Microstructural evolution of a heat-treated H23 tool steel

Meilinda Nurbanasari , Panos Tsakiropoulos , Eric J. Palmiere

International Journal of Minerals, Metallurgy, and Materials ›› 2015, Vol. 22 ›› Issue (3) : 272 -284.

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International Journal of Minerals, Metallurgy, and Materials ›› 2015, Vol. 22 ›› Issue (3) : 272 -284. DOI: 10.1007/s12613-015-1071-5
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Microstructural evolution of a heat-treated H23 tool steel

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Abstract

The microstructure and the stability of carbides after heat treatments in an H23 tool steel were investigated. The heat treatments consisted of austenization at two different austenizing temperatures (1100°C and 1250°C), followed by water quenching and double-aging at 650°C, 750°C, and 800°C with air cooling between the first and second aging treatments. Martensite did not form in the as-quenched microstructures, which consisted of a ferrite matrix, M6C, M7C3, and MC carbides. The double-aged microstructures consisted of a ferrite matrix and MC, M6C, M7C3, and M23C6 carbides. Secondary hardening as a consequence of secondary precipitation of fine M2C carbides did not occur. There was disagreement between the experimental microstructure and the results of thermodynamic calculations. The highest double-aged hardness of the H23 tool steel was 448 HV after austenization at 1250°C and double-aging at 650°C, which suggested that this tool steel should be used at temperatures below 650°C.

Keywords

tool steel / microstructural evolution / heat treatment / carbides / stability / hardness

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Meilinda Nurbanasari, Panos Tsakiropoulos, Eric J. Palmiere. Microstructural evolution of a heat-treated H23 tool steel. International Journal of Minerals, Metallurgy, and Materials, 2015, 22(3): 272-284 DOI:10.1007/s12613-015-1071-5

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References

[1]

Roberts GA, Kraus G, Kennedy RL. Tool Steels, 1998, Ohio, Materials Park, ASM International

[2]

IOP Conf. Ser. Mater. Sci. Eng., 2012, 28(1art.012024)

[3]

Bała P, Krawczyk J. Transformation during quenching and ageing of hot-work tool steel. Hradec Moravici, 2009, 19, 1.

[4]

Zhang Z, Delagnes D, Bernhart G. Microstructure evolution of hot-work tool steels during tempering and definition of a kinetic law based on hardness measurements. Mater. Sci. Eng. A, 2004, 380, 222.

[5]

Medvedeva A, Bergström J, Gunnarsson S, Andersson J. High temperature properties and microstructural stability of hot work tool steels. Mater. Sci. Eng. A, 2009, 523(1–2): 39.

[6]

Nurbanasari M, Tsakiropoulos P, Palmiere EJ. A study of carbide precipitation in a H21 tool steel. ISIJ Int., 2014, 54(7): 1667.

[7]

Thomson RC, Bhadeshia HKDH. Carbide precipitation in 12Cr1MoV power plant steel. Metall. Trans. A, 1992, 23, 1171.

[8]

Dudova N, Kaibyshev R. On the precipitation sequence in a 10% Cr steel under tempering. ISIJ Int., 2011, 51(5): 826.

[9]

Asadabad MA, Kheirandish S, Novinrooz AJ. Tempering behavior of 4.5Cr-2W-0.25V steel. J. Iron Steel Res. Int., 2010, 17(10): 57.

[10]

Nurbanasari M, Tsakiropoulos P, Palmiere EJ. On the solidification of a H23 tool steel. Trans. Indian Inst. Met., 2014, 67(6): 935.

[11]

Mebarki N, Delagnes D, Lamesle P, Delmas F, Levaillant C. Relationship between microstructure and mechanical properties of a 5% Cr tempered martensitic tool steel. Mater. Sci. Eng. A, 2004, 387–389, 171.

[12]

Elrakayby AM, Mills B. Identification of carbides in high-speed steels. J. Mater. Sci. Lett., 1986, 5, 332.

[13]

Abe F, Araki H, Noda T. The effect of tungsten on dislocation recovery and precipitation behavior of low-activation martensitic 9Cr steels. Metall. Trans. A, 1991, 22, 2225.

[14]

Pickering FB. Krauss G, Nordberg H. The properties of tool steels for mould and die applications. Tool Materials for Molds and Dies: Application and Performance, 1987, Colorado, CSM Press Golden, 3.

[15]

Dyson DJ, Andrews KW. Carbide M7C3 and its formation in alloy steels. J. Iron Steel Inst., 1969, 207(2): 208.

[16]

Kuo K. Carbides in chromium, molybdenum, and tungsten steels. J. Iron Steel Inst., 1953, 173, 363.

[17]

Wilson R. Metallurgy and Heat Treatment of Tool Steel, 1975, London, Mc Graw-Hill

[18]

Totten GE, Xie L, Funatani K. Handbook of Mechanical Alloy Design, 2004, New York, Marcel Dekker Inc

[19]

Karagoz S, Fischmeister H. Microstructure and toughness in high speed tool steels: the influence of hot reduction and austenitization temperature. Steel Res., 1987, 58(8): 353.

[20]

Podder A S, Bhadeshia HKDH. Thermal stability of austenite retained in bainitic steels. Mater. Sci. Eng. A, 2010, 527(7–8): 2121.

[21]

Cai GJ, Andren HO, Svensson LE. Microstructural change of a 5% Cr steel weld metal during tempering. Mater. Sci. Eng. A, 1998, 242(1–2): 202.

[22]

Baker RG, Nutting J. The tempering of 2.25Cr%-1%Mo steel after quenching and normalizing. J. Iron Steel Inst., 1959, 202, 257.

[23]

Bhadeshia HKDH, Honeycombe RWK. Steels: Microstructure and Properties, 2006, Oxford, Elsevier Ltd.

[24]

Bjärbo A, Hättestrand M. Complex carbide growth, dissolution and coarsening in a modified 12 pct chromium steel-an experimental and theoretical study. Metall. Mater. Trans. A, 2001, 32(1): 19.

[25]

Asakura K, Kohyama A, Yamada T. Mechanical properties and microstructure changes of low-activation 3Cr-2W-V-Ti ferritic steels developed for nuclear applications. ISIJ Int., 1990, 30(11): 947.

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