Micromechanical properties of granite with insights into mineral interface mechanics

Pengli Zhou , Cunbao Li , Heping Xie

Int J Min Sci Technol ›› 2025, Vol. 35 ›› Issue (9) : 1419 -1437.

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Int J Min Sci Technol ›› 2025, Vol. 35 ›› Issue (9) :1419 -1437. DOI: 10.1016/j.ijmst.2025.08.009
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Micromechanical properties of granite with insights into mineral interface mechanics
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Abstract

Understanding the mechanical behavior of diagenetic mineral granules and interfaces in granite provides essential experimental references for constructing micromechanical models of granite. The micromechanical behavior of Yanshanian granite is investigated using scanning electron microscopy-energy dispersive spectroscopy (SEM-EDS) and nanoindentation tests. The results demonstrate transitional mechanical properties at mineral interfaces. The elastic modulus and hardness exhibit intermediate values between adjacent mineral phases. The higher plasticity indices at the interfaces suggest higher plastic deformation capacity of hard-phase minerals in these regions. Additionally, fracture toughness measurements of minerals and interfaces were obtained, with interfacial values ranging from 0.90 to 1.63 MPa·m0.5. The analysis of mechanical property relationships shows a significant positive linear correlation between rock-scale elastic modulus and fracture toughness. However, this correlation is substantially lower at the mineral scale, demonstrating a scale effect in the relationship of different mechanical properties.

Keywords

Nanoindentation / Interface mechanics / Micro-mesoscale mechanics / Elasto-plastic deformation / Fracture morphology

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Pengli Zhou, Cunbao Li, Heping Xie. Micromechanical properties of granite with insights into mineral interface mechanics. Int J Min Sci Technol, 2025, 35(9): 1419-1437 DOI:10.1016/j.ijmst.2025.08.009

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Acknowledgement

This study was funded by the National Natural Science Founda-tion of China (Nos. 52422403 and U22A20166), the Deep Earth Probe and Mineral Resources Exploration-National Science and Technology Major Project (No. 2024ZD1003903), the Department of Science and Technology of Guangdong Province (No. 2019ZT08G315), and Guangdong Basic and Applied Basic Research Foundation (No. 2023A1515012654).

Supplementary material

Supplementary data to this article can be found online at https://doi.org/10.1016/j.ijmst.2025.08.009.

References

[1]

Xie HP, Li CB, Zhou T, Chen JL, Liao JX, Ma JC, Li BX. Conceptualization and evaluation of the exploration and utilization of low/medium-temperature geothermal energy: a case study of the Guangdong-Hong Kong-Macao Greater Bay Area. Geomech Geophys Geo-energ Geo-resour 2020; 6:18.

[2]

Qiao MZ, Jing ZF, Feng CC, Li MH, Chen C, Zou XP, Zhou YJ. Review on heat extraction systems of hot dry rock: Classifications, benefits, limitations, research status and future prospects. Renew Sustain Energy Rev 2024; 196:19.

[3]

Dong LJ, Zhang YH, Wang LC, Wang L, Zhang S. Temperature dependence of mechanical properties and damage evolution of hot dry rocks under rapid cooling. J Rock Mech Geotech Eng 2024; 16(2):645-60.

[4]

Espinoza WF, Pereira JM, Kneafsey T, Dai S. Mechanical and creep properties of granitic minerals of albite, biotite, and quartz at elevated temperature. Geomech Energy Environ 2023; 34:100465.

[5]

Li YH, Xie HP, Zhang R, Zhang ZT, Zhang ZL, Gao H, Huang W, Zhang JX, Gao JM, Ma X, Xu RB. Design and development of the deep-rock in situ condition-preserved coring calibration platform. Int J Min Sci Technol 2023; 33 (11):1377-95.

[6]

Sun CL, Li GC, Gomah ME, Xu JH, Sun YT. Creep characteristics of coal and rock investigated by nanoindentation. Int J Min Sci Technol 2020; 30(6):769-76.

[7]

Ma ZY, Zhang CP, Pathegama Gamage R, Zhang GL. Uncovering the creep deformation mechanism of rock-forming minerals using nanoindentation. Int J Min Sci Technol 2022; 32(2):283-94.

[8]

Liu YW, Zhang GP, Qiao JM, Tang XH. Micromechanical testing and property upscaling of planetary rocks: a critical review. Int J Min Sci Technol 2024; 34 (9):1217-41.

[9]

Yin SH, Wang YJ, Liu JG. Predicting the probability distribution of Martian rocks mechanical property based on microscale rock mechanical experiments and accurate grain-based modeling. Int J Min Sci Technol 2024; 34(9):1327-39.

[10]

Bennett KC, Berla LA, Nix WD, Borja RI. Instrumented nanoindentation and 3D mechanistic modeling of a shale at multiple scales. Acta Geotech 2015; 10 (1):1-14.

[11]

Kumar V, Curtis ME, Gupta N, Sondergeld CH, Rai CS. Estimation of Elastic Properties of Organic Matter and Woodford Shale Through Nano-indentation Measurements. In: Canadian Unconventional Resources Conference SPE. Calgary: SPE; 2012.

[12]

Mondol NH, Jahren J, Bjørlykke K, Brevik I. Elastic properties of clay minerals. Lead Edge 2008; 27(6):758-70.

[13]

Liu KQ, Ostadhassan M. Microstructural and geomechanical analysis of Bakken shale at nanoscale. J Petrol Sci Eng 2017; 153:133-44.

