Effect of forging on the microstructure and texture of a high Nb containing γ-TiAl alloy

Hui Tao, Hui-zhong Li, Li Wang, Rui Zhou, Yi-xuan Che, Yong-hui Chen, Xiao-peng Liang

Journal of Central South University ›› 2024, Vol. 31 ›› Issue (6) : 1763-1773. DOI: 10.1007/s11771-024-5677-5
Article

Effect of forging on the microstructure and texture of a high Nb containing γ-TiAl alloy

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Abstract

The effect of forging on the microstructure and texture evolution of a high Nb containing Ti-45Al-7Nb-0.3W (at.%) alloy was investigated by X-ray diffractometer (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The results show that the as-cast alloy is mainly composed of α 2/γ lamellar colonies with a mean size of 70 µm, but the hot-forged pancake displays a near duplex microstructure (DP). Kinking and bending of lamellar colonies, deformation twinning and dynamic recrystallization (DRX) occur during hot forging. Meanwhile, dense dislocations in the β phase after forging suggest that the high-temperature β phase with a disordered structure is favorable for improving the hot-workability of the alloy. Unlike the common TiAl casting texture, the solidification process of the investigated as-cast alloy with high Nb content is completely via the β phase region, resulting in the formation of a <110> γ fiber texture where the <110> γ aligns parallel to the heat-flow direction. In comparison, the relatively strong <001> and weak <302> texture components in the as-forged alloy are attributed to the deformation twinning. After annealing, static recrystallization occurs at the twin boundary and intersections, which weakens the deformation texture.

Keywords

high Nb containing γ-TiAl alloy / forging / microstructure / texture / β phase

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Hui Tao, Hui-zhong Li, Li Wang, Rui Zhou, Yi-xuan Che, Yong-hui Chen, Xiao-peng Liang. Effect of forging on the microstructure and texture of a high Nb containing γ-TiAl alloy. Journal of Central South University, 2024, 31(6): 1763‒1773 https://doi.org/10.1007/s11771-024-5677-5

