Microstructural evolution of ECAPed 1050 alloy under magnetic annealing

Yi-heng Cao , Pin-feng Jia , Kang Wang , Li-zi He , Ping Wang , Jian-zhong Cui

International Journal of Minerals, Metallurgy, and Materials ›› 2014, Vol. 21 ›› Issue (12) : 1205 -1214.

PDF
International Journal of Minerals, Metallurgy, and Materials ›› 2014, Vol. 21 ›› Issue (12) : 1205 -1214. DOI: 10.1007/s12613-014-1028-0
Article

Microstructural evolution of ECAPed 1050 alloy under magnetic annealing

Author information +
History +
PDF

Abstract

Hardness and microstructure evolutions in 1050 aluminum alloy prepared by equal-channel angular pressing (ECAP) were investigated by hardness testing, optical microscopy, and transmission electron microscopy after samples were annealed at different temperatures for 1 h both in the absence and presence of a 12-T magnetic field. The results showed that the hardness of samples after magnetic annealing were lower than that of samples after normal annealing at 150–250°C, but it was higher than that of samples after normal annealing at >250°C. During annealing, the rate of softening was faster, and the grains were more homogeneous in 8-ECAPed samples than in 2-ECAPed samples. A rapid grain growth occurred when 2-ECAPed samples were annealed at high temperature (≥300°C). The magnetic field enhanced the mobility of dislocations and grain boundaries. A more homogeneous grain size was observed in samples prepared under an applied magnetic field.

Keywords

aluminum alloys / magnetic annealing / equal channel angular pressing / microstructural evolution / grain growth

Cite this article

Download citation ▾
Yi-heng Cao, Pin-feng Jia, Kang Wang, Li-zi He, Ping Wang, Jian-zhong Cui. Microstructural evolution of ECAPed 1050 alloy under magnetic annealing. International Journal of Minerals, Metallurgy, and Materials, 2014, 21(12): 1205-1214 DOI:10.1007/s12613-014-1028-0

登录浏览全文

4963

注册一个新账户 忘记密码

References

[1]

Stolyarov VV, Zhu YT, Alexandrov IV, Lowe TC, Valiev RZ. Influence of ECAP routes on the microstructure and properties of pure Ti. Mater. Sci. Eng. A, 2001, 299(1–2): 59.

[2]

Makhlouf T, Rebhi A, Couzinié JP, Champion Y, Njah N. Microstructural evolution of a recycled aluminum alloy deformed by equal channel angular pressing process. Int. J. Miner. Metall. Mater., 2012, 19(11): 1016.

[3]

Singh D, Rao PN, Jayaganthan R. Microstructures and impact toughness behavior of Al 5083 alloy processed by cryorolling and afterwards annealing. Int. J. Miner. Metall. Mater., 2013, 20(8): 759.

[4]

Oh-Ishi K, Horita Z, Furukawa M, Nemoto M, Langdon TG. Optimizing the rotation conditions for grain refinement in equal-channel angular pressing. Metall. Mater. Trans. A, 1998, 29(7): 2011.

[5]

Furukawa M, Iwahashi Y, Horita Z, Nemoto M, Langdon TG. The shearing characteristics associated with equal-channel angular pressing. Mater. Sci. Eng. A, 1998, 257(2): 328.

[6]

Hosseini E, Kazeminezhad M. The effect of ECAP die shape on nano-structure of materials. Comput. Mater. Sci., 2009, 44(3): 962.

[7]

Hasegawa H, Komura S, Utsunomiya A, Horita Z, Furukawa M, Nemoto M, Langdon TG. Thermal stability of ultrafine-grained aluminum in the presence of Mg and Zr additions. Mater. Sci. Eng. A, 1999, 265(1–2): 188.

[8]

Sergueeva AV, Stolyarov VV, Valiev RZ, Mukherjee AK. Advanced mechanical properties of pure titanium with ultrafine grained structure. Scripta Mater., 2001, 45(7): 747.

[9]

Popov AA, Pyshmintsev IY, Demakov SL, Illarionov AG, Lowe TC, Sergeyeva AV, Valiev RZ. Structural and mechanical properties of nanocrystalline titanium processed by severe plastic deformation. Scripta Mater., 1997, 37(7): 1089.

[10]

Ferrasse S, Segal VM, Alford F. Texture evolution during equal channel angular extrusion (ECAE): Part II. An effect of post-deformation annealing. Mater. Sci. Eng. A, 2004, 372(1–2): 235.