[14]

Akono AT, Dávila G, Druhan J, Shi ZF, Jessen K, Tsotsis T. Influence of geochemical reactions on the creep behavior of Mt. Simon sandstone. Int J Greenh Gas Contr 2020; 103:103183.

[15]

Borodich FM, Bull SJ, Epshtein SA. Nanoindentation in studying mechanical properties of heterogeneous materials. J Min Sci 2015; 51(3):470-6.

[16]

Kossovich E, Epshtein S, Dobryakova N, Minin M, Gavrilova D. Mechanical properties of thin films of coals by nanoindentation. In:Physical and Mathematical Modeling of Earth and Environment Processes. Cham: Springer International Publishing; 2018. p. 45-50.

[17]

Xie HP, Yang ZK, Deng JH. Assessment of geothermal resource potential in the Guangdong-Hong Kong-Macao greater bay area. Adv Eng Sci 2019; 51(1):1-8. In Chinese.

[18]

Zakira U, Bajpayee A, Pharr M, Banerjee S, Birgisson B. Grid nanoindentation on calcium sulfoaluminate (CSA)-Kaolinite pastes. Constr Build Mater 2022; 335:127523.

[19]

Du JT, Luo SM, Hu LM, Guo B, Guo DD, Zhang GP. Multiscale mechanical properties of shales: grid nanoindentation and statistical analytics. Acta Geotech 2022; 17(2):339-54.

[20]

Oliver WC, Pharr GM. An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments. J Mater Res 1992; 7(6):1564-83.

[21]

Liu XY, Xu DP, Li SJ, Qiu SL, Jiang Q. An insight into the mechanical and fracture characterization of minerals and mineral interfaces in granite using nanoindentation and micro X-ray computed tomography. Rock Mech Rock Eng 2023; 56(5):3359-75.

[22]

Tang XH, Zhang YH, Xu JJ, Rutqvist J, Hu MS, Wang ZZ, Liu QS. Determining Young’s modulus of granite using accurate grain-based modeling with microscale rock mechanical experiments. Int J Rock Mech Min Sci 2022; 157:105167.

[23]

Mikowski A, Soares P, Wypych F, Lepienski CM. Fracture toughness, hardness, and elastic modulus of kyanite investigated by a depth-sensing indentation technique. Am Min 2008;93(5-6):844-52.

[24]

Nasseri MHB, Rezanezhad F, Young RP. Analysis of fracture damage zone in anisotropic granitic rock using 3D X-ray CT scanning techniques. Int J Fract 2011; 168(1):1-13.

[25]

Fujii Y, Takemura T, Takahashi M, Lin WR. Surface features of uniaxial tensile fractures and their relation to rock anisotropy in Inada granite. Int J Rock Mech Min Sci 2007; 44(1):98-107.

[26]

Liu L, Du GY, Li EB, Guo Q, Xia H.Fracture mechanical behaviors and acoustic emission characteristics of Beishan granite under CCNBD test. Chin J Rock Mech Eng 2020; 39:3237-44.

[27]

Wang YS, Hu XZ. Determination of tensile strength and fracture toughness of granite using notched three-point-bend samples. Rock Mech Rock Eng 2017; 50(1):17-28.

[28]

Mahabadi O. Investigating the influence of micro-scale heterogeneity and microstructure on the failure and mechanical behaviour of geomaterials. Doctoral dissertation. Canada: University of Toronto; 2012.

[29]

Jeong SS, Nakamura K, Yoshioka S, Obara Y, Kataoka M. Fracture toughness of granite measured using micro to macro scale specimens. Procedia Eng 2017; 191:761-7.

[30]

Sebastiani M, Johanns KE, Herbert EG, Pharr GM. Measurement of fracture toughness by nanoindentation methods: recent advances and future challenges. Curr Opin Solid State Mater Sci 2015; 19(6):324-33.

[31]

Mahabadi OK, Tatone BSA, Grasselli G. Influence of microscale heterogeneity and microstructure on the tensile behavior of crystalline rocks. J Geophys Res Solid Earth 2014; 119(7):5324-41.

[32]

Liu KQ, Ostadhassan M, Bubach B. Applications of nano-indentation methods to estimate nanoscale mechanical properties of shale reservoir rocks. J Nat Gas Sci Eng 2016; 35:1310-9.

[33]

Du JT, Whittle AJ, Hu LM, Divoux T, Meegoda JN. Characterization of meso-scale mechanical properties of Longmaxi shale using grid microindentation experiments. J Rock Mech Geotech Eng 2021; 13(3):555-67.

[34]

Ma XY, Kang X, Cao JW. Origin of the elastic anisotropy of silica particles: Insights from first-principles calculations and nanoindentation molecular dynamic simulations. Comput Geotech 2023; 159:105489.

[35]

Peng L, Li XL, Peng X, Gan YC, Wang JG. Analysis of physical and mechanical behaviors and microscopic mineral characteristics of thermally damaged granite. Sci Rep 2024; 14(1):14776.

[36]

Mukherjee R, Misra S. Nanomechanics of minerals: Understandings and developments through instrumented nanoindentation techniques. Phys Chem Miner 2023; 50(1):10.

[37]

Zhang QS, Liu ZB, Tang YS, Deng YF, Luo TY, Wang YT. Mechanical property characterization of mudstone based on nanoindentation technique combined with upscaling method. Environ Earth Sci 2023; 82(21):485.

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