Influence of water content on the failure modes and macro-micromechanical properties of sulfate rocks: Insights from experimental and DEM simulations

Li Yu , Youlin Qin , Hualao Wang , Mingnian Wang , Zhaohui Chen , Mingyang Yu , Hong Jin

Underground Space ›› 2025, Vol. 25 ›› Issue (6) : 387 -409.

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Underground Space ›› 2025, Vol. 25 ›› Issue (6) :387 -409. DOI: 10.1016/j.undsp.2025.06.005
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Influence of water content on the failure modes and macro-micromechanical properties of sulfate rocks: Insights from experimental and DEM simulations
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Abstract

The initial water content significantly affects rock mechanics, especially with swelling minerals. However, the effects of initial water content on the mechanical properties and failure mode of sulfate rocks remain unclear. This study explores these effects by conducting unconfined compressive strength (UCS) experiments and discrete element method simulations on sulfate rocks. The results indicate that as the initial water content increased from 0 to 9%, the Young’s modulus and Poisson’s ratio of sulfate rock exponentially decreased by 48.9% and 290%, respectively. Additionally, the crack initiation stress ($\sigma _{ci}$), crack damage stress ($\sigma _{cd}$), and UCS decreased by 62.4%, 51.5%, and 53.3%, respectively. The stress responses to initial water content follow linear functions. Notable decreases were also observed in the normal and shear stiffness parameters ($k_n$ and $k_s$ of contact, diminishing by 46.53% and 46.54%, respectively; peak cohesion decreased by 69.70%; peak friction angle by 17.39%; peak tensile strength by 124%. Rising initial water content leads to increased damage and softening of sulfate rock, causing decreased mechanical properties. It can be observed that as the initial water content increases, the proportion of micro-tensile fractures in the total number of fractures increases, and the dominant failure mode of sulfate rock gradually transitions from shear to tensile failure.

Keywords

Sulfate rock / Anhydrite / Initial water content / Failure model / 3DEC-GBM

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Li Yu, Youlin Qin, Hualao Wang, Mingnian Wang, Zhaohui Chen, Mingyang Yu, Hong Jin. Influence of water content on the failure modes and macro-micromechanical properties of sulfate rocks: Insights from experimental and DEM simulations. Underground Space, 2025, 25(6): 387-409 DOI:10.1016/j.undsp.2025.06.005

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Data availability

The data that support the findings of this study are available from the corresponding author upon reasonable request.

CRediT authorship contribution statement

Li Yu: Writing - original draft, Formal analysis, Methodology, Investigation. Youlin Qin: Methodology, Investigation, Writing - review & editing, Formal analysis. Hualao Wang: Funding acquisition, Formal analysis, Writing - review & editing. Mingnian Wang: Supervision, Methodology, Writing - review & editing. Zhaohui Chen: Software, Investigation. Mingyang Yu: Writing - review & editing, Visualization, Data curation. Hong Jin: Writing - original draft, Investigation.

Declaration of competing interest

The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.

Acknowledgement

This work was supported by the Special Science and Technology Innovation fund of Research Institute of Highway, Ministry of Transport of the People's Republic of China (Grant No. 2019-C505).

References

[1]

Alejano, L. R., Arzúa, J., Bozorgzadeh, N., & Harrison, J. P. (2017). Triaxial strength and deformability of intact and increasingly jointed granite samples. International Journal of Rock Mechanics and Mining Sciences, 95, 87-103.

[2]

Alonso, E., Berdugo, I., & Ramon, A. (2013). Extreme expansive phenomena in anhydritic-gypsiferous claystone: The case of Lilla tunnel. Géotechnique, 63(7), 584-612.

[3]

Alonso, E., & Ramon, A. (2013). Heave of a railway bridge induced by gypsum crystal growth: Field observations. Géotechnique, 63(10), 894.

[4]

Azocar, K. D. (2016). Investigating the mesh dependency and upscaling of 3D grain-based models for the simulation of brittle fracture processes in low-porosity crystalline rock. Queen’s University (Canada), Doctoral dissertation.

[5]

Bornert, M., Vales, F., Gharbi, H., & Nguyen Minh, D. (2010). Multiscale full-field strain measurements for micromechanical investigations of the hydromechanical behaviour of clayey rocks. Strain, 46(1), 33-46.

