Role of grain size in governing the mechanical response in friction-stir-welded high-aluminum low-density ferrite steel

Junqi Chen , Takuya Miura , Kohsaku Ushioda , Abhishek Sharma , Hidetoshi Fujii

International Journal of Minerals, Metallurgy and Materials ›› 2026, Vol. 33 ›› Issue (9) : 3002 -3014.

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International Journal of Minerals, Metallurgy and Materials ›› 2026, Vol. 33 ›› Issue (9) :3002 -3014. DOI: 10.1007/s12613-025-3324-2
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Role of grain size in governing the mechanical response in friction-stir-welded high-aluminum low-density ferrite steel
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Abstract

The susceptibility of high-Al ferritic steels to thermal cracking and microstructural coarsening during fusion welding restricts their practical implementation. To address this challenge, high-quality joints of Fe–10Al alloy were successfully fabricated by friction stir welding (FSW) under ultra-low rotation (80 r/min) and high load (40 kN) at sub-700°C. The effects of the unique thermomechanical conditions, combined with post-weld heat treatments, on microstructural evolution and mechanical performance were systematically examined. Grain refinement (∼6 µm) was found to markedly enhance ductility and toughness. The Fe–10Al alloy exhibited a local elongation (L-El) of 28%, surpassing previously reported values, while the ductile-to-brittle transition temperature was −15°C and the upper shelf energy increased to 402 kJ/m2, both due to improved crack propagation resistance. Grain refinement also shifted the dominant deformation mode from twinning to dislocation slip and raised the fraction of “effective grains” with high-angle boundaries (15°–65°) to ∼64%. These findings demonstrate that FSW provides an effective strategy to overcome weldability issues in high-Al ferritic steels, offering a pathway to their broader structural applications.

Keywords

friction stir welding / Fe–10Al / grain size / tensile properties / Charpy impact toughness / deformation mechanism

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Junqi Chen, Takuya Miura, Kohsaku Ushioda, Abhishek Sharma, Hidetoshi Fujii. Role of grain size in governing the mechanical response in friction-stir-welded high-aluminum low-density ferrite steel. International Journal of Minerals, Metallurgy and Materials, 2026, 33 (9) : 3002-3014 DOI:10.1007/s12613-025-3324-2

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References

[1]

Rana R, Liu C, Ray RK. Low-density low-carbon Fe–Al ferritic steels. Scripta Mater., 2013, 686354.

[2]

F. Czerwinski, Current trends in automotive lightweighting strategies and materials, Materials, 14(2021), No. 21, art. No. 6631.

[3]

Frommeyer G, Drewes EJ, Engl B. Physical and mechanical properties of iron-aluminium-(Mn, Si) lightweight steels. Metall. Res. Technol., 2000, 97101245

[4]

Lehnhoff GR, Findley KO, De Cooman BC. The influence of silicon and aluminum alloying on the lattice parameter and stacking fault energy of austenitic steel. Scripta Mater., 2014, 92: 19.

[5]

X.Y. Xu, J.Z. Li, W.J. Li, et al., Experimental and theoretical study on static recrystallization of a low-density ferritic steel containing 4 mass% aluminum, Mater. Des., 180(2019), art. No. 107924.

[6]

Satya Prasad VV, Khaple S, Baligidad RG. Melting, processing, and properties of disordered Fe–Al and Fe–Al–C based alloys. JOM, 2014, 6691785.

[7]

Doi T, Kitamura K, Nakanishi K, et al. Characterization of rust layers formed on Al-bearing steels exposed to coastal environments. J. Jpn. Inst. Met., 2010, 74110.

[8]

Frommeyer G, Habrock HJ, Wittig JE, von Czarnowski P, Geenen J, Kreuss M. Investigations on phase transformations and B2-DO3 superlattices in ordered iron aluminium alloys by FIM: Atom probe and TEM. Scr. Mater., 1990, 24151.

[9]

B.C. Maji, S. Ukai, and N. Oono-Hori, Microstructural stability and intermetallic embrittlement in high Al containing FeCrAlODS alloys, Mater. Sci. Eng. A, 807(2021), art. No. 140858.

[10]

Morris DG, Gunther S. Order-disorder changes in Fe3Al based alloys and the development of an iron-base α-α” superalloy. Acta Mater., 1996, 4472847.

[11]

J.Q. Chen, T. Miura, K. Ushioda, A. Sharma, and H. Fujii, Elucidating the role of ordered phases and carbides in the mechanical performance of friction stir welded high aluminum low-density ferrite steels, J. Mater. Process. Technol., 343(2025), art. No. 118959.

[12]

Liu HB, Wu CH, Xie RS, et al. Interface optimization design and bonding mechanism of friction rolling additive manufactured aluminum/steel dissimilar metal. J. Manuf. Process., 2024, 132: 1041.

[13]

Stoloff NS. Iron aluminides: Present status and future prospects. Mater. Sci. Eng. A, 1998, 2581–21.

[14]

Huang YW, Tung PC, Wu CY. Tuning PID control of an automatic arc welding system using a SMAW process. Int. J. Adv. Manuf. Technol., 2007, 341–256.

[15]

Tjong SC, Zhu SM, Ho NJ, Ku JS. Solidification microstructure and creep rupture behaviour of electron beam welded austenitic Fe–28M–6Al–1C alloy. Mater. Sci. Technol., 1997, 133251.

[16]

Liu HB, Hou R, Wu CH, Xie RS, Chen SJ. Multi-layer multi-pass friction rolling additive manufacturing of Al alloy: Toward complex large-scale high-performance components. Int. J. Miner. Metall. Mater., 2025, 322425.

