Improving creep strength of the fine-grained heat-affected zone of novel 9Cr martensitic heat-resistant steel via modified thermo-mechanical treatment

Jingwen Zhang, Liming Yu, Yongchang Liu, Ran Ding, Chenxi Liu, Zongqing Ma, Huijun Li, Qiuzhi Gao, Hui Wang

International Journal of Minerals, Metallurgy, and Materials ›› 2024, Vol. 31 ›› Issue (5) : 1037-1047. DOI: 10.1007/s12613-023-2760-0
Research Article

Improving creep strength of the fine-grained heat-affected zone of novel 9Cr martensitic heat-resistant steel via modified thermo-mechanical treatment

Author information +
History +

Abstract

The infamous type IV failure within the fine-grained heat-affected zone (FGHAZ) in G115 steel weldments seriously threatens the safe operation of ultra-supercritical (USC) power plants. In this work, the traditional thermo-mechanical treatment was modified via the replacement of hot-rolling with cold rolling, i.e., normalizing, cold rolling, and tempering (NCT), which was developed to improve the creep strength of the FGHAZ in G115 steel weldments. The NCT treatment effectively promoted the dissolution of preformed M23C6 particles and relieved the boundary segregation of C and Cr during welding thermal cycling, which accelerated the dispersed reprecipitation of M23C6 particles within the fresh reaustenitized grains during post-weld heat treatment. In addition, the precipitation of Cu-rich phases and MX particles was promoted evidently due to the deformation-induced dislocations. As a result, the interacting actions between precipitates, dislocations, and boundaries during creep were reinforced considerably. Following this strategy, the creep rupture life of the FGHAZ in G115 steel weldments can be prolonged by 18.6%, which can further push the application of G115 steel in USC power plants.

Keywords

G115 steel / fine-grained heat-affected zone / creep strength / element segregation / nano-sized precipitates

Cite this article

Download citation ▾
Jingwen Zhang, Liming Yu, Yongchang Liu, Ran Ding, Chenxi Liu, Zongqing Ma, Huijun Li, Qiuzhi Gao, Hui Wang. Improving creep strength of the fine-grained heat-affected zone of novel 9Cr martensitic heat-resistant steel via modified thermo-mechanical treatment. International Journal of Minerals, Metallurgy, and Materials, 2024, 31(5): 1037‒1047 https://doi.org/10.1007/s12613-023-2760-0