References

[[1]]
Appel F, Oehring M, Wagner R. Novel design concepts for gamma-base titanium aluminide alloys [J]. Intermetallics, 2000, 8(9–11): 1283-1312,
CrossRef Google scholar
[[2]]
Bewlay B P, Nag S, Suzuki A, et al.. TiAl alloys in commercial aircraft engines [J]. Materials at High Temperatures, 2016, 33(4–5): 549-559,
CrossRef Google scholar
[[3]]
Li H-z, Long Y, Liang X-p, et al.. Effects of multiaxial forging on microstructure and high temperature mechanical properties of powder metallurgy Ti-45Al-7Nb-0.3W alloy [J]. Intermetallics, 2020, 116: 106647,
CrossRef Google scholar
[[4]]
Li Y-q, Xie F-q, Yang S-lin. Microstructure and hot corrosion resistance of Si-Al-Y coated TiAl alloy [J]. Journal of Central South University, 2020, 27(9): 2530-2537,
CrossRef Google scholar
[[5]]
Kong F-t, Cui N, Chen Y-y, et al.. Characterization of hot deformation behavior of as-forged TiAl alloy [J]. Intermetallics, 2014, 55: 66-72,
CrossRef Google scholar
[[6]]
Kothari K, Radhakrishnan R, Wereley N M. Advances in gamma titanium aluminides and their manufacturing techniques [J]. Progress in Aerospace Sciences, 2012, 55: 1-16,
CrossRef Google scholar
[[7]]
Xu S-h, Han M, Shen K-j, et al.. Fatigue properties of binary Ti-Ta metal-metal composite with lamellar microstructure [J]. Journal of Central South University, 2023, 30(9): 2878-2889,
CrossRef Google scholar
[[8]]
Wang L, Liang X-p, Jiang F-q, et al.. Phase transformation and deformation behavior of a TiAl - Nb composite under quasi-static and dynamic loadings [J]. Materials Science and Engineering A, 2022, 829: 142155,
CrossRef Google scholar
[[9]]
Huang H-l, Li D, Chen C, et al.. Selective laser melted near-beta titanium alloy Ti-5Al-5Mo-5V-1Cr-1Fe: Microstructure and mechanical properties [J]. Journal of Central South University, 2021, 28(6): 1601-1614,
CrossRef Google scholar
[[10]]
Li Y-z, Liu S-f, Zhang G-x, et al.. Effects of sintering temperature and holding time on microstructure and mechanical properties of Ti-1Al-8V-5Fe prepared by spark plasma sintering [J]. Journal of Central South University, 2021, 28(4): 1183-1194,
CrossRef Google scholar
[[11]]
Dong Z-w, Xia Y, Guo X-y, et al.. Preparing low-oxygen Ti-6Al-4V alloy powder through direct reduction of oxides and its synergistic reaction mechanism [J]. Journal of Central South University, 2022, 29(6): 1811-1822,
CrossRef Google scholar
[[12]]
Tang B, Cheng L, Kou H-c, et al.. Hot forging design and microstructure evolution of a high Nb containing TiAl alloy [J]. Intermetallics, 2015, 58: 7-14,
CrossRef Google scholar
[[13]]
Chen Z-x, Liu B, Liu Y, et al.. Microstructural evolution in a powder metallurgical Ti-7Mo alloy with continuous oxygen gradient [J]. Journal of Central South University, 2016, 23(3): 508-514,
CrossRef Google scholar
[[14]]
Qu S J, Tang S Q, Feng A H, et al.. Microstructural evolution and high-temperature oxidation mechanisms of a titanium aluminide based alloy [J]. Acta Materialia, 2018, 148: 300-310,
CrossRef Google scholar
[[15]]
Wallgram W, Schmölzer T, Cha L-m, et al.. Technology and mechanical properties of advanced γ-TiAl based alloys [J]. International Journal of Materials Research, 2009, 100(8): 1021-1030,
CrossRef Google scholar
[[16]]
Schloffer M, Iqbal F, Gabrisch H, et al.. Microstructure development and hardness of a powder metallurgical multi phase γ-TiAl based alloy [J]. Intermetallics, 2012, 22: 231-240,
CrossRef Google scholar
[[17]]
Qiang F-m, Kou H-c, Li Y-q, et al.. Enhanced strength-ductility synergy of β-solidifying TiAl alloy with preferred lamellar orientation by texturing high-temperature α phase through hot extrusion [J]. Materials Science and Engineering A, 2023, 885: 145626,
CrossRef Google scholar
[[18]]
Zhang D-d, Bao L-y, Li Q, et al.. Microstructure evolution and properties of powder metallurgy Ti43Al9V0.3Y alloy sheets at different rolling temperatures [J]. Materials Science and Engineering A, 2023, 866: 144685,
CrossRef Google scholar
[[19]]
Tao H, Li H-z, Wang L, et al.. Improvement on high-temperature tensile strength and ductility of selective electron beam melting TiAl alloys via small-strain forging [J]. Materials Science and Engineering A, 2023, 873: 145009,
CrossRef Google scholar
[[20]]
Luo Y-f, Liu B, Wang Y, et al.. Effect of texture on mechanical anisotropy of Ti-47Al-2Cr-0.2Mo intermetallics [J]. Intermetallics, 2022, 151: 107742,
CrossRef Google scholar
[[21]]
Zhang M-y, Zhang Y-q, Yu H, et al.. Revealing the deformation behavior and resultant texture evolution in extruded dilute Mg-Bi-Sn-Ca alloy during hot compression [J]. Materials Science and Engineering A, 2022, 853: 143788,
CrossRef Google scholar
[[22]]
