Evolution laws of microstructures and mechanical properties during heat treatments for near-α high-temperature titanium alloys

Xiaozhao Ma , Zhilei Xiang , Tao Li , Yilan Chen , Yingying Liu , Ziyong Chen , Qun Shu

International Journal of Minerals, Metallurgy, and Materials ›› 2022, Vol. 29 ›› Issue (8) : 1596 -1607.

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International Journal of Minerals, Metallurgy, and Materials ›› 2022, Vol. 29 ›› Issue (8) : 1596 -1607. DOI: 10.1007/s12613-021-2248-8
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Evolution laws of microstructures and mechanical properties during heat treatments for near-α high-temperature titanium alloys

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Abstract

Evolution laws of microstructures, mechanical properties, and fractographs after different solution temperatures were investigated through various analysis methods. With the increasing solution temperatures, contents of the primary α phase decreased, and contents of transformed β structures increased. Lamellar α grains dominated the characteristics of transformed β structures, and widths of secondary α lamellas increased monotonously. For as-forged alloy, large silicides with equiaxed and rod-like morphologies, and nano-scale silicides were found. Silicides with large sizes might be (Ti, Zr, Nb)5Si3 and (Ti, Zr, Nb)6Si3. Rod-like silicides with small sizes precipitated in retained β phase, exhibiting near 45° angles with α/β boundaries. Retained β phases in as-heat treated alloys were incontinuous. 980STA exhibited an excellent combination of room temperature (RT) and 650°C mechanical properties. Characteristics of fracture surfaces largely depended on the evolutions of microstructures. Meanwhile, silicides promoted the formation of mico-voids.

Keywords

solution temperatures / microstructures / mechanical properties / fractographs / silicides

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Xiaozhao Ma, Zhilei Xiang, Tao Li, Yilan Chen, Yingying Liu, Ziyong Chen, Qun Shu. Evolution laws of microstructures and mechanical properties during heat treatments for near-α high-temperature titanium alloys. International Journal of Minerals, Metallurgy, and Materials, 2022, 29(8): 1596-1607 DOI:10.1007/s12613-021-2248-8

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