[17]

J.L. Zhang, H.J. Zhang, X. Chen, Z.L. Li, and G.S. Huang, Microstructural mechanisms and mechanical behavior of friction-stir-welded Mg alloy laminate joints, J. Mater. Process. Technol., 338(2025), art. No. 118779.

[18]

Shen YJ, Wang JJ, Wang BB, et al. Strengthening strategy for high-performance friction stir lap welded joints based on 5083 Al alloy. Int. J. Miner. Metall. Mater., 2024, 31112498.

[19]

Wang ZW, Zhang M, Li C, et al. Achieving a high-strength dissimilar joint of T91 heat-resistant steel to 316L stainless steel via friction stir welding. Int. J. Miner. Metall. Mater., 2023, 301166.

[20]

Xie GM, Duan RH, Wang YQ, Luo ZA, Wang GD. Microstructure and toughness of thick-gauge pipeline steel joint via double-sided friction stir welding combined with preheating. Int. J. Miner. Metall. Mater., 2023, 304724.

[21]

J.Q. Chen, T. Miura, K. Ushioda, and H. Fujii, Effects of microstructure and phosphorus segregation on tensile properties of friction stir welded high phosphorus weathering steel, Mater. Sci. Eng. A, 916(2024), art. No. 147315.

[22]

Sun YY, Liu HB, Xie RS, Chen Y, Chen SJ. Heat-balance control of friction rolling additive manufacturing based on combination of plasma preheating and instant water cooling. J. Mater. Sci. Technol., 2025, 205: 168.

[23]

Chen JQ, Miura T, Ushioda K, Fujii H. Microstructures and mechanical properties of FSWed Fe–xAl and Fe–0.1C–xAl alloys. J. Mater. Res. Technol., 2025, 36: 888.

[24]

Herrmann J, Inden G, Sauthoff G. Deformation behaviour of iron-rich iron-aluminum alloys at low temperatures. Acta Mater., 2003, 51102847.

[25]

Khaple S, Golla BR, Prasad VVS. A review on the current status of Fe–Al based ferritic lightweight steel. Def. Technol., 2023, 26: 1.

[26]

Naik SN, Walley SM. The Hall–Petch and inverse Hall–Petch relations and the hardness of nanocrystalline metals. J. Mater. Sci., 2020, 5572661.

[27]

Chen SP, Rana R, Haldar A, Ray RK. Current state of Fe–Mn–Al–C low density steels. Prog. Mater. Sci., 2017, 89: 345.

[28]

Honda R. Cleavage fracture in single crystals of silicon iron. J. Phys. Soc. Jpn., 1961, 1671309.

[29]

Garrison WM, Moody NR. Ductile fracture. J. Phys. Chem. Solids, 1987, 48111035.

[30]

Pineau A, Benzerga AA, Pardoen T. Failure of metals I: Brittle and ductile fracture. Acta Mater., 2016, 107: 424.

[31]

Meyers MA, Vöhringer O, Lubarda VA. The onset of twinning in metals: A constitutive description. Acta Mater., 2001, 49194025.

[32]

Reid CN. A review of mechanical twinning in body-centred cubic metals and its relation to brittle fracture. J. Less-Common Met., 1965, 92105.

[33]

T. Kawakubo, K. Ushioda, and H. Fujii, Grain boundary segregation and toughness of friction-stir-welded high-phosphorus weathering steel, Mater. Sci. Eng. A, 832(2022), art. No. 142350.

[34]

Takebe H, Ushioda K. Effects of grain size, thickness and tensile direction on ductility of pure titanium sheet. Mater. Trans., 2021, 627952.

[35]

Miyazaki S, Shibata K, Fujita H. Effect of specimen thickness on mechanical properties of polycrystalline aggregates with various grain sizes. Acta Metall., 1979, 275855.

[36]

Christian JW, Mahajan S. Deformation twinning. Prog. Mater. Sci., 1995, 391–21.

[37]

Y.T. Yang, J.Y. Pang, H.W. Zhang, et al., Ultrahigh strength and exceptional work hardening in a hierarchical-structured alloy via hetero-interface-mediated twinning, Adv. Sci., 12(2025), No. 38, art. No. e09584.

[38]

Higashida K, Tanaka M. Mechanism behind brittle-to-ductile transition understood by the interaction between a crack and dislocations. ISIJ Int., 2012, 524704.

[39]

K. Higashida, S. Sadamatsu, and M. Tanaka, High-voltage electron microscopy analyses for crack-tip dislocations and their shielding effect on fracture toughness in MgO and Si crystals, J Am Ceram Soc., 108(2025), No. 6, art. No. e20378.

[40]

Qin XM, Chen LQ, Deng W, Di HS. Effect of strain rate on mechanical properties of Fe–23Mn–2Al–0.2C TWIP steel. Chin. J. Mater. Res., 2011, 253278

[41]

Kim MC, Oh YJ, Hong JH. Characterization of boundaries and determination of effective grain size in Mn–Mo–Ni low alloy steel from the view of misorientation. Scripta Mater., 2000, 433205.

[42]

Bhattacharjee D, Davis CL. Influence of processing history on mesotexture and microstructure-toughness relationship in control-rolled and normalised steels. Scripta Mater., 2002, 4712825.

[43]

Wu SJ, Davis CL. Investigation of the microstructure and mesotexture formed during thermomechanical controlled rolling in microalloyed steels. J. Microsc., 2004, 2133262.

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