[11]

Nemati J, Majzoobi GH, Sulaiman S, Baharudin BTHT, Hanim MAA. Improvements in the microstructure and fatigue behavior of pure copper using equal channel angular extrusion. Int. J. Miner. Metall. Mater., 2014, 21(6): 569.

[12]

Watanabe T, Fujii H, Oikawa H, Arai KI. Grain boundaries in rapidly solidified and annealed Fe-6.5 mass% Si polycrystalline ribbons with high ductility. Acta Metall., 1989, 37(3): 941.

[13]

Watanabe T, Tsurekawa S, Fujii H, Kanno T. The control of texture and grain boundary microstructure by magnetic annealing. Mater. Sci. Forum, 2005, 495–497, 1151.

[14]

Masahashi N, Matsuo M, Watanabe K. Development of preferred orientation in annealing of Fe-3.25% Si in a high magnetic field. J. Mater. Res., 1998, 13(2): 457.

[15]

Martikainen HO, Lindroos VK. Observations of the effect of magnetic field on the recrystallization in ferrite. Scand. J. Metall., 1981, 10(1): 3.

[16]

Watanabe T, Suzuki Y, Tanii S, Oikawa H. The effects of magnetic annealing on recrystallization and grain-boundary character distribution (GBCD) in iron-cobalt alloy polycrystals. Philos. Mag. Lett., 1990, 62(1): 9.

[17]

Wu Y, Zhao X, He CS, Zhang YD, Zuo L, Esling C. Effect of high magnetic field annealing on microstructure and texture at the initial stage of recrystallization in a cold-rolled interstitial-free steel. Mater. Trans., 2007, 48(11): 2809.

[18]

Bhaumik S, Molodova X, Molodov DA, Gottstein G. Magnetically enhanced recrystallization in an aluminum alloy. Scripta Mater., 2006, 55(11): 995.

[19]

Molodov DA, Bhaumik S, Molodova X, Gottstein G. Annealing behaviour of cold rolled aluminum alloy in a high magnetic field. Scripta Mater., 2006, 54(12): 2161.

[20]

Harada K, Tsurekawa S, Watanabe T, Palumbo G. Enhancement of homogeneity of grain boundary microstructure by magnetic annealing of electrodeposited nanocrystalline nickel. Scripta Mater., 2003, 49, 367.

[21]

Tsurekawa S, Kawahara K, Okamoto K, Watanabe T, Faulkner R. Application of magnetic field to the control of grain boundary segregation in iron. Mater. Sci. Eng. A, 2004, 387–389, 442.

[22]

Tsurekawa S, Okamoto K, Kawahara K, Watanabe T. The control of grain boundary segregation and segregation-induced brittleness in iron by the application of a magnetic field. J. Mater. Sci., 2005, 40(4): 895.

[23]

Ferrasse S, Segal VM, Hartwig KT, Goforth RE. Microstructure and properties of copper and aluminum alloy 3003 heavily worked by equal channel angular extrusion. Metall. Mater. Trans. A, 1997, 28(4): 1047.

[24]

Zheng LJ, Li HX, Hashmi MF, Chen CQ, Zhang Y, Zeng MG. Evolution of microstructure and strengthening of 7050 Al alloy by ECAP combined with heat-treatment. J. Mater. Process. Technol., 2006, 171(1): 100.

[25]

Humphreys FJ, Prangnell PB, Bowen JR, Gholinia A, Harris C. Developing stable fine-grain microstructures by large strain deformation. Philos. Trans. R. Soc. A, 1999, 357(1756): 1663.

[26]

Horita Z, Fujinami T, Nemoto M, Langdon TG. Equal-channel angular pressing of commercial aluminum alloys: grain refinement, thermal stability and tensile properties. Metall. Mater. Trans. A, 2000, 31(3): 691.

[27]

Klement U, Erb U, Ei-Sherik AM, Aust KT. Thermal stability of nanocrystalline Ni. Mater. Sci. Eng. A, 1995, 203(1–2): 177.

[28]

Wang ZC, Prangnell PB. Microstructure refinement and mechanical properties of severely deformed Al-Mg-Li alloys. Mater. Sci. Eng. A, 2002, 328(1–2): 87.

[29]

Hibbard GD, McCrea JL, Palumbo G, Aust KT, Erb U. An initial analysis of mechanisms leading to late stage abnormal grain growth in nanocrystalline Ni. Scripta Mater., 2002, 47(2): 83.

AI Summary AI Mindmap
PDF

96

Accesses

0

Citation

Detail

Sections
Recommended

AI思维导图

/