References

[[1]]
Dak G, Pandey C. A critical review on dissimilar welds joint between martensitic and austenitic steel for power plant application. J. Manuf. Process., 2020, 58: 377,
CrossRef Google scholar
[[2]]
J.W. Zhang, L.M. Yu, Q.Z. Gao, et al., Creep behavior, microstructure evolution and fracture mechanism of a novel martensite heat resistance steel G115 affected by prior cold deformation, Mater. Sci. Eng. A, 850(2022), art. No. 143564.
[[3]]
He HS, Yu LM, Liu CX, Li HJ, Gao QZ, Liu YC. Research progress of a novel martensitic heat-resistant steel G115. Acta Metall. Sin., 2022, 58(3): 311
[[4]]
Xu LQ, Zhang DT, Liu YC, et al.. Precipitation behavior and martensite lath coarsening during tempering of T/P92 ferritic heat-resistant steel. Int. J. Miner. Metall. Mater., 2014, 21(5): 438,
CrossRef Google scholar
[[5]]
Zhou JH, Shen YF, Jia N. Strengthening mechanisms of reduced activation ferritic/martensitic steels: A review. Int. J. Miner. Metall. Mater., 2021, 28(3): 335,
CrossRef Google scholar
[[6]]
Q.Z. Gao, Z. Yuan, Q.S. Ma, L.M. Yu, and H.J. Li, Strengthening and toughening optimizations of novel G115 martensitic steel: Utilizing secondary normalizing process, Mater. Sci. Eng. A, 852(2022), art. No. 143621.
[[7]]
H.S. He, J.W. Zhang, L.M. Yu, et al., Effects of Cu-rich phases on microstructure evolution and creep deformation behavior of a novel martensitic heat-resistant steel G115, Mater. Sci. Eng. A, 855(2022), art. No. 143937.
[[8]]
Liu Z, Liu ZD, Wang XT, Chen ZZ. Investigation of the microstructure and strength in G115 steel with the different concentration of tungsten during creep test. Mater. Charact., 2019, 149: 95,
CrossRef Google scholar
[[9]]
Z. Liu, X.T. Wang, and C. Dong, Effect of boron on G115 martensitic heat resistant steel during aging at 650°C, Mater. Sci. Eng. A, 787(2020), art. No. 139529.
[[10]]
Xiao B, Xu LY, Cayron C, Xue J, Sha G, Logé R. Solute-dislocation interactions and creep-enhanced Cu precipitation in a novel ferritic-martensitic steel. Acta Mater., 2020, 195: 199,
CrossRef Google scholar
[[11]]
Liu Z, Liu ZD, Wang XT, Chen ZZ, Ma LT. Evolution of the microstructure in aged G115 steels with the different concentration of tungsten. Mater. Sci. Eng. A, 2018, 729: 161,
CrossRef Google scholar
[[12]]
Z. Liu, Z.D. Liu, X.T. Wang, C. Dong, Z.Z. Chen, and H.S. Bao, The microstructural evolution and mechanical property in G115 steels during long-term aging at 650°C, Mater. Res. Express, 6(2019), No. 11, art. No. 116527.
[[13]]
Y.H. Yu, Z.D. Liu, C. Zhang, et al., Correlation of creep fracture lifetime with microstructure evolution and cavity behaviors in G115 martensitic heat-resistant steel, Mater. Sci. Eng. A, 788(2020), art. No. 139468.
[[14]]
Wang ZW, Zhang M, Li C, et al.. Achieving a high-strength dissimilar joint of T91 heat-resistant steel to 316L stainless steel via friction stir welding. Int. J. Miner. Metall. Mater., 2023, 30(1): 166,
CrossRef Google scholar
[[15]]
J.W. Zhang, L.M. Yu, R. Ding, et al., Deformation behavior, microstructure evolution, and rupture mechanism of the novel G115 steel welded joint during creep, Mater. Charact., 205(2023), art. No. 113275.
[[16]]
Pandey C, Mahapatra MM, Kumar P. Effect of post weld heat treatments on fracture frontier and type IV cracking nature of the crept P91 welded sample. Mater. Sci. Eng. A, 2018, 731: 249,
CrossRef Google scholar
[[17]]
Wang YY, Kannan R, Li LJ. Correlation between inter-critical heat-affected zone and type IV creep damage zone in grade 91 steel. Metall. Mater. Trans. A, 2018, 49(4): 1264,
CrossRef Google scholar
[[18]]
J.W. Zhang, L.M. Yu, Q.Z. Gao, et al., A new strategy to improve the creep strength of a novel G115 steel by accelerating the precipitation of nano-sized MX and Cu-rich particles, Scripta Mater., 220(2022), art. No. 114903.
