Pore-fracture response characteristics of coal under triaxial stress paths revealed by in-situ LF-NMR and fractal theory

Hexiang Xu , Cheng Zhai , Hongda Wen , Jizhao Xu , Yong Sun , Ting Liu , Shuang Li , Zhengzheng Tang , Bingyou Jiang , Bobo Li

Int J Min Sci Technol ›› 2026, Vol. 36 ›› Issue (8) : 1569 -1587.

PDF (10572KB)
Int J Min Sci Technol ›› 2026, Vol. 36 ›› Issue (8) :1569 -1587. DOI: 10.1016/j.ijmst.2026.06.004
Research Article
research-article
Pore-fracture response characteristics of coal under triaxial stress paths revealed by in-situ LF-NMR and fractal theory
Author information +
History +
PDF (10572KB)

Abstract

To investigate the evolution of pore-fracture structure (PFS) in coal under stress constraints, real-time nuclear magnetic resonance tests were conducted on coal samples subjected to four stress paths (SP-I to IV). The PFS evolution, fractal characteristics, failure morphology, and permeability contribution were analyzed using T2 spectra, nuclear magnetic resonance images (NMRIs), and fractal theory. The results show that stress paths significantly influence pore compaction, dilation, and fracture development. SP-III exhibits the most significant promotion of pore dilation before coal failure, followed by SP-IV and SP-II, whereas SP-I suppresses pore dilation. Confining pressure unloading promotes pore dilation, whereas the effect of axial loading depends on the confining pressure reduction. Coal failure significantly reduces pore heterogeneity, accompanied by a decrease in the pore fractal dimension (Db). Multifractal parameters Da and Ac were associated with pore compression, dilation and microfracture nucleation, while Hc served as a robust index of pore connectivity. The failure mode of SP-I was shear-dominant, while the remaining stress paths manifested a combined tensile-shear failure. The failure zone of SP-III exhibited the highest morphological complexity, followed by SP-IV, SP-II, and SP-I. The stress path significantly influenced the permeability contribution of PFS within the 100–1000 ms, highlighting distinct permeability responses under different stress paths. These findings provide valuable insights into the mechanisms governing gas migration in coal seams.

Keywords

In-situ LF-NMR / Triaxial stress path / Pore-fracture structure / Fractal dimension / Permeability contribution

Cite this article

Download citation ▾
Hexiang Xu, Cheng Zhai, Hongda Wen, Jizhao Xu, Yong Sun, Ting Liu, Shuang Li, Zhengzheng Tang, Bingyou Jiang, Bobo Li. Pore-fracture response characteristics of coal under triaxial stress paths revealed by in-situ LF-NMR and fractal theory. Int J Min Sci Technol, 2026, 36 (8) : 1569-1587 DOI:10.1016/j.ijmst.2026.06.004

登录浏览全文

4963

注册一个新账户 忘记密码

References

[1]

Karacan , Ruiz FA, Cotè M, Phipps S. Coal mine methane: a review of capture and utilization practices with benefits to mining safety and to greenhouse gas reduction. Int J Coal Geol 2011; 86(2—3):121-56.

[2]

Wang ZQ, Yuan L, Hu B, Li B, Huang LS. Quantitative calibration method for the evolution of mechanical properties of gas—containing coal under mining—induced stress and microscopic failure evaluation. Int J Min Sci Technol 2026; 36(3):475-97.

[3]

Zou MJ, Wei CT, Huang ZQ, Wei SM. Porosity type analysis and permeability model for micro—trans—pores, meso—macro—pores and cleats of coal samples. J Nat Gas Sci Eng 2015; 27:776-84.

[4]

Liu T, Lin BQ, Yang W, Liu T, Xiao W, Zha W. Study of effects of hard thick roof on gas migration and field experiment of roof artificially guided pre—splitting for efficient gas control. Nat Resour Res 2020; 29(3):1819-41.

[5]

He SQ, Ou SN, Lu Y, Jin LZ, Chen T, Ma YR. Failure mechanism of methane drainage borehole in soft coal seams: insights from simulation, theoretical analysis and in—borehole imaging. Process Saf Environ Prot 2022; 168:410-21.

