Synthesis of new complex salt crystal K[InCl]

Front. Chem. China ›› 2008, Vol. 3 ›› Issue (2) : 125 -127.

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Front. Chem. China ›› 2008, Vol. 3 ›› Issue (2) : 125 -127. DOI: 10.1007/s11458-008-0023-2

Synthesis of new complex salt crystal K[InCl]

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Abstract

During the experiment of preparing ITO (Indium Tin Oxide) nanopowder, a new complex salt crystal K3[InCl6] was found and synthesized using a solution growth method. The diffraction pattern, morphology, element composition and structure of the crystal were analyzed by XRD, SEM and CCD. The results implied that K3[InCl6] is monoclinic, is of the space group P21/c, has a chemical formula of K3[InCl6], a Z = 4 and with the following cell parameters: a = 12.188 Å, b = 7.553 Å, c = 12.703 Å, ? = 90.00°, ? = 108.96°, ? = 90.00°, V = 1105.98 Å3.

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null. Synthesis of new complex salt crystal K[InCl]. Front. Chem. China, 2008, 3(2): 125-127 DOI:10.1007/s11458-008-0023-2

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