Rouzbeh A, Atifeh S M, Sedighi M, et al.. Experimental investigation of strain path effects on mechanical properties, forming limit curves, and texture evolution of AA1050 aluminum sheet [J]. Journal of Central South University, 2023, 30(8): 2472-2484,
CrossRef Google scholar
[[23]]
Bartels A, Kestler H, Clemens H. Deformation behavior of differently processed γ-titanium aluminides [J]. Materials Science and Engineering: A, 2002, 329–331: 153-162,
CrossRef Google scholar
[[24]]
Schillinger W, Bartels A, Gerling R, et al.. Texture evolution of the γ- and the α/α 2-phase during hot rolling of γ-TiAl based alloys [J]. Intermetallics, 2006, 14(3): 336-347,
CrossRef Google scholar
[[25]]
Chen Y-h, Xiao Z-y, Li H-z, et al.. Anisotropy of TiAl alloy hot-rolling sheet [J]. The Chinese Journal of Nonferrous Metals, 2017, 27(6): 1148-1154 (in Chinese)
[[26]]
Brokmeier H G, Oehring M, Lorenz U, et al.. Neutron diffraction study of texture development during hot working of different gamma-titanium aluminide alloys [J]. Metallurgical and Materials Transactions A, 2004, 35(11): 3563-3579,
CrossRef Google scholar
[[27]]
Bystrzanowski S, Bartels A, Clemens H, et al.. Creep behaviour and related high temperature microstructural stability of Ti-46Al-9Nb sheet material [J]. Intermetallics, 2005, 13(5): 515-524,
CrossRef Google scholar
[[28]]
Yang W-g, Li M-g, Zhou T, et al.. Deformation behavior and dynamic recrystallization mechanism of a novel high Nb containing TiAl alloy in (α+γ) dual-phase field [J]. Journal of Alloys and Compounds, 2023, 945: 169250,
CrossRef Google scholar
[[29]]
Lavasani N N, Jafarian H R, Arabi H, et al.. Texture analysis and development of ultrafine grained structure during thermo-mechanical treatment in a gamma-TiAl intermetallic [J]. Materials Science and Engineering A, 2018, 711: 259-267,
CrossRef Google scholar
[[30]]
Yuan Y, Liu H W, Zhao X N, et al.. Dissociation of superdislocations and the stacking fault energy in TiAl based alloys with Nb-doping [J]. Physics Letters A, 2006, 358(3): 231-235,
CrossRef Google scholar
[[31]]
Li H-z, Che Y-x, Liang X-p, et al.. Microstructure and high-temperature mechanical properties of near net shaped Ti-45Al-7Nb-0.3W alloy by hot isostatic pressing process [J]. Transactions of Nonferrous Metals Society of China, 2020, 30(11): 3006-3015,
CrossRef Google scholar
[[32]]
Nieh T G, Hsiung L M, Wadsworth J. Superplastic behavior of a powder metallurgy TiAl alloy with a metastable microstructure [J]. Intermetallics, 1999, 7(2): 163-170,
CrossRef Google scholar
[[33]]
Appel F, Paul J D H, Oehring M. . Gamma titanium aluminide alloys: Science and technology [M], 2011 Weinheim Wiley,
CrossRef Google scholar
[[34]]
Hsiung L M, Nieh T G, Choi B W, et al.. Interfacial dislocations and deformation twinning in fully lamellar TiAl [J]. Materials Science and Engineering A, 2002, 329–331: 637-643,
CrossRef Google scholar
[[35]]
Chen Y-y, Li L, Li H, et al.. Dynamic recrystallization mechanism and twinning behavior in hot deformation of Ti-46.5Al-2Nb-2Cr with initial duplex microstructure [J]. Materials Characterization, 2023, 197: 112678,
CrossRef Google scholar
[[36]]
Wang P, Tan X-p, Nai M L S, et al.. Deformation induced nanoscale twinning improves strength and ductility in additively manufactured titanium alloys [J]. Materials Science and Engineering A, 2022, 833: 142568,
CrossRef Google scholar
[[37]]
Xu X-s, Ding H-s, Huang H-t, et al.. Twinning-induced dislocation and coordinated deformation behavior of a high-Nb TiAl alloy during high-cycle fatigue [J]. International Journal of Fatigue, 2023, 171: 107597,
CrossRef Google scholar
[[38]]
Sankaran A, Bouzy E, Fundenberger J J, et al.. Texture and microstructure evolution during tempering of gamma-massive phase in a TiAl-based alloy [J]. Intermetallics, 2009, 17(12): 1007-1016,
CrossRef Google scholar
[[39]]
Ohnuma I, Fujita Y, Mitsui H, et al.. Phase equilibria in the Ti-Al binary system [J]. Acta Materialia, 2000, 48(12): 3113-3123,
CrossRef Google scholar
[[40]]
Guyon J, Hazotte A, Bouzy E. Evolution of metastable α phase during heating of Ti48Al2Cr2Nb intermetallic alloy [J]. Journal of Alloys and Compounds, 2016, 656: 667-675,
CrossRef Google scholar
[[41]]
Jin Y-g, Wang J N, Yang J, et al.. Microstructure refinement of cast TiAl alloys by β solidification [J]. Scripta Materialia, 2004, 51(2): 113-117,
CrossRef Google scholar
[[42]]
Chen G, Peng Y-b, Zheng G, et al.. Polysynthetic twinned TiAl single crystals for high-temperature applications [J]. Nature Materials, 2016, 15(8): 876-881,
CrossRef Google scholar
[[43]]
Hartig C, Fukutomi H, Mecking H, et al.. Texture and microstructure of Ti-49at% Al after dynamic recrystallization and annealing [J]. ISIJ International, 1993, 33(2): 313-320,
CrossRef Google scholar

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