[6]

Liu T, Lin BQ, Fu XH, Zhao Y, Gao YB, Yang W. Modeling coupled gas flow and geomechanics process in stimulated coal seam by hydraulic flushing. Int J Rock Mech Min Sci 2021; 142:104769.

[7]

Xie HP, Zhao XP, Liu JF, Zhang R, Xue DJ. Influence of different mining layouts on the mechanical properties of coal. Int J Min Sci Technol 2012; 22(6):749—55.

[8]

Zhang ZT, Zhang R, Xie HP, Gao MZ, Xie J. Mining—induced coal permeability change under different mining layouts. Rock Mech Rock Eng 2016; 49(9):3753—68.

[9]

Vishal V, Chandra D. Mechanical response and strain localization in coal under uniaxial loading, using digital volume correlation on X—ray tomography images. Int J Rock Mech Min Sci 2022; 154:105103.

[10]

Ju Y, Xi CD, Zhang Y, Mao LT, Gao F, Xie HP. Laboratory in situ CT observation of the evolution of 3D fracture networks in coal subjected to confining pressures and axial compressive loads: a novel approach. Rock Mech Rock Eng 2018; 51(11):3361—75.

[11]

Wang DK, Zeng FC, Wei JP, Zhang HT, Wu Y, Wei Q. Quantitative analysis of fracture dynamic evolution in coal subjected to uniaxial and triaxial compression loads based on industrial CT and fractal theory. J Petrol Sci Eng 2021; 196:108051.

[12]

Liu HZ, Mao LT, Ju Y, Hild F. Damage evolution in coal under different loading modes using advanced digital volume correlation based on X—ray computed tomography. Energy 2023; 275:127447.

[13]

Dang ZZ, Zhang B, Wang HP, Du QZ, Fan JG, Sui JC, et al. Experimental study of leakage characteristics and microscopic mechanisms in the sealing plug areas of underground compressed air energy storage caverns. Int J Min Sci Technol 2026; 36(5):997-1020.

[14]

Shi Y, Lin BQ, Liu T, Liu T, Zhang XL, Yang W. Study on the influence of stress constraint conditions on multi—scale gas emission characteristics in in—situ coal. Energy 2024; 290:130160.

[15]

Yu X, Xu HX, Zhai C, Regenauer—Lieb K, Sang SX, Sun Y, et al. Characterization of water migration behavior during spontaneous imbibition in coal: from the perspective of fractal theory and NMR. Fuel 2024; 355:129499.

[16]

Qin L, Zhai C, Liu SM, Xu JZ, Wu SJ, Dong RW. Fractal dimensions of low rank coal subjected to liquid nitrogen freeze—thaw based on nuclear magnetic resonance applied for coalbed methane recovery. Powder Technol 2018; 325:11-20.

[17]

Golsanami N, Sun JM, Liu Y, Yan WC, Lianjun C, Jiang LS, et al. Distinguishing fractures from matrix pores based on the practical application of rock physics inversion and NMR data: a case study from an unconventional coal reservoir in China. J Nat Gas Sci Eng 2019; 65:145—67.

[18]

Zhao Y, Wang CL, Ning L, Zhao HF, Bi J. Pore and fracture development in coal under stress conditions based on nuclear magnetic resonance and fractal theory. Fuel 2022; 309:122112.

[19]

Xu HX, Zhai C, Ranjith PG, Xu JZ, Wen HD, Liu T, et al. Pore—fracture evolution and fractal characteristics of coal under triaxial compression: insights from in—situ nuclear magnetic resonance. Int J Rock Mech Min Sci 2026; 204:106566.

[20]

Wang CL, Zhao Y, Ning L, Bi J. Permeability evolution of coal subjected to triaxial compression based on in—situ nuclear magnetic resonance. Int J Rock Mech Min Sci 2022; 159:105213.

[21]

Zhang SS, Wu CF, Fang XJ, Liu NN, Jiang XM, Han J. Mapping of stress sensitivity affected by water variation to microscopic pore distributions in medium— and high—rank coals. Nat Resour Res 2022; 31(3):1601-19.

[22]

Jia WH, Zhou HW, Xie SL, Wang YM, Hu XF, Zhang L. Pore—pressure and stress—coupled creep behavior in deep coal: insights from real—time NMR analysis. Int J Min Sci Technol 2024; 34(1):77-90.