[[19]]
Hoffmann J, Rieth M, Klimenkov M, Baumgärtner S. Improvement of EUROFER’s mechanical properties by optimized chemical compositions and thermo-mechanical treatments. Nucl. Mater. Energy, 2018, 16: 88,
CrossRef Google scholar
[[20]]
Hollner S, Fournier B, Le Pendu J, et al.. High-temperature mechanical properties improvement on modified 9Cr–1Mo martensitic steel through thermomechanical treatments. J. Nucl. Mater., 2010, 405(2): 101,
CrossRef Google scholar
[[21]]
Klueh RL, Hashimoto N, Maziasz PJ. New nanoparticle-strengthened ferritic/martensitic steels by conventional thermo-mechanical treatment. J. Nucl. Mater., 2007, 367–370: 48,
CrossRef Google scholar
[[22]]
Sakthivel T, Shruti P, Parameswaran P, Rao GVSN, Laha K, Rao TS. Enhancement in creep strength of modified 9CR–1MO steel through thermo-mechanical treatment. Trans. Indian Inst. Met., 2017, 70(5): 1177,
CrossRef Google scholar
[[23]]
Vivas J, Capdevila C, Altstadt E, Houska M, San-Martín D. Importance of austenitization temperature and ausforming on creep strength in 9Cr ferritic/martensitic steel. Scripta Mater., 2018, 153: 14,
CrossRef Google scholar
[[24]]
Sakthivel T, Nandeswarudu SM, Shruti P, et al.. An improvement in creep strength of thermo-mechanical treated modified 9Cr–1Mo steel weld joint. Mater. High Temp., 2019, 36(1): 76,
CrossRef Google scholar
[[25]]
Prakash P, Vanaja J, Srinivasan N, Parameswaran P, Rao GVSN, Laha K. Effect of thermo-mechanical treatment on tensile properties of reduced activation ferritic-martensitic steel. Mater. Sci. Eng. A, 2018, 724: 171,
CrossRef Google scholar
[[26]]
Nöhrer M, Mayer W, Primig S, Zamberger S, Kozeschnik E, Leitner H. Influence of deformation on the precipitation behavior of Nb(CN) in austenite and ferrite. Metall. Mater. Trans. A, 2014, 45(10): 4210,
CrossRef Google scholar
[[27]]
Prakash P, Vanaja J, Reddy GVP, Laha K, Rao GVSN. On the effect of thermo-mechanical treatment on creep deformation and rupture behaviour of a reduced activation ferriticmartensitic steel. J. Nucl. Mater., 2019, 520: 65,
CrossRef Google scholar
[[28]]
Shassere BA, Yamamoto Y, Babu SS. Toward improving the type IV cracking resistance in Cr–Mo steel weld through thermo-mechanical processing. Metall. Mater. Trans. A, 2016, 47(5): 2188,
CrossRef Google scholar
[[29]]
Yan P, Liu ZD, Bao HS, Weng YQ, Liu W. Effect of normalizing temperature on the strength of 9Cr–3W–3Co martensitic heat resistant steel. Mater. Sci. Eng. A, 2014, 597: 148,
CrossRef Google scholar
[[30]]
Yan P, Liu ZD, Bao HS, Weng YQ, Liu W. Effect of tempering temperature on the toughness of 9Cr–3W–3Co martensitic heat resistant steel. Mater. Des., 2014, 54: 874,
CrossRef Google scholar
[[31]]
Zhang JW, Yu LM, Gao QZ, et al.. Development of weld filler material to match the advanced martensitic heat resistance steel G115 and tailoring the performance by tempering temperature. J. Mater. Res. Technol., 2022, 21: 2515,
CrossRef Google scholar
[[32]]
Vivas J, Capdevila C, Altstadt E, Houska M, Sabirov I, San-Martín D. Microstructural degradation and creep fracture behavior of conventionally and thermomechanically treated 9% chromium heat resistant steel. Met. Mater. Int., 2019, 25(2): 343,
CrossRef Google scholar
[[33]]
Khajuria A, Akhtar M, Bedi R, et al.. Microstructural investigations on simulated intercritical heat-affected zone of boron modified P91-steel. Mater. Sci. Technol., 2020, 36(13): 1407,
CrossRef Google scholar
[[34]]
Dunđer M, Vuherer T, Samardžić I, Marić D. Analysis of heat-affected zone microstructures of steel P92 after welding and after post-weld heat treatment. Int. J. Adv. Manuf. Technol., 2019, 102(9–12): 3801,
CrossRef Google scholar
[[35]]
A. Khajuria, M. Akhtar, R. Bedi, et al., Influence of boron on microstructure and mechanical properties of Gleeble simulated heat-affected zone in P91 steel, Int. J. Press. Vessels Pip., 188(2020), art. No. 104246.