[6]

Butscher, C., Breuer, S., & Blum, P. (2018). Swelling laws for clay-sulfate rocks revisited. Bulletin of Engineering Geology and the Environment, 77, 399-408.

[7]

Butscher, C., Einstein, H. H., & Huggenberger, P. (2011). Effects of tunneling on groundwater flow and swelling of clay-sulfate rocks. Water Resources Research, 47(11), W11520.

[8]

Butscher, C., Mutschler, T., & Blum, P. (2016). Swelling of clay-sulfate rocks: A review of processes and controls. Rock Mechanics and Rock Engineering, 49(4), 1533-1549.

[9]

Cherblanc, F., Berthonneau, J., Bromblet, P., & Huon, V. (2016). Influence of water content on the mechanical behaviour of limestone: Role of the clay minerals content. Rock Mechanics and Rock Engineering, 49(6), 2033-2042.

[10]

Farahmand, K., Vazaios, I., Diederichs, M. S., & Vlachopoulos, N. J. (2018). Investigating the scale-dependency of the geometrical and mechanical properties of a moderately jointed rock using a synthetic rock mass (SRM) approach. Geotechnics, 95, 162-179.

[11]

Gao, F., Stead, D., & Elmo, D. (2016). Numerical simulation of microstructure of brittle rock using a grain-breakable distinct element grain-based model. Geotechnics, 78, 203-217.

[12]

Gao, H., Liang, W. G., Yang, X., Zhang, C., Yue, G., & Zhang, P. (2011). Experimental study of mechanical property of gypsum rock soaked in hot saturated brine. Chinese Journal of Rock Mechanics and Engineering, 30, 935-943 (in Chinese).

[13]

Ghazvinian, E., Diederichs, M. S., & Quey, R. (2014). 3D random Voronoi grain-based models for simulation of brittle rock damage and fabric-guided micro-fracturing. Journal of Rock Mechanics and Geotechnical Engineering, 6(6), 506-521.

[14]

He, H., & Ahrens, T. J. (1994). Mechanical properties of shock-damaged rocks. International Journal of Rock Mechanics and Mining Sciences, 31(5), 525-533.

[15]

Huang, D., Tang, W., & Li, X. (2023). Numerical modeling and damage evolution research on the effect of joint geometrical parameters in nonpersistent jointed rock masses. Bulletin of Engineering Geology and the Environment, 82(4), 137.

[16]

Hu, D. W., Zhang, F., Shao, J. F., & Gatmiri, B. (2014). Influences of mineralogy and water content on the mechanical properties of argillite. Rock Mechanics and Rock Engineering, 47(1), 157-166.

[17]

Inga, C. E. C., Sinha, S., Walton, G., & Holley, E. (2023). Modeling Brazilian tensile strength tests on a brittle rock using deterministic, semi-deterministic, and Voronoi bonded block models. Rock Mechanics and Rock Engineering, 56(7), 5293-5313.

[18]

Itasca Consulting Group Inc. (2025). Three-dimensional Distinct Element Code (Version 9.1).

[19]

Kanit, T., Forest, S., Galliet, I., Mounoury, V., & Jeulin, D. (2003). Determination of the size of the representative volume element for random composites: Statistical and numerical approach. Journal of the Mechanics and Physics of Solids, 40, 3647-3679.

[20]

Kazerani, T., & Zhao, J. (2010). Micromechanical parameters in bonded particle method for modelling of brittle material failure. International Journal for Numerical and Analytical Methods in Geomechanics, 34(18), 1877-1895.

[21]

Lee, D. T., & Schachter, B. J. (1980). Two algorithms for constructing a delaunay triangulation. International Journal of Computer & Information Sciences, 9(3), 219-242.

[22]

Lemaitre, J. (2013). A course on damage mechanics. Springer Science and Business Media.

[23]

Li, Z. C., Zhu, Y., Zhou, H., & Li, J. (2022). Equivalent simulation method of humidity and temperature expansion for subway tunnels in swelling rock considering elastic softening. Rock and Soil Mechanics, 43, 497-507 (in Chinese).

[24]

Li, X. F., Li, H. B., Liu, L. W., Liu, Y. Q., Ju, M. H., & Zhao, J. (2020). Investigating the crack initiation and propagation mechanism in brittle rocks using grain-based finite-discrete element method. International Journal of Rock Mechanics and Mining Sciences, 127, 104219.