[23]

Xie SL, Zhou HW, Jia WH, Gu YS, Cao YP, Liu ZL. Spatial evolution of pore and fracture structures in coal under unloading confining pressure: A stratified nuclear magnetic resonance approach. Energy 2024; 289:130083.

[24]

Sun Y, Zhai C, Zhao Y, Xu JZ, Cong YZ, Zheng YF, et al. Multifractal analysis and neural network prediction of pore structures in coal reservoirs based on NMR T2 spectra. Energy Fuels 2021; 35(14):11306—18.

[25]

Zhao Y, Lin BQ, Liu T, Zheng YN, Sun Y, Zhang GY, et al. Multifractal analysis of coal pore structure based on NMR experiment: a new method for predicting T2 cutoff value. Fuel 2021; 283:119338.

[26]

Zhang N, Wang XY, Wang SD, Wang RC, Wu JQ, Li Z, et al. Multifractal characteristics on pore structure of Longmaxi shale using nuclear magnetic resonance (NMR). Geoenergy Sci Eng 2024; 241:213176.

[27]

Zhang N, Guo SH, Wang SD, Tong YZ, Li Z, Wu JQ. Fractal and multifractal characteristics on pore structure of coal—based sedimentary rocks using nuclear magnetic resonance. SPE J 2024; 29(5):2624-37.

[28]

Liu T, Zhao Y, Kong XG, Lin BQ, Zou QL. Dynamics of coalbed methane emission from coal cores under various stress paths and its application in gas extraction in mining—disturbed coal seam. J Nat Gas Sci Eng 2022; 104:104677.

[29]

Yao YB, Liu DM, Che Y, Tang DZ, Tang SH, Huang WH. Petrophysical characterization of coals by low—field nuclear magnetic resonance (NMR). Fuel 2010; 89(7):1371—80.

[30]

Civan F. Stress—dependent porosity and permeability of porous rocks represented by a mechanistic elastic cylindrical pore—shell model. Transp Porous Medium 2019; 129(3):885-99.

[31]

Yu BM. Analysis of flow in fractal porous media. Appl Mech Rev 2008; 61(5):050801.

[32]

Yu BM, Cheng P. A fractal permeability model for bi—dispersed porous media. Int J Heat Mass Transf 2002; 45(14):2983—93.

[33]

Fan YR, Liu JY, Ge XM, Deng SG, Liu HL, Gu DN. Permeability evaluation of tight sandstone based on dual T2 cutoff values measured by NMR. Chin J Geophys 2018; 61(4):1628—38.in Chinese.

[34]

Zhao PQ, Wang XX, Cai JC, Luo M, Zhang J, Liu YM, et al. Multifractal analysis of pore structure of Middle Bakken formation using low temperature N2 adsorption and NMR measurements. J Petrol Sci Eng 2019; 176:312—20.

[35]

Halsey TC, Jensen MH, Kadanoff LP, Procaccia I, Shraiman BI. Fractal measures and their singularities: the characterization of strange sets. Nucl Phys B Proc Suppl 1987; 2:501—11.

[36]

Ferreiro JP, Vidal VE. Multifractal analysis of Hg pore size distributions in soils with contrasting structural stability. Geoderma 2010; 160(1):64-73.

[37]

Halsey TC, Jensen MH, Kadanoff LP, Procaccia I, Shraiman BI. Fractal measures and their singularities: the characterization of strange sets. Phys Rev A 1986; 33(2):1141-51.

[38]

Timur A. Pulsed nuclear magnetic resonance studies of porosity, movable fluid, and permeability of sandstones. J Petrol Technol 1969; 21(6):775-86.

[39]

Yao YB, Liu DM, Liu JG, Xie SB. Assessing the water migration and permeability of large intact bituminous and anthracite coals using NMR relaxation spectrometry. Transp Porous Med 2015; 107(2):527—42.

[40]

Cheng GX, Jiang B, Li M, Li FL, Xu SC. Quantitative characterization of fracture structure in coal based on image processing and multifractal theory. Int J Coal Geol 2020; 228:103566.

PDF (10572KB)

0

Accesses

0

Citation

Detail

Sections
Recommended

/