[[36]]
Pandey C, Mahapatra MM, Kumar P, Thakre JG, Saini N. Role of evolving microstructure on the mechanical behaviour of P92 steel welded joint in as-welded and post weld heat treated state. J. Mater. Process. Technol., 2019, 263: 241,
CrossRef Google scholar
[[37]]
H.Y. Azad, S.H.M. Anijdan, and H. Najafi, The effect of PWHT on the microstructural evolution, carbides formation and mechanical properties of a Nb containing martensitic heat resistance steel used in gas turbine, Mater. Sci. Eng. A, 793(2020), art. No. 139810.
[[38]]
Z. Liu, Z.D. Liu, Z.Z. Chen, X.T. Wang, H.S. Bao, and C. Dong, Microstructure and creep strength evolution in G115 steel during creep at 650°C, Mater. Res. Express, 7(2020), No. 1, art. No. 016528.
[[39]]
Gao QZ, Wang C, Qu F, Wang YL, Qiao ZX. Martensite transformation kinetics in 9Cr–1.7W–0.4Mo–Co ferritic steel. J. Alloys Compd., 2014, 610: 322,
CrossRef Google scholar
[[40]]
Liu Y, Tsukamoto S, Shirane T, Abe F. Formation mechanism of type IV failure in high Cr ferritic heat-resistant steel-welded joint. Metall. Mater. Trans. A, 2013, 44(10): 4626,
CrossRef Google scholar
[[41]]
Matsunaga T, Hongo H, Tabuchi M, Sahara R. Suppression of grain refinement in heat-affected zone of 9Cr–3W–3Co–VNb steels. Mater. Sci. Eng. A, 2016, 655: 168,
CrossRef Google scholar
[[42]]
Liang Y, Yan W, Shi XB, et al.. On Laves phase in a 9Cr3W3CoB martensitic heat resistant steel when aged at high temperatures. J. Mater. Sci. Technol., 2021, 85: 129,
CrossRef Google scholar
[[43]]
F. Abe, Precipitate design for creep strengthening of 9% Cr tempered martensitic steel for ultra-supercritical power plants, Sci. Technol. Adv. Mater., 9(2008), No. 1, art. No. 013002.
[[44]]
Abe F. Gianfrancesco AD. New martensitic steels. Materials for Ultra-Supercritical and Advanced Ultra-Supercritical Power Plants, 2017 Cambridge Woodhead Publishing 323,
CrossRef Google scholar
[[45]]
Abe F, Igarashi M, Wanikawa S, et al.. Neumann P, Allen D, Teuckhoff E, et al.. Ultra steel project for advanced ferritic steels for 650°C USC boilers. Steels and Materials for Power Plants, 2000 Weinheim Wiley-VCH Verlag GmbH 299,
CrossRef Google scholar
[[46]]
Wang YK, Ma QS, Gao QZ, et al.. Precipitation and strengthening behavior of M23C6 carbides in tempered G115 steel. JOM, 2022, 74(12): 4755,
CrossRef Google scholar
[[47]]
Wang H, Yan W, van Zwaag S, et al.. On the 650°C thermostability of 9–12Cr heat resistant steels containing different precipitates. Acta Mater., 2017, 134: 143,
CrossRef Google scholar
[[48]]
J. Vivas, D. De-Castro, E. Altstadt, M. Houska, D. San-Martín, and C. Capdevila, Design and high temperature behavior of novel heat resistant steels strengthened by high density of stable nanoprecipitates, Mater. Sci. Eng. A, 793(2020), art. No. 139799.
[[49]]
Vivas J, Capdevila C, Altstadt E, et al.. Effect of ausforming temperature on creep strength of G91 investigated by means of small punch creep tests. Mater. Sci. Eng. A, 2018, 728: 259,
CrossRef Google scholar
[[50]]
Benaarbia A, Xu X, Sun W, Becker AA, Jepson MAE. Investigation of short-term creep deformation mechanisms in MarBN steel at elevated temperatures. Mater. Sci. Eng. A, 2018, 734: 491,
CrossRef Google scholar
[[51]]
Kipelova A, Belyakov A, Kaibyshev R. Laves phase evolution in a modified P911 heat resistant steel during creep at 923 K. Mater. Sci. Eng. A, 2012, 532: 71,
CrossRef Google scholar
[[52]]
Prat O, Garcia J, Rojas D, Carrasco C, Inden G. Investigations on the growth kinetics of Laves phase precipitates in 12% Cr creep-resistant steels: Experimental and DICTRA calculations. Acta Mater., 2010, 58(18): 6142,
CrossRef Google scholar

Accesses

Citations

Detail

Sections
Recommended

/