[25]

Li, X. F., Li, H. B., & Zhao, J. (2019). The role of transgranular capability in grain-based modelling of crystalline rocks. Computers and Geotechnics, 110, 161-183.

[26]

Liu, C. D., Cheng, Y., Jiao, Y. Y., Zhang, G.-H., Zhang, W. S., Ou, G. Z., & Tan, F. (2021). Experimental study on the effect of water on mechanical properties of swelling mudstone. Engineering Geology, 295, 106448.

[27]

Liu, Y., Yu, H., Wang, C., & Wang, C. (2011). Research on mechanism of damage of anhydrock in dolomite layer to tunnel structure. Rock and Soil Mechanics, 32, 2704-2708 (in Chinese).

[28]

Madsen, F., & Nüesch, R. (1991). The swelling behaviour of clay-sulfate rocks. Proceedings of the ISRM Congress. ISRM.

[29]

Mardalizad, A., Scazzosi, R., Manes, A., & Giglio, M. (2018). Testing and numerical simulation of a medium strength rock material under unconfined compression loading. Journal of Rock Mechanics and Geotechnical Engineering, 10(2), 197-211.

[30]

Maximiliano, R. V., & Triantafyllidis, T. (2016). Influence of initial water content on the mechanical properties of an argillaceous swelling rock. Rock Mechanics and Rock Engineering, 49(7), 2555-2568.

[31]

Nicksiar, M., & Martin, C. J. (2012). Evaluation of methods for determining crack initiation in compression tests on low-porosity rocks. Rock Mechanics and Rock Engineering, 45(4), 607-617.

[32]

Pimentel, E., & Anagnostou, G. (2013). New apparatus and experimental setup for long-term swelling tests on sulphatic claystones. Rock Mechanics and Rock Engineering, 46(6), 1271-1285.

[33]

Pimentel, E. (2015). Existing methods for swelling tests-a critical review. Environmental Earth Sciences, 76, 96-105.

[34]

Schweizer, D., Prommer, H., Blum, P., Siade, A. J., & Butscher, C. (2018). Reactive transport modeling of swelling processes in clay-sulfate rocks. Water Resources Research, 54(9), 6543-6565.

[35]

Serafeimidis, K., & Anagnostou, G. (2014). On the crystallisation pressure of gypsum. Environmental Earth Sciences, 72, 4985-4994.

[36]

Serafeimidis, K., & Anagnostou, G. (2013). On the time-development of sulphate hydration in anhydritic swelling rocks. Rock Mechanics and Rock Engineering, 46(3), 619-634.

[37]

Serafeimidis, K., & Anagnostou, G. (2015). The solubilities and thermodynamic equilibrium of anhydrite and gypsum. Rock Mechanics and Rock Engineering, 48(1), 15-31.

[38]

Sinha, S., Shirole, D., & Walton, G. (2020). Investigation of the micromechanical damage process in a granitic rock using an inelastic bonded block model (BBM). Journal of Geophysical Research: Solid Earth, 125(3), e2019JB018844.

[39]

Sinha, S., & Walton, G. (2020). A study on bonded block model (BBM) complexity for simulation of laboratory-scale stress-strain behavior in granitic rocks. Computers and Geotechnics, 118, 103363.

[40]

Steiner, W. (1993). Swelling rock in tunnels: Rock characterization, effect of horizontal stresses and construction procedures. International Journal of Rock Mechanics and Mining Sciences, 30(4), 361-380.

[41]

Su, C., Wei, S., Xu, C., & Su, F. (2019). Experimental study on physico-mechanical effects of high temperature dehydrated gypsum rock. Journal of Rock Mechanics and Engineering, 38(2), 254-266 (in Chinese).

[42]

Turichshev, A., & Hadjigeorgiou, J. (2017). Development of synthetic rock mass bonded block models to simulate the behaviour of intact veined rock. Geotechnical and Geological Engineering, 35(1), 313-335.

[43]

Vásárhelyi, B. (2005). Statistical analysis of the influence of water content on the strength of the Miocene limestone. Rock Mechanics and Rock Engineering, 38(1), 69-76.

[44]

Vásárhelyi, B., & Ván, P. (2006). Influence of initial water content on the strength of rock. Engineering Geology, 84(1/2), 70-74.

[45]

Wang, X., & Cai, M. (2019). A comprehensive parametric study of grain-based models for rock failure process simulation. International Journal of Rock Mechanics and Mining Sciences, 115, 60-76.

