, Logé RE. A review of dynamic recrystallization phenomena in metallic materials. Mater. Des., 2016, 111, 548.

[41]

Kaibyshev R, Shipilova K, Musin F, Motohashi Y. Continuous dynamic recrystallization in an Al—L—Mg—Sc alloy during equal-channel angular extrusion. Mater. Sci. Eng. A, 2005, 396(1–2): 341.

[42]

Su N, Guan RG, Wang X, Wang YX, Jiang WS, Liu HN. Grain refinement in an Al—Er alloy during accumulative continuous extrusion forming. J. Alloys Compd., 2016, 680, 283.

[43]

Wang YX, Guan RG, Hou DW, Zhang Y, Jiang WS, Liu HN. The effects of eutectic silicon on grain refinement in an Al—Si alloy processed by accumulative continuous extrusion forming. J. Mater. Sci., 2017, 52(2): 1137.

[44]

Humphreys FJ, Hatherly M. Recrystallization and Related Annealing Phenomena, 2004, 2nd ed. Amsterdam, Elsevier

[45]

Shen YF, Guan RG, Zhao ZY, Misra RDK. Ultrafinegrained Al—0.2Sc—0.1Zr alloy: The mechanistic contribution of nano-sized precipitates on grain refinement during the novel process of accumulative continuous extrusion. Acta Mater., 2015, 100, 247.

[46]

Aretxabaleta Z, Pereda B, López B. Analysis of the effect of Al on the static softening kinetics of C—Mn steels using a physically based model. Metall. Mater. Trans. A, 2014, 45(2): 934.

[47]

Rehman MK, Zurob HS. A novel approach to model static recrystallization of austenite during hot rolling of Nb microalloyed steel. part I: Precipitate-free case. Metall. Mater. Trans. A, 2013, 44(4): 1862.

[48]

Cahn JW. The impurity-drag effect in grain boundary motion. Acta Metall., 1962, 10(9): 789.

[49]

Simielli EA, Yue S, Jonas JJ. Recrystallization kinetics of microalloyed steels deformed in the intercritical region. Metall. Trans. A, 1992, 23(2): 597.

[50]

Lens A, Maurice C, Driver JH. Grain boundary mobilities during recrystallization of Al—Mn alloys as measured by in situ annealing experiments. Mater. Sci. Eng. A, 2005, 403(1–2): 144.

[51]

J. Tang, F.L. Jiang, C.H. Luo, G.W. Bo, K.Y. Chen, J. Teng, D.F. Fu, and H. Zhang, Integrated physically based modeling for the multiple static softening mechanisms following multistage hot deformation in Al—Zn—Mg—Cu alloys, Int. J. Plast., 134(2020), art. No. 102809.

[52]

Du Y, Chang YA, Huang BY, Gong WP, Jin ZP, Xu HH, Yuan ZH, Liu Y, He YH, Xie FY. Diffusion coefficients of some solutes in fcc and liquid Al: Critical evaluation and correlation. Mater. Sci. Eng. A, 2003, 363(1–2): 140.

[53]

Lücke K, Detert K. A quantitative theory of grain-boundary motion and recrystallization in metals in the presence of impurities. Acta Metall., 1957, 5(11): 628.

[54]

Frost HJ, Ashby MF. Deformation-Mechanism Maps: The Plasticity and Creep of Metals and Ceramics, 1982, Oxford, Pergamon

[55]

Sitdikov O, Sakai T, Avtokratova E, Kaibyshev R, Kimura Y, Tsuzaki K. Grain refinement in a commercial Al—Mg—Sc alloy under hot ECAP conditions. Mater. Sci. Eng. A, 2007, 444(1–2): 18.

[56]

Xu C, Horita Z, Langdon TG. The evolution of homogeneity in an aluminum alloy processed using high-pressure torsion. Acta Mater., 2008, 56(18): 5168.

[57]

To’th LS, Molinari A, Estrin Y. Strain hardening at large strains as predicted by dislocation based polycrystal plasticity model. J. Eng. Mater. Technol., 2002, 124(1): 71.

[58]

McKenzie PWJ, Lapovok R, Estrin Y. The influence of back pressure on ECAP processed AA 6016: Modeling and experiment. Acta Mater., 2007, 55(9): 2985.

AI Summary AI Mindmap
PDF

160

Accesses

0

Citation

Detail

Sections
Recommended

AI思维导图

/