Synthesis of -amino--keto-esters (-oxodipeptides)

ISSN 1673-3495 (Print) ISSN 1673-3614 (Online) CN 11-5726/O6 (Ceased publications)

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Synthesis of -amino--keto-esters (-oxodipeptides)

Front. Chem. China ›› 2008, Vol. 3 ›› Issue (4) : 485 -488.

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Front. Chem. China ›› 2008, Vol. 3 ›› Issue (4) : 485 -488. DOI: 10.1007/s11458-008-0067-3

Synthesis of -amino--keto-esters (-oxodipeptides)

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Abstract

The synthesis of ?-amino-?-keto-esters (?-oxo dipeptides) was studied. Corresponding ?-amino-?-keto-esters were prepared from BOC-(L)-Valine and BOC-(L)-isoleucine by coupling with (D,L)-threonine hydrochloride and oxidation with Dess-Martin periodinane (DMP) with a total yield of 48% and 38%, respectively.

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α-amino-β-keto-esters / dipeptide / oxidation / Dess-Martin Periodinane (DMP)

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null. Synthesis of -amino--keto-esters (-oxodipeptides). Front. Chem. China, 2008, 3(4): 485-488 DOI:10.1007/s11458-008-0067-3

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