[46]

Wang, X., & Cai, M. (2018). Modeling of brittle rock failure considering inter- and intra-grain contact failures. Computers and Geotechnics, 101, 224-244.

[47]

Wang, Y., Li, X., Ben, Y. X., Wu, Y. F., & Zhang, B. (2014). Prediction of initiation stress of dilation of brittle rocks. Chinese Journal of Rock Mechanics and Engineering, 33(4), 737-746 (in Chinese).

[48]

Wanninger, T. (2019). Experimental investigations for the modelling of anhydritic swelling claystones. ETH Zurich (Zurich), Doctoral dissertation.

[49]

Xu, C. B., Hao, X. Y., & Wei, S. J. (2019). Experimental study on uniaxial compressive strength of water immersed anhydrite. Journal of Hydraulic Research and Development, 36, 86-92 (in Chinese).

[50]

Xu, C. B., Zhou, X. Y., Wang, H. L., Gao, X. J., & Li, X. F. (2021). A case study of thaumasite sulfate attack in tunnel engineering. Advances in Civil Engineering, 2021, 1-14.

[51]

Yan, B., Kang, H., Li, X., Qi, Q., Zhang, B., & Liu, J. (2023). Damage constitutive model and mechanical properties of jointed rock mass under hydro-mechanical coupling. Theoretical and Applied Fracture Mechanics, 123, 103735.

[52]

Yang, J. P., & Du, F. Y. (2016). The influence of temperature and humidity effect on water absorption softening of swelling rock. Science Technology and Engineering, 16(20), 259-263 (in Chinese).

[53]

Yang, X., Yuan, X., Wu, Z., & Su, C. (2001). Experimental study on mechanical properties of blasting damaged rock. Chinese Journal of Rock Mechanics and Engineering, 20, 436-439 (in Chinese).

[54]

Zhang, C. L., & Rothfuchs, T. (2004). Experimental study of the hydromechanical behaviour of the Callovo-Oxfordian argillite. Applied Clay Science, 26(1/2/3/4), 325-336.

[55]

Zhang, H. J., Adoko, A. C., Meng, Z. J., Wang, H., & Jiao, Y. Y. (2017). Mechanism of the mudstone tunnel failures induced by expansive clay minerals. Geotechnical and Geological Engineering, 35(1), 263-275.

[56]

Zhang, K., Xia, K., & Liu, F. (2021). Simulation of rock failure by Voronoi-based discontinuous deformation analysis. Chinese Journal of Rock Mechanics and Engineering, 40, 725-738 (in Chinese).

[57]

Zhang, K. Y., Liu, F., Xia, K. W., Xu, Y., Dong, P., & Yu, C. Y. (2023). On the calibration and verification of Voronoi-based discontinuous deformation analysis for modeling rock fracture. Journal of Rock Mechanics and Geotechnical Engineering, 15(8), 2025-2038.

[58]

Zhang, Q. B., & Wu, K. (2020). Research on the strength and expansive characteristics of full weathered mudstone in Karawang area. Journal of Railway Engineering Society, 37(8), 15-19 (in Chinese).

[59]

Zhang, S., Jiang, Q., Qiu, S., Li, S., Kou, Y., & Xu, D. (2025). Assessment of strain bursting using a Voronoi-based breakable block model: A case study of 2400-m-deep tunnels. Engineering Fracture Mechanics, 318, 110930.

[60]

Zhang, S. K., Leng, X. L., & Sheng, Q. (2020). Study of water swelling and softening characteristics of expansive rock. Rock and Soil Mechanics, 41(2), 561-570 (in Chinese).

[61]

Zhao, X., Cai, M., Wang, J., Li, P., & Ma, L. (2015). Objective determination of crack initiation stress of brittle rocks under compression using AE measurement. Rock Mechanics and Rock Engineering, 48, 2473-2484.

[62]

Zhong, Z. B., Li, A. H., Deng, R. G., Wu, P. P., & Jun, X. (2019). Experimental study on the time-dependent swelling characteristics of red-bed mudstone in Central Sichuan. Chinese Journal of Rock Mechanics and Engineering, 38(1), 76-86 (in Chinese).

[63]

Zhu, Y. B., Wu, Y. L., & Yu, H. M. (2013). Strength behavior of tunnel’s gypsiferous surrounding rock. Journal of Yangtze River Scientific Research Institute, 30, 53 (in Chinese).

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